Papers by Author: Vincent Klosek

Abstract: A theoretical and experimental study was carry out to investigate deformation mechanisms in a textured titanium alloy. In situ neutron diffraction measurements were performed to analyze different {hk.l} family planes ({10.0}, {10.1}, {11.0} and {00.2}) and determine the corresponding internal strain pole figures. This method was applied to a pure titanium (a-Ti) submitted to a uniaxial tensile load up to 2 %. The experimental data was then used to validate the EPSC model in order to predict the distribution of lattice strains determined by neutron diffraction for various diffraction vector directions. This comparison reveals that the model results were in good agreement with the experimental data and the simulations reproduced the lattice strain development observed on the strain pole figures determined by neutron diffraction.

Abstract: The TOF neutron diffraction measurements were done for Al/SiC_p metal–matrix composite (17% of SiC) subjected to T6 thermal treatment. Using three separated diffraction peaks of SiC phase and four peaks of Al phase, the lattice strains were measured for both phases independently during in situ tensile test. The experimental results were presented in comparison with elastoplastic model, which allows to find the values of parameters determining plastic deformation of Al matrix (critical resolved shear stress and hardening parameter). Additionally, the results of TOF method were compared with those which were obtained with monochromatic neutron radiation (LLB, Saclay). In the latter experiment Al/SiC_p composite containing 25% of SiC was measured. It was shown that after elastoplastic deformation the mismatch stresses determined for both phases relax during tensile deformation.

Abstract: This study is an experimental comparison of in-depth X-ray diffraction residual stress measurements with neutron diffraction measurements. The goal is to evaluate the relevance of the Savaria-Bridier-Bocher [1] stress relaxation correction method. Neutron diffraction are performed on a bent notched specimen. Destructive X-ray diffraction is performed until 5.25mm below the surface by polishing the material. This polishing induces stress relaxation and X-ray diffraction results have to be corrected. For that purpose, a finite element analysis is realised and show good correlation with neutron measurements results. The application of the stress correction method improves the X-ray measurements especially after 2 mm below the surface. The differences between measured and corrected residual stresses from both diffraction techniques are analyzed and discussed.

Abstract: Diffraction methods for lattice strain measurement provide useful information concerning the nature of grains behaviour during elastoplastic deformation. The main advantage of the diffraction methods is the possibility of studying mechanical properties of polycrystalline materials separately in each phase and in groups of grains with a specific orientation. In this work we present application of the neutron and X-ray diffraction to study “in situ” deformation of two phase stainless steels during tensile loading. The experimental results are compared with self-consistent model.

Abstract: This work aims to study by neutron diffraction the evolution of metastable phases of CuAlBe shape memory alloy after plastic deformation. Two samples were studied: the first one deformed by cold rolling at a reduction rate of 15% and the second, deformed by cold rolling at 15% followed by hot rolling at 200°C for a reduction rate of 30% respectively. Before plastic deformation, the material is fully austenitic at ambient temperature. Its crystallographic texture is mainly characterized by a <001> partial fibber. After deformation, this partial fibber disappears and the crystallographic texture is composed by isolated orientations. At higher reduction rates, the texture of austenitic phase remaining in the material is characterized by a <111> fibber. The rolling process modifies metastable phase quantities. After deformation at a reduction rate of 15%, the volume fraction of metastable austenite remaining is close to 8%. Plastic deformation also greatly modifies the characteristic transformation temperatures and enlarges the hysteresis. The material plastically deformed after hot rolling presents large variations of intensities of diffraction peaks belonging to martensite phase during a thermal cycle at low temperature. This effect is attributed to a reorganization of variants due to an evolution of crystallographic texture of martensite.

Abstract: The aim of the present work is to study effects occurring during elatoplastic deformation and unloading of Al/SiCp metal–matrix composite material. We have measured lattice strains for both phases independently using two separated diffraction peaks (the 111 reflections of Al and SiC) during in situ tensile testing. Lattice strains were measured in the direction parallel to the applied load. The results were compared with an elastoplastic model in order to find parameters determining the plastic deformation of Al matrix (critical resolved shear stress and hardening parameter). We have found that during initial deformation relaxation of the thermal stresses occurs in both phases. Afterwards, the distribution of strains measured during the in situ test and unloading of the sample agree very well with self-consistent model prediction.

Abstract: In this work a new method for analysis of neutron diffraction results obtained during “in situ” tensile load is proposed and tested. The methodology is based on the measurements of lattice strains during “in situ” tensile test for several hkl reflections and for different orientations of the sample with respect to the scattering vector. As the result the full stress tensor for preferred texture orientations in function of applied stress can be determined with help of crystallite group method. The experimental data are presented and compared with self-consistent model calculations performed for groups of grains corresponding to the measured hkl reflections.

Abstract: This work was devoted to the study of a copper based shape memory alloy using the neutron diffraction method. We present the crystallographic texture evolution of the austenite phase of the Cu-11%Al-0.62%Be (wt. %) alloy which was subjected to cold and hot rolling processes. The texture of the cold rolled samples at reduction rates of 5%, 10% and 15% respectively was measured and compared to the raw material. A <001> partial fiber is observed for the raw material and for cold rolled samples whereas the texture of the hot rolled sample is mainly characterized by a <111> fiber. On the second part, we have studied the influence of the rolling treatment on the transition temperatures by following the integrated intensity of the {220} austenite reflection. The increase of the rolling rate seems to shift the characteristic temperatures towards low temperatures.

Abstract: This work presents the texture evolution of the austenitic phase of a copper based shape memory alloy by neutron diffraction. The Cu-11%Al-0.62%Be (in mass %) alloy was subjected to cold and hot rolling processes. The texture of the rolled samples at reduction rates of 5%, 10% and 15% respectively were compared to those of the raw material. A <001> partial fiber is observed for the raw material and cold rolled samples whereas the texture of the hot rolled sample is mainly characterized by a <111> fiber. The influence of these mechanical treatments on the transition temperatures and the hysteresis evolution was also analysed by following the integrated intensity of the {220} reflection of the austenitic phase. A shift towards low temperatures of martensitic transition temperatures is observed with the increasing of the rolling rate.

Abstract: Dissimilar metal joints between pipes of ferritic and austenitic steels are present in primary coolant circuit of pressurized water reactors. Over the last years in particular in USA and Japan, stress corrosion cracks, often associated with weld repairs, have been observed for some dissimilar welds made with an Inconel filler metal. The integrity of this type of components is thus a major safety issue. In this context, the goal of this work is to evaluate the welding residual stresses field for a dissimilar weld joint. A representative bi-metallic tubular weld joint was fabricated and residual stresses profiles in the different weld zones were evaluated by means of the hole drilling and neutron diffraction methods.