Authors: Zu Qing Sun, Long Fei Li, Wang Yue Yang
Abstract: Dynamic recrystallization(DRX) of ferrite in low carbon steels was investigated by hot
compression tests at temperatures of 550 to 700oC at strain rates of 0.001 to 10s-1. The results indicate
that DRX of ferrite can occur in low carbon steels and lead to grain refinement. With increasing
Zener-Hollomon parameter Z, its mechanism changes from discontinuous dynamic recrystallization
to continuous dynamic recrystallization, the turning point is approximately at Z=1×1016s-1 for a low
carbon steel with 0.171wt% C. The results also indicate that changing the minor constituents of the
low carbon steel from pearlite colonies to fine cementite particles has an effect on promoting DRX of
ferrite, and the increase of Mn content and the presence of tiny Nb precipitates have opposite effects
respectively. However, all these changes are of benefit to the refinement of recrystallized grains.
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Authors: Ping Yang, Wang Yue Yang, Zu Qing Sun
Abstract: Texture evolutions are determined by XRD and EBSD techniques during ferrite
refinement through deformation-enhanced ferrite transformation (DEFT) and dynamic recrystallization (DREX). Evidences of transformation texture, deformation texture and recrystallization texture during DEFT are provided and compared with the texture during DREX. The influence of pass-interval during DEFT on texture is illustrated. Results are discussed in terms of the influences of ferrite grain size and deforming temperature.
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Authors: Long Fei Li, Wang Yue Yang, Zu Qing Sun
Abstract: The hot deformation behavior of a low carbon Nb-microalloyed steel is investigated by hot compression test in the ferrite phase region compared with a low carbon steel with similar compositions, and the effect of Nb on dynamic recrystallization of ferrite is analyzed. Results indicate that during hot deformation in the ferrite phase region, the effect of Nb solely depends on the size of NbC precipitates. Tiny particles which average size is about 7.5nm have a retarding effect on dynamic recrystallization process of ferrite, on the contrary, coarser particles which average size is about 30.6nm have a promoting effect and are of benefit to the refinement of recrystallized grains.
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Authors: Guoan Chen, Wang Yue Yang, Shou Zhen Guo, Zu Qing Sun
Abstract: By using TEM strain-induced precipitation of Nb(CN) during deformation of undercooled austenite was investigated in Nb-microalloyed steel. The results showed that at 1200°C all of Nb were dissolved and there were no Nb(CN) precipitates formed during cooling until down to 760°C; During deformation enhanced ferrite transformation Nb(CN) of dynamic precipitation required an incubation
period, but compared with isothermal transformation it reduced significantly. Only when the strain increased to 0.69, Nb(CN) began to precipitate on dislocation nodes and grain boundaries. Furthermore the volume fraction of Nb(CN) precipitation increased with increasing strain but their coarsening wasn’t significant. Results showed that the measured grain size is in good agreement with
the calculated value.
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Authors: Jun Jie Qi, Wang Yue Yang, Zu Qing Sun, X. Zhang
Abstract: Quantitative characterization of microstructural development during deformation
enhanced transformation in a low carbon steel was investigated on a Gleeble 1500 machine. General conclusions of the features of austenite transformation kinetics during deformation-enhanced transformation were formulated. It was shown that the process of deformation-enhanced transformation can be divided into three stages according to the characteristics of transformation kinetics: The kinetics equations of two early stages fitted well in J-M-A equation. The kinetics of the first stage obeys Cahn’s site saturation mechanism, with the value of kinetics parameter n of 4. Ferrite nucleates at austenite grain boundaries and triple points during the first stage. Kinetics of the second stage doesn’t obey Cahn’s theory, with the value of kinetics parameter n of 1-1.5, corresponding to ferrite nucleation repeatedly at areas with high stored energy in front of the ferrite/austenite interface. The kinetics doesn’t obey the law of J-M-A equation any more in the final stage, and only few
nucleation sites left at this moment.
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Authors: Zu Qing Sun, Wang Yue Yang, Jun Jie Qi
Abstract: The concept of deformation-enhanced transformation of ferrite in plain low carbon steel is introduced. The characteristics are presented. Systematic works conclude that deformation significantly enhances the ferrite transformation of undercooled austenite in plain low carbon steel. Nucleation is the dominant process of the transformation. Until the completion of the transformation, nucleation is always repeated, especially at the zone in front of the newly formed ferrite grains, which restrict the grain growth and lead to formation of very fine ferrite grains. Three stages of kinetics are clearly shown from the experimental measurement, which correspond to nucleation at grain boundaries, at the zone in front of newly formed ferrite grains and within residual austenite.
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