Papers by Author: Wen Jiang Ding

Abstract: The microstructure and mechanical properties of Mg95.9Zn3.5Gd0.6 and Mg94.4Zn3.5Gd0.6Cu1.5 alloys reinforced by icosahedral quasicrystalline phase (I-phase) and Laves phase has been studied after extrusion at 573K. Extrusion can significantly refined the I-phase and Laves phase, and the strengthening effect of I-phase and Laves phase has been analyzed. Large volume of icosahedral phase in Mg95.9Zn3.5Gd0.6 has important role in its high UTS and elongation due to strong bonding effect at the I-phase/matrix interface for low interface energy. The Laves phase with cubic topological and close-packed structure in Mg94.4Zn3.5Gd0.6Cu1.5 alloy result in the higher heat resistance at elevated temperatures.

Abstract: Microstructure and mechanical properties of Mg-6.0wt%Zn-0.5wt%Zr (ZK60) alloy were studied as a function of cooling rate. The temperature field and cooling rate during the casting process were investigated by use of finite element analysis (FEA) simulation. The results showed that the microstructure was refined and the eutectic phase distributed much uniformly with the increase of cooling rate. The increase of yield strength, ultimate strength and elongation can be ascribed to the strengthening effect of fine grain. Relationship between grain size and yield strength is consistent with the Hall-Petch formalism: 1/ 2 80.37 132.56 − = + d y σ .

Abstract: The effect of second-phase particles on the grain refinement of AZ61 and AZ91 Mg-Al-Zn alloys with different volume fractions of β-Mg17Al12 phase particles during equal channel angular extrusion (ECAE) has been investigated. The microstructure were observed by optical microscopy (OM), scanning electron microscopy (SEM) and transmission electron microscopy (TEM), which revealed that grain refinement was enhanced by second phase particles at initial stage of ECAE. And finer grains with the high angle grain boundaries (HAGBs) and disperse second-phase particles could be obtained in AZ61 and AZ91 after 8 passes of ECAE.

Abstract: Microstructure and tensile properties of AZ31 rolled at different temperatures were characterized. Rolling of extruded AZ31 plates was carried out at room temperature, 573K, 623K and 673K. Cold rolling of extruded AZ31 plates was difficult due to the poor formability at room temperature. And deformation twinning plays an important role in rolling of AZ31 alloy at room temperature. The microstructural analysis showed that the nucleation of dynamic recrystallization (DRX) occurred at 573K, DRX was almost completed at 623K and grain growth was determined at 673K. The ultimate tensile strength (UTS) as large as 377MPa was achieved after rolled at 573K. And the anisotropy in strength was obviously examined due to the rolling texture. The anisotropy reduced as rolling temperature increasing from 573K to 673K and this may be attributed to the completion of DRX.

Abstract: Effects of extrusion on mechanical properties and damping capacity of Mg-1.8wt.%Cu -0.5wt.%Mn (MCM1805) alloy have been investigated. Tensile tests and dynamic mechanical analyzer were respectively used to measure tensile properties and damping capacity at room temperature of as-cast and as-extruded MCM1805 alloy. The microstructure was studied using optical microscope, X-ray diffraction and scanning electron microscope with an energy dispersive X-ray spectrometer. Granato-Lücke model was used to explain the influences of extrusion on damping capacity of MCM1805 alloy. The results showed that extrusion dramatically decreases the grain size but has little influence on phase composition and solute atoms concentration of MCM1805 alloy, and the grain refinement was the dominant reason for the obvious increase of tensile properties and decrease of internal friction of MCM1805 alloy.

Abstract: The effect of second phase on the mechanical properties of AZ61 and AZ91 Mg-Al-Zn magnesium alloy processed by equal-channel angular extrusion (ECAE) has been investigated. The results revealed that cracks initiated at and propagated through the α-Mg/β-Mg17Al12 interfaces and grain boundaries of Mg-Al-Zn alloys during tensile deformation. For AZ61, the elongation increased with the increase of ECAE pass number and the decrease of grain size. However, the elongation of AZ91 with more second phase particles decreased with the increase of ECAE pass number and the decrease of grain size.

Abstract: Tensile tests were performed on T4-treated specimens of GN62K (Mg-6Gd-2Nd-Zr(wt%)) and GN112K (Mg-11Gd-2Nd-Zr) alloys at room temperature and on T6-treated ones from room temperature to 300°C. The fracture behavior was investigated by using SEM images of fracture surfaces together with optical metallographs adjacent to the surface. Quasi-cleavage fracture was observed in the fracture surfaces of both alloys in T4-treated condition, and it seems that RE content has no significant effect on the fracture mechanism in T4-treated alloys. As for T6 treated condition, cracking was in a manner of transgranular cleavage and/or quasi-cleavage fracture in GN62K alloy but intergranular fracture in GN112K alloy, which implies that the fracture mechanism in T6-treated Mg-Gd-Nd-Zr alloys can be altered by the amount of RE addition. This phenomenon is interpreted in association with the relative strength of grain bulk and boundary.

Abstract: Mg-10wt%Gd-3wt%Y alloy was cast in a step-like mould, which provided five different cooling rates. The dentrite morphology and hardness of the as-cast alloy from the surface to the center was investigated and the influence of the cooling rates on these was analyzed. It was indicated that there were two different trends for the hardness distribution: in the section of the step castings with the two slowest cooling rates, the hardness decreased with the increase of depth; while in the other three step castings the hardness increased with the increase of depth. Also it was founded that the hardness could be influenced by the grain boundary, dentrite morphology and dentrite arm spacing (DAS) in the alloy. At last, according to the standard deviation curves of the hardness, the chilled depths were about 5mm in 1st step and 10mm in 2nd step. And the other steps were fully chilled.

Abstract: Tensile and compressive creep properties of Mg-5wt.%Al-1wt.%Sr alloy produced by gravity casting were investigated in this paper. Creep tests were carried out in the temperature range from 125 °C to 200 °C and stress range from 35 to 85MPa. The second creep rate in tension is significant different from that in compression, indicating that coarse-grained Mg-Al-Sr alloy exhibits tension/compression asymmetric behavior. Moreover, the activation energies and stress exponent in tension and compression are not the same, which suggest that creep mechanisms in tension and compression are different.

Abstract: Microstructure and mechanical properties of Mg-Zn-Er-Zr alloys were characterized in detail. The grain size of as-cast Mg-Zn-Er-Zr alloy was greatly decreased by the Mg-Zn-Er phases formed at grain boundaries. The addition of Er can increase the yield strength (YS) but decrease the ultimate tensile strength (UTS) and elongation of as-cast Mg-Zn-Zr alloy. The thermally stable Mg-Zn-Er phases were just partially dissolved into the matrix during solution treatment. And the addition of Er can prolong the precipitation process of Mg-Zn-Zr alloy. Solution-plus-ageing treatment can increase the strength of both the Mg-Zn-Zr and Mg-Zn-Er-Zr alloys, but the strengthening effect of Mg-Zn-Er-Zr alloy was greatly weakened, for the incompletely solution of Mg-Zn-Er phases. Er can greatly enhance the high temperature elongation of Mg-Zn-Zr alloy, but the increase of high temperature tensile strength was just a little.