Authors: Jing Yang Chen, Qing Li, Ming Jun Zhang, Xin Tang, Cheng Bo Xiao
Abstract: The influence of W and Al on the solidus and liquidus temperatures, microstructure and stress-rupture property at 980 °C/250 MPa was investigated in three Re-free experimental Ni-based single crystal superalloys. The results indicated that the solidus temperature increased for 14.0 °C and 9.8 °C by adding 0.84 wt.% W only and adding 0.45 wt.% Al and 0.44 wt.% W to the base alloy, respectively. The γ′ morphology changed from nearly cuboidal in the base alloy to cuboidal by adding 0.45 wt.% Al and 0.44 wt.% W. The volume fraction of γ′ precipitates increased, while the γ channel width decreased after adding Al and W. The additions of Al and W improved the stress-rupture life at 980 °C/250 MPa because of higher γ′ volume fraction, narrower γ matrix channel and more complete rafting structure.
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Authors: Wen Bo Luo, Xin Tang, Rong Guo Zhao, Jiang Hua Tan, Yoshihiro Tomita
Abstract: In this work, the physical aging and its effect on nonlinear creep behavior of poly(methyl
methacrylate) are presented. After annealing above Tg to release the previous thermal and stress
history, the samples were quenched to 60oC, aged for various times, and were then tested at three
different stress levels (22MPa, 26MPa and 30MPa) at room temperature of 27oC. At each stress level,
the creep strain was converted to compliance and measured as a function of test time and aging time.
The test results show that higher stress accelerates creep rate of the material while physical aging
plays a reverse role. The time-aging time superposition is applicable to build a master creep
compliance curve at each stress level, and it is demonstrated that the shift rate deceases with
increasing stress. Moreover, based on the time-stress superposition principle, a unified master curve
was constructed by further shifting the sub-master curves at 30MPa and 26 MPa to a reference stress
level of 22MPa.
2041
Authors: Rong Guo Zhao, Wen Bo Luo, Chu Hong Wang, Xin Tang
Abstract: Temperature induced change, and stress induced change as well, in intrinsic timescale
were investigated by nonlinear creep tests on poly(methyl methacrylate). With four different
experimental temperatures, from 14 to 26 degrees centigrade, time-dependent axial elongations of
the specimen were measured at seven different stress levels, from 14 MPa to 30 MPa, and modeled
according to the concept of time-temperature-stress equivalence. The test duration was only 4000
seconds. The corresponding temperature shift factors, stress shift factors and temperature-stress
shift factors were obtained according to the time-temperature superposition principle (TTSP), the
time-stress superposition principle (TSSP) and the time-temperature-stress superposition principle
(TTSSP). The master creep compliance curve up to about two-year at a reference temperature 14
degrees centigrade and a reference stress 14 MPa was constructed by shifting the creep curves
horizontally along the logarithmic time axis using shift factors. It is shown that TTSSP provides an
effective accelerated test technique in the laboratory, the results obtained from a short-term creep
test of PMMA specimen at high temperature and stress level can be used to construct the master
creep compliance curve for prediction of the long-term mechanical properties at relatively lower
temperature and stress level.
1386
Authors: Rong Guo Zhao, Wen Bo Luo, Chu Hong Wang, Xin Tang
Abstract: The mechanical behaviors were investigated by nonlinear creep tests of poly(methyl
methacrylate) under different temperatures. The test duration was 4000 seconds. The corresponding
temperature shift factors, stress shift factors and temperature-stress shift factors were obtained
according to time-temperature superposition principle, the time-stress superposition principle and
the time-temperature-stress superposition principle (TTSSP). The master creep compliance curve up
to about 1-month at a reference temperature 22 degrees centigrade and a reference stress 14 MPa
was constructed, and the effect of stress-induced damage evolution on the long-term creep behavior
of polymeric material was accounted. It was shown that TTSSP provides an effective accelerated
test technique in the laboratory, the results obtained from a short-term creep test of poly(methyl
methacrylate) specimen at high temperature and stress level can be used to construct the master
creep compliance curve for prediction of the long-term mechanical properties at relatively lower
temperature and stress level, and the master creep compliance curve with damage considered can be
applied to accurately characterize the long-term creep behavior of nonlinear viscoelastic polymer.
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