Papers by Author: Yong Hwan Kim

Abstract: This study investigated the microstructure and mechanical properties of the wide-gap region brazed with various powder mixing ratios of additive powder (IN738) to filler metal powder (DF4B). The wide-gap brazing process was carried out in a vacuum of 2×10-5 torr at 1230°C for 1 hr. The microstructure of the brazed region was analyzed by FESEM and AES. The wide-gap region brazed with 60wt.% IN738 additive powder and 40 wt.% DF 4B filler metal powder had a microstructure consisting of Ni solid solution + γ' and (Cr, W)2B. The fracture strength of the wide-gap region brazed with 60 wt.% IN738 additive and 40 wt.% DF 4B powder was as high as 832 MPa at room temperature. It was found that the (Cr, W)2B and pores in the brazed region are important microstructural factors affecting the mechanical properties of the wide-gap brazed region.

Abstract: The effects of adding Y2O3, and the precipitation of Ni3Nb by heat treatment, on the mechanical properties of mechanically alloyed Ni20Cr20Fe5Nb alloy were studied. The addition of Y2O3 caused an increase in the tensile strength at room temperature, 400°C and 600°C. The difference in the tensile strength between the Ni20Cr20Fe5Nb and Ni20Cr20Fe5Nb1Y2O3 alloys decreased gradually with increasing test temperature. The tensile strength of the Ni20Cr20Fe5Nb1Y2O3 alloy at relatively low temperature was increased by the addition of Y2O3, but decreased abruptly at temperature above 600°C. This seems to result from a change in the deformation mechanism due to the ultra-fine grain size, that is, grain boundary sliding is predominant at temperatures above 600°C while internal dislocation movement is predominant at temperatures below 600°C. Following the conventional heat treatment of the solution and subsequent aging, only a small amount of δ(Ni3Nb) phase was formed in the Ni20Cr20Fe5Nb alloy, whereas in a previous report it was indicated that a large amount of γ″(Ni3Nb) was formed in IN 718 alloy. The small amount of δ(Ni3Nb) phase formed in the present case is due to the exhaustion of the Nb content resulting from the formation of NbC during consolidation.

Abstract: The cyclic deformation in Cu and Cu-35Zn alloy were studied using ultrasonic nondestructive evaluation (NDE) technique to measure the ultrasonic velocity, attenuation coefficient and a nonlinear parameter. These materials were cyclically deformed under total strain amplitude control to investigate their ultrasonic reaction to different dislocation substructures, depending on the stacking fault energy difference. The microstructure evolution was observed using a transmission electron microscope, and the ultrasonic NDE parameter was measured after several cycles of fatigue deformation, in order to clarify the relationship between them. In both materials, the ultrasonic velocity was observed to decrease as the fatigue life fraction increased, which was attributed to the increasing dislocation density caused by the cyclic deformation. In the case of Cu, with its cell structure evolving during cyclic deformation, the rate of increase of the ultrasonic attenuation coefficient and the ultrasonic nonlinear parameter was higher than that observed in the case of the Cu-35Zn alloy with its planar array structure. This result implies that the dislocation cell structure is more sensitive to the ultrasonic parameter changes than the planar array structure formed during cyclic deformation.

Abstract: This study investigated the microstructure and mechanical properties of a wide-gap region brazed with various process variables. The IN738 and DF 4B alloy powders were used as additive and filler metal powder for the brazing process. The wide-gap brazing process was carried out in a vacuum of 2×10-5 torr. The wide-gap region brazed with 60wt.% IN738 additive powder had a microstructure consisting of IN738 additive and (Cr, W)2B. The fracture strength of the wide-gap region (60 wt.% additive and 40 wt.% filler metal powder) brazed at 1230°C for 30hr was as high as 862MPa (93% of base material strength). It was observed that the brazing temperature was the main process variable affecting the mechanical properties of the wide-gap brazed region. The creep rupture life of the region brazed with 60wt.% additive and 40 wt.% was longer than that of other brazed samples. The Cracks in the wide-gap brazed region initiated at the (Cr, W)2B and propagated through them. It was found that the (Cr, W)2B and the pore in the brazed region are important microstructural factors affecting the mechanical properties of the wide-gap brazed region.

Abstract: The effects of adding Al, Y2O3 and the use of H2O as a PCA (process control agent), on the mechanical properties of mechanically alloyed Ni20Cr20Fe5Nb alloy were studied. The addition of Y2O3 and Al caused an increase in the tensile strength at room temperature, 400°C and 600°C. However, it was confirmed that the increase of tensile strength at room temperature and 400°C was predominantly caused by addition of Y2O3, while that at 600°C was mainly due to addition of Al. These results can be attributed to the dispersion strengthening of Y2O3, preventing the formation of Cr2O3 and the change of fracture mode at 600°C by the addition of Al. Therefore, the Ni20Cr20Fe5Nb2Al alloy using H2O as a PCA showed superior tensile strength at room temperature, 400°C and 600°C. The increase in the tensile strength at room temperature and 400°C can be attributed to the strengthening of the solid solution induced by the increase in the amount of Nb solid solution, resulting from the prevention of NbC formation, while the increase in the tensile strength at 600°C can be attributed to the strengthening of the grain boundary afforded by the presence of Al1.54Cr0.46O3 formed by the addition of Al. After aging treatment for 10 hours at 600°C, g²(Ni3Nb) precipitates were formed in the Ni20Cr20Fe5Nb2Al alloy in which H2O used as the PCA, and the formation of these precipitates caused an increase in hardness.

Abstract: The microstructural changes and the relations between mechanical properties and additive powder with various brazing temperatures and times were investigated. The IN738 and BNi-3 alloy powders were used as an additive and filler metal powders for the brazing process. The wide-gap brazing process was carried out in a vacuum of 2×10-5 torr. The wide-gap region brazed with 60wt.% IN738 additive powder had a microstructure consisting of IN738 additive, and binary eutectic of Ni3B-Ni, and (Cr, W)B. As the brazing temperature and time were increased, the size of IN738 additive powder increased to 181µm, which decreased the amount of low strength Ni3B-Ni eutectic structure, thereby increasing the fracture strength of the wide-gap brazed region. Cracks in the brazed region were observed to propagate through the Ni3B-Ni structure, which lowered the fracture strength of the wide-gap brazed region.