Papers by Keyword: Bimodal

Abstract: In this paper, we focus on the stress-strain behavior prediction of the bimodal bulk Al5083 series which are comprised of ultra-fine grains (UFG) separated by coarse grain (CG) regions. The CGs in the UFG matrix effectively prevents microcracks from propagation, leading to enhance ductility and toughness while the strength remains high. In this work, initially, XFEM is implemented for bimodal materials considering various fracture criteria for brittle and ductile phases in maximum traction and cohesive law. Then the stress-strain behavior dependency of the model on the CG distribution in a constant volume fraction is investigated by extraction of RVEs from optical microscopy (OM) images of the real material. The solution convergence of such a problem with irregular geometry, plasticity and crack initiation-propagation demanded extreme efforts that accomplished by refining and arranging meshes as well as adding damage stabilizations. As a result of the above procedures, the sensitivity of the modeling procedure to various RVEs is obtained, the crack initiation-propagation pattern in microscale is predicted and consequently, the global stress-strain behavior result is calculated. It is shown that the predicted results are in good agreement with the available experimental results.

Abstract: This paper presents the preparation of bimodal crystalline macro-/mesoporous titania powders by using a pluronic polymer (EO20PO70EO20, P123) as a template through a hydrothermal treatment. The as-prepared powders were characterized by X-ray diffraction (XRD), nitrogen adsorption-desorption, scanning electron microscope (SEM) and transmission electron microscope (TEM). The results reveal that the amount of P123 has a significant effect on the surface area of the mesoporous titania. When the mass ratio of P123:TBOT is 1:14, the crystalline macro-/mesoporous titania has the largest surface area (120.96 m2/g), the average pore diameter of this sample reaches a minimum of 6.67 nm.

Abstract: Crack growth in AA6060 after two and eight equal-channel angular extrusions (ECAE), showing a bimodal microstructure and a homogenous ultrafine-grained microstructure, respectively, are compared to the coarse grained counterpart. Furthermore, an optimized condition, obtained by combining one ECA-extrusion and a subsequent short aging treatment is included. Fatigue crack growth behaviour in the near-threshold regime and the region of stable crack growth is investigated and related to microstructural features such as grain size, grain size distribution, grain boundary characteristics and ductility. Micrographs of crack propagation surfaces reveal information on crack propagation features such as crack path deflection and give an insight to the underlying microstructure. Instrumented Charpy impact tests are performed to investigate crack initiation and propagation under impact conditions. Due to the recovery of ductility during the post-ECAE heat treatment, the optimized condition shows improved fatigue crack properties and higher energy consumption in Charpy impact tests, when compared to the as-processed conditions without heat treatment.

Abstract: In this study, the production of β-Si6-zAlzOzN8-z (z =3) powders by the carbothermal reduction and nitridation of kaolin (Al2O3.2SiO2.2H2O) of Turkish origin (Can-Canakkale) was carried out with different processing parameters. It was found that the morphology of the produced SiAlON powder was mixture of irregular and whisker like grains. Therefore this morphology is suitable for liquid metal infiltration since the powders are already high porous. The kaolin powder containing stoichiometric rate carbon black and 30 % charcoal were pressed and reacted under nitrogen flow (2 lt/min) between 1400-1475°C for 4 h. After a carbothermal reduction and nitridation (CRN) process, porous β- SiAlON ceramic was produced from natural kaolin. Residual carbon and charcoal in the produced ß-SiAlON ceramic were fired at 1000°C giving extra porosity. The porous ß-SiAlON ceramics were sintered under N2 atmosphere at 1550°C for 2 h to make preform for infiltration process. SEM image analyses were carried out to determine preform and pore morphology and XRD analysis were performed for phase transformation.

Abstract: A bimodal porous hydroxyapatite (HAp) body with high flexural strength was prepared through slip casting. HAp fine powder used in this study was synthesized by wet milling, drying and heating of a mixture of calcium hydrogen phosphate di-hydrate and calcium carbonate. The synthesized HAp powder was 0.32
0.05 μm in size and 38.1
0.8m2/g in specific surface area. The slip was prepared by adding deflocculant and foaming reagent. The optimum value for the minimum viscosity in the present HAp slip with respect to its solid loading and the optimum amount of the deflocculant were studied. The total porosity of the specimens obtained from a slip of 48 wt% HAp solid loading is in the range of 49 – 61vol %, and the resultant porous HAp sintered body had large spherical pores of 300 -m with interconnecting rectangular voids. Many small pores in the size range of 2-3 -m or below were observed in the specimen obtained by heating at 1100, and 1200 . The flexural strength of the bimodal porous HAp ceramics sintered at 1200 C showed a large value of 17.6 MPa, with a porosity of 60.5vol.

Abstract: A numerical study on the effects of the distribution of rubber particles size on the fracture toughness of rubber-modified polymer alloys was computed. FEM analyses were conducted on the deformation field near the crack tip under mode I for small scale yielding condition. Near the crack tip is modelled as composite of matrix materials and rubber particles. On the other hand, outer region is modelled as homogeneous material whose constitutive equation has been obtained by analysing unit cell model of matrix and rubber particle. Perfect bonding or partial debonding of the interface is assumed in the computation. Matrix and rubber particles are treated as Mises and Mooney-Rivlin materials, respectively. It is shown that energy flux into fracture process zone; Ĵ -integral is smaller for bimodal type than monomodal one. This behavior largely occurred on the partial debonding case. These results imply that the screening effects occurred in the bimodal type larger than monomodal one.