Papers by Keyword: Boride Coatings

Abstract: In this work, the mechanical behavior on AISI 4140 with boride coating and hardened quenching-tempering was studies subsequently to boriding. The boriding is conducted at temperatures 1203 and 1233 K for 7 h, after that all samples at a temperature of 1143 K for 1 h and tempering 473 K were exposed for 1 h 30 minutes. The microstructural characterization was examined by scanning electron microscopy with saw-tooth morphology of boride coatings type Fe₂B. Three-point bend test was used to study the effect of hydrogen cathodic charging on the mechanical behavior of AISI 4140 with boride coatings, the results show a reduction of ductility and 58.17% of indices of embrittlement () and show a crack on the substrate due to interaction of hydrogen atom. Also, sample boride at 1203 K with hydrogen show a low decrease of the bending stress with respectively a sample boride without hydrogen and a decrease of the parameter () with 35.32% due to the formation of boride coatings.

Abstract: The wear resistant composite coatings on the basis of titanium borides, which are synthesized from thermoreactive powder components of a boron-containing mixture at electron beam surfacing, are interesting for applications today.

Abstract: The paper studies how microalloying with amorphous boron (B_am) and zirconia (ZrO₂) influences the structure and properties of boride coatings. Two factors are found to strongly affect the structure and phase formation in composite coatings produced by electron beam surfacing, especially when using thermoreactive powders: (i) high reactive diffusion between the composite and substrate components, which causes the coating structure degradation, and (ii) slight deviations from phase concentrations and equilibrium crystallization, which give rise to such nonequilibrium phases in the coating structure under the electron beam as ferroboron, ferrotitanium and binary eutectics.

Abstract: In many applications, even high-performance alloys have to be covered with protective coatings, providing higher corrosion and oxidation resistance, as compared to the alloy itself. This study investigates the feasibility to apply boron coatings on P91 steel by pack cementation process, to increase the steel durability in oxidative and corrosive environments, as well as its mechanical strength. Micro-indentation and the coating impact test were used to characterize the hardness and fatigue properties of the film respectively. The coating corrosion resistance versus the one of the uncoated P91 steel was tested in a salt spray chamber. The coating performance was characterized by optical and scanning electron microscopy to check the consistency of the coated and uncoated surfaces and the oxidation extend. The results show an increased film strength, good fatigue performance and adequate corrosion resistance.

Abstract: In this study, the evaluation of interfaces on iron boride Fe2B growth obtained by paste boriding process was carried out. Fractal geometry is used like a powerful tool for the roughness analysis present during iron boride growth. Experiments were performed in AISI 1045 steel at temperatures of 1193K for exposure times of 2, 4 and 6 h, and 1223K for treatment times of 2, 4, 5 and 6 h, varying the boron paste thicknesses in the range of 1 – 5 mm for each temperature and time. The fronts of the interfaces in iron boride coatings were characterized and digitized with mean of an optic microscope and Scion Image software. Self-affine methods were applied to the interface growths for validate the fractality of the system. It was established that the interface width, ω , scales to ω (L) ∼ L H , where H represents the roughness exponent of the boride layers.