Authors: Rajendra Doiphode, S.V.S. Narayana Murty, Nityanand Prabhu, Bhagwati Prasad Kashyap
Abstract: – Mg-3Al-1Zn (AZ31) alloy was caliber rolled isothermally at the temperature of 300 °C to develop fine grains of 3.6 μm. Annealing was carried out at various times and temperatures. Along with microstructure, annealing affects the hardness and hardness penetration depth. The hardness penetration depth of caliber rolled bar during annealing at 300 to 450 °C was investigated for 5 to 60 minutes. The change in hardness penetration depth were analysed and the mechanisms involved were discussed.
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Authors: Rajendra Doiphode, S.V.S. Narayana Murty, Nityanand Prabhu, Bhagwati Prasad Kashyap
Abstract: Mg-3Al-1Zn (AZ31) alloy was caliber rolled at 250, 300, 350, 400 and 450 °C. The effects of caliber rolling temperature on the microstructure and tensile properties were investigated. The room temperature tensile tests were carried out to failure at a strain rate of 1 x 10 -4 s-1. The nature of stress-strain curves obtained was found to vary with the temperature employed in caliber rolling. The yield strength and tensile strength followed a sinusoidal behaviour with increasing caliber rolling temperature but no such trend was noted in ductility. These variations in tensile properties were explained by the varying grain sizes obtained as a function of caliber rolling temperature.
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Authors: Rajendra Doiphode, Rahul Ramesh Kulkarni, S.V.S. Narayana Murty, Nityanand Prabhu, Bhagwati Prasad Kashyap
Abstract: Fine grains were developed in Mg-3Al-1Zn (AZ31) alloy by isothermal caliber rolling at five different temperatures in the range of 250-450°C. The samples of different grain sizes were deformed by constant strain rate and differential strain rate test techniques over the temperature range of 220-450 °C and strain rate range of 10-5 to 10-1 s-1. The effects of grain size, test temperature and strain rate on flow stSuperscSuperscript textript textress were analysed to develop the constitutive relationship for supSuperscript texterplastic deformation. The parameters of the constitutive relationship obtained from the constant strain rate tests and differential strain rate tests were used to find out the material constant A of the constitutive relationship.
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Authors: Niraj Nayan, S.V.S. Narayana Murty, S.C. Sharma, K. Sreekumar, Parameshwar Prasad Sinha
Abstract: A novel technique of pure Lithium addition has been adopted for the processing of Al-Cu-Li alloy AA2195 cast ingots (7-8 kg each) in VIM under dynamic inert atmosphere, which gives more than 95% recovery of Lithium. The cast billets were homogenized, forged and converted into 12mm diameter rods by caliber rolling in the temperature range of 250°C, 300°C, 350°C and 400°C. The caliber rolled rods were treated to T8 (Solution Treatment+WQ+CW+Aging) condition. Mechanical properties were evaluated for T8 tempered bars at room temperature and correlated with microstructural observations. Highest mechanical properties in T87 temper have been obtained for rods caliber rolled at 350°C temperature.
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Authors: S.V.S. Narayana Murty, Shiro Torizuka
Abstract: Steel bars having a cross section of 18mm square with uniform distribution of ultrafine ferrite grains were produced through a multi-pass warm caliber rolling process in a 0.15%C-0.3%Si-1.5%Mn steel. The average ferrite grain sizes of 0.43μ m, 0.70μ m and 1.2 μ m were obtained in the isothermal warm caliber rolling processes at 773K, 823K and 873K respectively. Even though caliber rolling results in inhomogeneous strain distribution, multi-pass caliber rolling to large cumulated strains of 2 or 3 can be uniformly introduced in to the bar samples. Strain accumulation due to the multi-pass warm deformations was confirmed by comparing microstructural evolution through the multi-pass deformations with that of single pass deformation. The size of ultrafine grains formed through warm deformation was found to depend on the Zener-Hollomon parameter. The similarity of the microstructural evolution with single pass deformation reveals that the multi-pass warm deformation is an effective method to obtain ultrafine grained ferrite structure in bulk materials. It is proposed that compressive strain-Z parameter plots along with grain size-Z parameter plots help in establishing the processing conditions for obtaining products with a desired microstructure and grain size. Finally, such “processing maps” developed for a variety of materials serve useful purpose in bridging the science and technology of developing bulk ultrafine grained materials in semi-finished / finished products.
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Authors: Shiro Torizuka, Akio Ohmori, S.V.S. Narayana Murty, Kotobu Nagai
Abstract: Ultrafine-grained structures formed dynamically through simple compression at warm deformation temperatures were investigated in a 0.15%C- 0.4%Si-1.5%Mn steel. The effects of strain, strain rate and deformation temperature on the microstructural evolution were examined using an isothermal plane strain compression technique with a pair of anvils. The maximum strain was 4, the deformation temperature was below the AC1 temperature, and the Zener-Hollomon parameter (Z) ranged between 1012 s-1 and 1016 s-1. Ultrafine ferrite grains surrounded by high angle boundaries are generated by simple compression when the strain exceeded a critical value. The number of newly generated ultrafine grains increased with the strain; however, the average sizes were found to be independent of strain. The grain size, `d`, was found to depend on Z parameter. An equation, d (μm) =102.07Z-0.16, was found to satisfy the experimentally obtained data. This study demonstrates the possibility of obtaining ultrafine ferrite through multi-pass caliber rolling as a high Z- large strain deformation technique for producing bulk engineering components. It was also noted that the empirical relation established based on single pass compression tests is valid for multi-pass caliber rolling.
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Authors: Yohei Tanno, Takaki Mukai, Motoo Asakawa, Masaru Kobayashi
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Authors: Toshio Fujii, Nobuyuki Fuyama, Chitoshi Masuda
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