Papers by Keyword: Crystallographic Texture

Abstract: The ferritic stainless steel type 430 stabilized with Nb, with and without annealing after hot rolling, was cold rolled and subjected to isothermal annealing at temperatures 650, 700 and 750°C for times ranging between 10 to 86400 s. The recrystallization kinetics was evaluated by JMAK model through microhardness measurements and KAM and GOS parameters. The Avrami exponent data indicate the occurrence of an unidimensional grain growth due only to high angle boundaries migration, with values ranging between 0.9 and 1.2. The nucleation rate and grain growth decreased continuously with time. The evolution of the texture was analyzed via EBSD analysis by ODF maps. The steel recrystallization is based on combination of ON and SG theories, due to presence of {111}<121>, {554}<225> and {111}<112> related to γ fiber. The rotated cube component, feature of the hot rolled steel, decreased with annealing time.

Abstract: Texture and substructure changes in cladding tubes from Zr-based alloys under neutron irradiation in the atomic reactor during 6 years were investigated by use of X-ray methods. For this aim in the “hot” laboratory the automated X-ray diffractometer was set and the technique to handle with irradiated samples was elaborated. The residual radiation activity of samples correlates with integral texture Kearns parameters of tube, so that the texture weakens as the doze of neutron irradiation grows. Because of the initial substructure inhomogeneity of cladding tubes its changes under neutron irradiation are also inhomogeneous: relatively perfect grains of texture maxima become more distorted, whereas initially distorted grains of texture minima becomes more perfect.

Abstract: By using Eulerian adaptive modeling approach, both the round extrusion and sheet extrusion of magnesium alloy AZ31 were simulated. Furthermore, the history strains of material point flowing through the Eulerian domain was extracted and used as the foundation for defining the boundary conditions in the crystal plasticity finite element (CPFE) modeling for the extrusion texture. By virtue of this modeling method, the realistic grain boundaries can be approximated by using a 3D polycrystal generator and the intra-granular interactions can be well described. Both of the simulated round extrusion and sheet extrusion textures of alloy AZ31 show reasonable agreement with experimental results.

Abstract: Aluminium is a potential light weight alternative to steel for deep drawn sheet components, but generally does not compare well to steels in terms of formability. Research in polycrystalline plasticity indicates applying shear to rolled fcc alloys improves their deep drawability by favourably modifying their crystallographic texture. Such processing could be realised industrially by cold asymmetric rolling (ASR), but in order to gain detailed understanding of the influence of process parameters on the evolution and through thickness homogeneity of the texture a validated full field multi-scale model of the process is required. This study examines the ability of a hierarchical multi-scale approach to predict evolved textures for aluminium sheet subjected to a mechanical test exhibiting a deformation mode relevant for ASR, namely simple shear. The homogeneity of the deformation field is assessed with full field strain measurement by digital image correlation, and macrotexture is measured by x-ray diffraction. The discrepancies are discussed and further work to validate the modelling approach for simulation of texture evolution in the ASR process is briefly outlined.

Abstract: Rotation of grain crystal lattice is the basic mechanism of texture formation and of anisotropic behavior of metals during plastic deformation. The classical definition of crystal lattice rotation leads in some cases to different texture and residual stress predictions than the definition based on the orientation preservation of selected sample planes and/or directions. Also the intensity of grain-matrix interaction plays an important role in the prediction of the above quantities. These problems were studied using elasto-plastic deformation model of polycrystalline materials. Examples of austenite and ferrite steels were considered.

Abstract: Textures of rolled sheets are typically orthotropic along the mid-thickness plane, where the material undergoes plane strain compression. At the surface and in the subsurface layers, however, the achievement of the orthotropic symmetry can be impeded due to friction between the sheet and the rolls. The through-thickness strain distribution and texture have been found to also depend on the rolling draught [1], the load exerted on the rolls, the temperature and the rolling speed. Valid predictions of the influence of the shear deformation on the development of the microstructure and texture are not only important for controlling structural characteristics of the as-deformed material, but are also a pre-requisite to the investigation of the recrystallization process upon annealing. A recent experimental study of the texture development in heavily rolled aluminum revealed that the texture in each subsurface layer was dominated by one of the symmetric variants of the “copper” component. To investigate the conditions under which such variant selection is expected, a crystal plasticity theory combined with several mean-field as well as full-field scale-transition schemes is applied in the present work. Model predictions are compared to the texture development measured by EBSD in samples rolled to high and ultrahigh strains.

Abstract: The present work examines the microstructure and texture evolution in a Ni-30wt.%Fe austenitic model alloy deformed in torsion at 1000 °C, with a particular emphasis on the orientation dependence of the substructure characteristics within the deformed original grains. Texture of these grains was principally consistent with that expected for simple shear and comprised the main A, B and C components. The deformation substructure within the main texture component grains was characterised by “organised” arrays of parallel microbands with systematically alternating misorientations, locally accompanied by micro-shear bands within the C grains. With increasing strain, the mean subgrain size gradually decreased and the mean misorientation angle concurrently increased towards the saturation. The stored deformation energy within the main texture component grains was principally consistent with the respective Taylor factor values. The microband boundaries corresponded to the expected single slip {111} plane for the A oriented grains while these boundaries for the C oriented grains represented a variety of planes even for a single grain.

Abstract: A grain whose orientation and size were specified was embedded in a matrix grain structure. The matrix contained texture components in certain special orientations and those in general orientations, and the embedded grain had a certain special three-orientations-relation with grains in the former components. The dependence of growing behavior of an embedded grain on its number of faces of a grain has been examined by a modified Potts MC type 3D simulation and found to depend on the triple line dragging, suggesting that three-orientations-relation dependent triple line dragging can change the crystallographic texture through grain coarsening.

Abstract: The present work provides a summary of the recent findings obtained from the experimental investigation of the grain structure, crystallographic texture and dislocation substructure evolution in an austenitic Ni-30%Fe model alloy during dynamic recrystallization (DRX) and post-dynamic annealing. It has been found that the DRX texture characteristics become increasingly dominated by the low Taylor factor grains during DRX development, which presumably results from the preferred nucleation and lower consumption rates of these grains. The substructure of DRX grains is random in character and displays complex, hierarchical subgrain/cell arrangements characterized by accumulation of misorientations across significant distances. The stored energy within DRX grains appears to be principally consistent with the corresponding Taylor factor values. The changes observed within the fully dynamically recrystallized microstructure during post-dynamic annealing have provided a basis to suggest a novel mechanism of metadynamic softening for the current experimental conditions. It is proposed that the initial softening stage involves rapid growth of the dynamically formed nuclei and migration of the mobile boundaries. The sub-boundaries within DRX grains progressively disintegrate through dislocation climb and dislocation annihilation, which ultimately leads to the formation of dislocation-free grains, and the grain boundary migration gradually becomes slower. As a result, the DRX texture largely remains preserved throughout the annealing process.

Abstract: The substructure and crystallographic texture characteristics of both the deformed matrix and dynamically recrystallized (DRX) grains were investigated in a Ni-30%Fe austenitic model alloy subjected to hot torsion. Deformation was performed at a temperature of 1000°C using strain rates of 1, 0.1 and 0.01 s^-1, which produced a range of DRX grain sizes. Electron back-scattered diffraction and transmission electron microscopy were employed in the investigation. Both the deformed matrix and DRX grains revealed the texture components expected for simple shear deformation by crystallographic slip. The texture of DRX grains was dominated by low Taylor factor components as a result of their lower consumption rate during growth of these grains. There was a marked difference in the substructure characteristics between the deformed matrix and DRX grains regardless of the grain size and orientation. The deformed matrix substructure was largely characterized by organized, banded subgrain arrangements with alternating misorientations. By contrast, the substructure of DRX grains was generally more random in character and displayed complex, more equiaxed subgrain/cell arrangements characterized by local accumulation of misorientations. Based on the experimental observations, a mechanism of the distinct substructure development within DRX grains has been proposed.