Papers by Keyword: Cyclic Heat Treatment

Abstract: The subject of the article is focused on the refining of the cast structure of gamma TiAl–2Nb alloy using cyclic heat treatment and on the analysis of the grain refining mechanism. Microstructure evolution after applied cycles of heat treatment was characterized using light, laser and electron microscopy and using microhardness tests. Application of five heat treatment cycles during which two phase transformations (eutectoid and alfa-recrystallization reactions) repeatedly took place resulted αin refining of the cast columnar structure. The mean grain-lamellar colony size 0.512 mm was transformed to fully lamellar structure containing gamma and alfa2 phases having the mean grain size 0.229 mm. Lamellae thickness of gamma was not changed while the thickness of alfa2 phase decreased to 78 nm. Refining of alfa2 phase resulted in the increase of the microhardness by 20 %. The recrystallized cast structure obtained by cyclic heat treatment and the knowledge on the mechanisms of the refining the structure were compared and discussed with the literature data.

Abstract: In this paper, the possibility of refining grain of Ti-48Al-2Cr-2Nb alloy in the processes of multi-stage heat treatment consisted of initial heat treatment, cyclic heat treatment and under-annealing was evaluated. Microstructural changes that take place during the particular heat treatment procedures were also described. It was demonstrated that due to the application of combined cyclic heat treatment and under-annealing almost 24-fold grain refinement in relation to the state after homogenising could be obtained. Probable mechanisms of grain refinement in the proposed heat treatment processes were also presented and influence of individual procedures of the proposed treatment on selected properties of the investigated alloy was described

Abstract: This paper focuses on the variations of static and dynamic properties of tungsten heavy alloy with heat treatment. The matrix phase of 93W-4.9Ni-2.1Fe (weight percent) has been penetrated into W/W grain boundaries during a cyclic heat treatment which consists of repeated isothermal holdings at 1150 °C and water quenching between them. By applying the cyclic heat treatment, the impact energy of tungsten heavy alloy is increased about three times from 57 to 170 J. When the tungsten heavy alloy is cyclically heat treated at 1150 °C and then re-sintered at 1485 °C, W/matrix interface is changed from round to undulated shape. The irregularity of the interface is increased with increasing the number of heat treatment cycles. From the measurement of the residual stress of W grains by X-ray diffraction, it is found that the irregularity of the interface is closely related with strain energy stemmed from the difference of thermal expansion coefficient between W particles and matrix phase. From dynamic ballistic test, it is found that the tungsten heavy alloy with undulated W grains forms many narrow fracture bands which are preferential for the self sharpening effect, thus, for the improvement of the penetration performance.