Papers by Keyword: Dilatometer

Abstract: The quench and partition process is a means to develop third-generation high-strength steels using many possible process variants. In this work, two variants of quench and partitioning heat treatments, one-step and two-step, were carried out for high Si and high Al steel alloys. The kinetics of isothermal transformation occurring during the one-step quench and partition process were analysed using dilatometry. Experimental analysis revealed the swing-back phenomenon in high Si steel, and the transformation characteristics above and below the M_s temperature differed. The high Al alloy resulted in higher retained austenite (19%) compared to high Si steel (17%) during the one-step quench and partition process. Aluminium addition favoured bainite formation more than silicon addition. A comparison of two heat treatment variants shows the two-step quench and partition heat treatment seemed preferable as it produced more retained austenite (22%) in the high Si steel.

Abstract: The dilatometer study of the austenite transformations in steels with different chemical composition was conducted. The studied steels were classified as the air hardened steels of different alloying systems (Cr-Ni-Mo, Cr-Mn-Si-Mo and Cr-Mo-V) designed for the mining applications (rock drilling equipment, drilling instrument). The microstructure of the steels was investigated after continuous cooling at the rates of 0.1...30 °C/s from the austenitization temperature down to the ambient temperature. The CCT diagrams of the studied steels were plotted showing that the alloying with different set of elements can provide the desired hardenability and microstructure.

Abstract: State of the art of in-situ analysis on grain structure of metals during thermal and stress treatment is done by observation of the probe in a thermomechanical treatment system. Potential analysis methods are high energy x-ray scattering (e.g. in a synchrotron) or laser-ultrasonics (LUS). The most commonly used thermomechanical system, is the so called “Gleeble” from Dynamic Systems Inc., which is able to heat and load the material in a quite fast manner with extremely high heating rates, very high forces and fast force changes. There is a wide area of research and applications, though, where these capabilities are not fully required, a less complex deformation-and quenching dilatometer would often be sufficient. In this paper we will show the implementation of a LUS system in such a dilatometer and compare it to the “all inclusive” Gleeble system, pointing out benefits and downsides on different aspects, like the technical specifications, the needed footprint and more. A sketch of the full system and the beam path will show the general idea on the implementation of the LUS system into the dilatometer. We will also present first results of a thermal treatment on a metal sample suited for grain structure and phase transition analysis.

Abstract: Zirconium alloys are solid solutions of zirconium or other metals. Zirconium has very low absorption cross-section of thermal neutrons. Zirconium has high corrosion resistance, ductility and hardness. Zirconium is mainly used as a good refractory metal. Zirconium can be manufactured by using standard fabrication techniques. In the present scenario zirconium alloys are used in water reactors for the cladding of fuel rods in nuclear reactors in nuclear technology. We use the composition of zirconium alloys as more than 94.5 weight percentage of zirconium and less than 2.45 weight percentage of copper which are added to improve mechanical, thermal properties and corrosion resistance. This paper first focuses on the study of thermal properties of Zirconium. And this particularly concentrated on variation of Coefficient of Thermal Expansion by varying temperatures by using Dilatometer and as well as ANSYS

Abstract: Austempered Ductile Iron (ADI) is characterized by high tensile strength with acceptable ductility. Steel, as a large competitor to ADI, also meets the tensile and yield strength. Nevertheless, the main advantages of ADI compared to steel are the lower density (7.2 g/cm3 to 7.85 7.87 g/cm3) for weight reduction and lower manufacturing costs because of less energy consumption during the production. One of the main problems of producing ADI is the quenching process during heat treatment of thick-walled castings. The inner part of a massive casting – in contrast to the outer part – cools down more slowly, resulting in a heterogeneous microstructure with parts of pearlite and ferrite embedded in austenite before reaching the isothermal transformation temperature. Molybdenum is, besides nickel, copper and manganese, one of the possible alloying elements that postpone the transition point of ferrite and/or pearlite. To investigate the influence of molybdenum in thick-walled castings experiments with different molybdenum contents were performed. In dependence on the molybdenum content, different austenisation and ausferritisation temperatures and times are examined in order to investigate the transformation points, fraction and morphology of different phases. The mechanism of molybdenum in ADI has been investigated by means of dilatometer tests, microstructure analysis and mechanical tests.

Abstract: An advanced high strength steel (0.08 %C, 1.79 %Mn, 0.23 %Si) was subjected to different post-weld heat treatments by quenching & tempering treatments (Q&T) after laser welding to reduce the risk of martensite formation in a few seconds based on an idea of quench and partitioning (Q&P), mechanism. The thermal stability of retained austenite, microstructure development and mechanical properties have been studied at 2 tempering temperatures of 440°C (Ms) and 636°C (Bs), both for 15 minutes, by means of electron microscopy, dilatometry, hardness profile and tensile tests. Dilatometer study unveiled that redistribution of carbon atoms and precipitation of transition carbides occur around 150°C and austenite decomposition occur at 600°C. Tempering at 636°C resulted in notable effect on the mechanical properties, while no significant difference was detected at 440°C, except a slight hardness drop. The strength increased up to 12% for the different specimens without significant loss in ductility for all specimens tempered at 636°C, which may be caused by precipitation hardening and recrystallization of martensite lath boundaries during tempering around 600°C.

Abstract: The effect of silicon (Si) on the stability of heat-resistant ductile iron having ferrite matrix in high temperature was investigated by dilatometric test. Microstructure of heat-resistant ferritic ductile iron consists of ferrite, eutectic carbide at eutectic cell boundaries, precipitated carbide in grain and graphite. Pearlite was found around eutectic carbide in some specimens, however, all pearlite was decomposed by the annealing treatment. As Si content was increased, the number and size of carbide decreased and full ferrite matrix were obtained. The starting temperature of ferrite-austenite transformation and the coefficient of thermal expansion increased with the increase of Si content. The growth of Si 6.0wt% specimen during held at 1,000 ^oC is lower than other specimens, and it is considered that in the case of Si 6.0wt% specimen, the carbon movement is restrained due to the low solubility of carbon in matrix. In the case of annealed specimens, the contraction during ferrite-austenite transformation was not found when heating. This is because the re-distribution of the graphite was happened through the movement of carbon during annealing treatment.

Abstract: The paper presents the results of the physical and numerical modelling of heat treatment of experimental steels for pipelines. Simulation has been conducted at the Institute of Metal Forming and Safety Engineering of Częstochowa University of Technology. The numerical modelling of heat treatment has been carried using commercial program TTSteel. Based on the results of computer simulation, changes in steel microstructure during continuous cooling have been analysed, and the characteristics of temperature and the diagram of Continuous Cooling Transformation (CCT) have been constructed. Numerical research has been verified running the physical simulation of heat treatment of steel using dilatometer DIL805 A/D. The characteristic temperature of steel and the size of the former austenite grains have been determined. Also, the metallographic examination of the samples was conducted and Vickers hardness was tested. The obtained results have been used for building a real CCT diagram of steel.

Abstract: It’s really necessary to determine freeze-thaw resistance of concrete faster and correctly.The offered method is based on measurement of long strength by nondestructive method, based onacoustic issue. Also dilatometer is used. During this research, the theoretical analysis of concrete'sspecimen dependence on freeze-thaw resistance and energy, which is emitted by a specimen duringdestruction, has been carried out. Freeze-thaw resistance of a specimen is calculated as themathematical relation of these energies. Correctness of the offered method is proved byexperiments. The offered method is characterized by small labor input, high efficiency and a wideapplication scope, but special laboratory equipment is needed.

Abstract: The paper introduces the measuring principle of glass thermal expansion coefficient. It expresses the features and advantages of the linear variable differential transformer measuring principle by comparing the thermal expansion coefficient measurement methods analysis. Meanwhile, the paper introduces DIL402PC dilatometer measuring devices and measurement procedures. It use standard samples to execute thermal expansion instrument system check from the accuracy and repeatability. The result shows thermal expansion coefficient of linear expansion instrument bias of DIL402PC dilatometer is within the error range of the theoretical value. The process proves it has a wide range of applications.