Papers by Keyword: Dislocation

Abstract: Yield strength of low carbon mild steel decreases when temper-rolling is applied to release yield point elongation. Generally mobile dislocation used to be considered as the cause of the YS lowering. However from Bailey-Hirsch theory, strength should be higher with temper-rolling because of the increase of dislocation density. To newly explain the lowering yield strength by temper-rolling, standing at the point that a few ppm carbon change Hall-Petch coefficient , decrease in yield strength by temper-rolling is investigated using an ultra-low carbon steel. Yield strength of steel with the small amount of solute carbon increased after 2% temper-rolling and didn’t change after aging. On the other hand, yield strength of steel with the high amount of solute carbon decreased after 2% temper-rolling and increased again after aging. Despite solute carbon content, the Hall-Petch σ0 increased by dislocation strengthening of temper-rolling. Hall-Petch coefficient ky of low solute carbon steel remained at the low level even after temper-rolling or aging , however, that of high solute carbon steels significantly decreased after temper-rolling and increased again after aging. Yield strength reduction of the high solute carbon steel can be attributed to the decrease of ky.

Abstract: A new class of superplastic titanium alloy, Ti–4.5Al–2.5Cr–1.2Fe–0.1C–0.3Cu–0.3Ni, was deformed at 1073 K with strain rates of 1×10⁻⁴–1×10⁻¹ s⁻¹, and microstructures in the condition between superplastic regions II and III (= 1×10⁻² s⁻¹) were observed using scanning electron microscope and electron back-scattered diffraction. Continuous dynamic recrystallization was observed, resulting in grain refinement both in α and β phases. The grain size decreased significantly in α phase at the early stage of the deformation and in β phase at the later stage. In the recrystallized microstructure, the major sub-boundaries formed perpendicularly to slip directions <11−20> in α phase and parallel to slip planes {110} in β phase, which might be caused by the difference in the symmetry of the crystal structures.

Abstract: The analysis of the strength characteristics and electrical conductivity of annealed Cu-1.0wt.%Cr-0.1wt%Zr alloy subjected to subsequent deformation under various conditions was carried out by analytical modeling methods. The contributions of the regions with nanotwins, as well as such defects of the crystal structure as vacancies, alloying atoms, dislocations, and particles of the secondary phase to the strength and electrical conductivity of the material were estimated.

Abstract: The present study shows that warmly forged and low-temperature annealed twinning induced plasticity (TWIP) steel exhibited very high dislocation density and apparent yield-point phenomenon in addition to very high yield strength. The initial density of dislocations significantly affected the evolution of dislocations during the subsequent tensile deformation. Original high dense dislocations prompted the rapid increase of dislocations, and intensified the complexity of dislocation configurations. All these effects made the twinning deformation weakened but the dislocation deformation enhanced, leading to increased strength but decreased plasticity.

Abstract: Several studies have been carried out regarding the influence of dislocations on device characteristics; however, most of them had been limited to pseudo-vertical structures using high pressure high temperature (HPHT) insulating material as the substrate. In this study, we have investigated the influence of dislocations to the devices using vertical structure SBD on p+ HPHT substrate. SBDs were selectively fabricated on specific dislocation areas. The SBD fabricated on the threading dislocation area indicated fatal influence of the dislocation on the device characteristics.

Abstract: Aluminum nitride (AlN) single crystal boules were grown by physical vapor transport (PVT). Diameter expansion during boule growth, without the introduction of low angle grain boundaries (LAGB) around the boule periphery, was confirmed by crossed polarizer imaging, synchrotron white beam x-ray topography (SWBXT), and synchrotron monochromatic beam x-ray topography (SMBXT). The densities of basal plane dislocations (BPD) and threading edge dislocations (TED) averaged from high-magnification topographs of five regions of a high-quality substrate were 0 cm^-2 and 992 cm^-2, respectively. Substrates fabricated from AlN boules possessed excellent surface finishes suitable for epitaxy.

Abstract: The dislocation behavior during bulk crystal growth on the 4H-SiC (000-1) C-face using the solution method was investigated. A 2 inch wafer with a 4° off angle was fabricated from a bulk crystal grown by the TSSG method, and the dislocations in the crystal were evaluated using synchrotron X-ray topography and TEM observation. From the topograph images, it was found that the TSD density remarkably decreased as the growth progressed. Furthermore, the TEM observation suggested that TSD decreases as the threading dislocations convert to in-plane defects toward the center of the crystal. Conventionally, it was considered that conversion of threading dislocations hardly occurs in solution growth on the C-face. However, it is thought that this phenomenon was not observable because the conversion efficiency is remarkably low. We speculate that dislocations may be transformed by suddenly making macrosteps during bulk growth.

Abstract: Nanoscratching and nanoindentation simulations are performed to study the processability of Cu/Ni bilayers with interfaces using molecular dynamics (MD) method. Single crystals Cu and Ni are served as comparisons. In the nanoscratching processes, the interfaces of Cu/Ni bilayers appear as a barrier of dislocations gliding, and lead to larger friction forces and normal forces. For single crystals and bilayers, both their friction forces and normal forces increase with the increasement of scratch velocity at 100-300 m/s. Friction coefficients under scratching processes are calculated, and they are smaller than macrosacle scratching process because of coating effects of nano-chips on the tool. The effects are analyzed by conducting both molecular dynamics simulations in nanoscale and finite element simulations (FES) in macroscale. In the indentation process, the processing properties of Cu-Ni and Ni-Cu bilayers are different from each other, and their indentation forces are both larger than their single crystals. Recovery deformation takes place during the relaxation stage. When the tool is unloading, some workpiece atoms adhere to the tool. The simulation results of the two nanoscale machining processes reveal the strengthening mechanism of interface, and show comprehensive processability of metal bilayers.

Abstract: Evolution laws of structure and performance of Cu-10Ni-1Fe-1Mn alloy in the process of continuous casting-planetary rolling-drawing deformation were studied by OM, SEM, TEM, Brinell Hardness tester and universal material testing machine. Results demonstrated that the alloy ingot is composed of thick dendrites. The ingot makes grain crushing and dynamic recrystallization after planetary rolling. The hot rolling samples still have abundant fine recrystallization textures after multi-pass drawings. Due to roller-core head or internal-external mold opposite pressure, dislocations in different regions of sample move along the glide plane, forming a macroscopic slip band. Two adjacent macroscopic slip zones which move toward opposite directions compose the folded structures after the deformation. Refined crystalline strengthening, solution strengthening of Fe, Ni and Mn, work hardening, and iron-containing particle precipitation are major causes of alloy strengthening. SEM analysis of tensile fracture demonstrated that the material still maintained good plasticity after rolling and drawing deformation. However, material plasticity declined with the increase of cold processing-induced deformation.

Abstract: The evolution of microstructure of ZL205A alloy during equal channel angular pressing (ECAP) by route A at room temperature was investigated by OM, SEM and XRD, and the hardness of cast and heat treatment alloy from different strain were tested. The results showed that the grain of cast alloy were obviously refined, the massive q phase along the grain boundary were crushed, and prompts the distribution of q streamline after one pass through ECAP. After two passes of ECAP, the distribution of q phase is more uniform. After heat treatment through ECAP, the grains were also obviously refined, and elongated in axial direction, which also prompts the distribution of q streamline. The hardness was significantly improved after ECAP. The hardness of cast alloy increases from 65HV to 132HV after two passes, and that of heat treatment alloy increases from 112HV to 198HV. With the increase of extrusion passes, the number of dimples gradually increased and evenly distributed, the depth of dimples was of a similar level, and the distribution of precipitated phase is more uniform.