Papers by Keyword: Dynamic Recrystallization (DRX)

Abstract: The microstructure evolution of hot deformed Cu-Zn-Se-Bi-Sn alloy was investigated by Hitachi-800 transmission electron microscopy (TEM). The result shows that there are three different dislocation configurations such as dislocation network, dislocation wall and dislocation cell in hot deformed Cu-Zn-Se-Bi-Sn alloy. The dislocation network was firstly formed in some certain grains of Cu-Zn-Se-Bi-Sn alloy when the deformation strain amounted to 2%. Then dislocations initially arranged regularly beside original grain boundaries and the arranged dislocation walls were formed in some area and sub-grains merging emerged when the deformation strain amounted to 20%. Eventually, obvious dynamic recrystallization nucleation by sub-grain merging emerged in Cu-Zn-Se-Bi-Sn alloy when the strain attached 80%.

Abstract: Oxyfluoride phases have been synthesized in free atmosphere, using the initially synthesized perovskite BaTiO3 and the fluorides NaF and MgF2. The purity of BaTiO3 and oxyfluorides has been checked by X–Ray diffraction (XRD).The microstructures of these phases are observed by scanning electron microscopy. The phase transitions have been investigated by dielectric measurements and differential scanning calorimetry (DSC).

Abstract: The hot deformation behavior of as-cast AZ31 magnesium alloys have been investigated at 200~400°C and strain rates 0.001~1s-1 by means of hot compression tests on a Gleeble-1500D thermal-mechanical simulator. We have analyzed the flow stress-strain curve and presented the constitutive equation by calculating stress exponent, activation energy and Zemer-Hollomon parameter. Then, the processing map of AZ31 alloys has been developed based on the dynamic material model theories and Prasad instability criterion. The flow instability domain is observed at lower temperature and the larger power dissipation rate is emerging at 300~400°C. We have analyzed the corresponding deformation microstructures and it is characteristic of dynamic recrystallization. These results have shown that AZ31 alloy has good workability at 300~400°C and lower strain rate.

Abstract: Hot-compression experiments of 316LN stainless steel have been conducted on a Gleeble-1500D thermal-mechanical simulator. We have analyzed the flow stress-strain curve and acquired the constitutive equation of 316LN steel by calculating stress exponent, activation energy and Zemer-Hollomon parameter. Then, based on the material model theories and Prasad instability criterion, the iso-efficiency map at strain 0.6 of 316LN steel has been developed. The larger power dissipation rate is emerging at 1050~1200°C and lower strain rate. In addition, we have also analyzed the hot deformation microstructure mechanism of 316LN steel is discontinuous dynamic recrystallization by the observation of deformation microstructure. These results have been of great significance to understand microstructure evolution and to determine the optimum hot-working conditions in the production.

Abstract: The dynamic recrystallization (DRX) behavior in the isothermal hot compression of AISI 52100 steel was analyzed by using the phenomenological-based cellular automaton (CA) algorithm. The developed CA model was coded into DEFORM platform, which is a Finite Element Method (FEM)-based software for simulation of material deformation process. The developed CA-model can thus predict the nucleation and growth kinetics of dynamically recrystallized grains of the testing material in hot working process. Furthermore, the effects of the deformation temperature, true strain and strain rate on the microstructural evolution of the testing material were physically studied by using Gleeble-1500 thermo-mechanical simulator and the developed CA-model was verified by the experimental results. Through simulation and experiment, it is found that the results predicted by the CA-model have a good agreement with the experimental ones.

Abstract: In order to improve the effects of rare earths (RE) as microalloy on the recrystallization behavior in the high strength micro-alloyed steel, the X80 pipeline steels with different RE content were produced with a vacuum induction furnace, a series of hot torsion tests were performed under a range of deformation conditions, and the stress-strain curves were analyzed. The results showed that trace RE would improve the austenite recrystallization behavior. The activation energy of deformation and static recrystallization of the austenite in the X80 pipeline steel without RE additions were respectively 393 and 366 kJ/mol. When the RE addition was 0.0025 wt.%, the activation energy of deformation and static recrystallization were reduced by 33 and 29 kJ/mol respectively. But when the RE addition was increased to 0.0220 wt.%, RE would significantly inhibit the dynamic recrystallization of the austenite, the activation energy of deformation would be increased by 35 kJ/mol, but the activation energy of static recrystallization would reduce by 15 kJ/mol.

Abstract: The high-manganese austenitic steels are an answer for new demands of automotive industry concerning the safety of passengers by the use of materials absorbing high values of energy during collisions. The chemical compositions of two high-manganese austenitic steels containing various Al and Si concentrations were developed. Additionally, the steels were microalloyed by Nb and Ti in order to control the grain growth under hot-working conditions. The influence of hot-working conditions on a recrystallization behaviour was investigated. Flow stresses during the multistage compression test were measured using the Gleeble 3800 thermo-mechanical simulator. To describe the hot-working behaviour, the steel was compressed to the various amount of deformation (4x0.29, 4x0.23 and 4x0.19). The microstructure evolution in successive stages of deformation was determined in metallographic investigations using light microscopy. The flow stresses are much higher in comparison with austenitic Cr-Ni and Cr-Mn steels and slightly higher compared to Fe-(15-25) Mn alloys. Making use of dynamic and metadynamic recrystallization, it is possible to refine the microstructure and to decrease the flow stress during the last deformation at 850°C. Applying the true strains of 0.23 and 0.19 requires the microstructure refinement by static recrystallization. The obtained microstructure – hot-working relationships can be useful in the determination of powerful parameters of hot-rolling and to design a rolling schedule for high-manganese steel sheets with fine-grained austenitic structures.

Abstract: Compressive deformation behaviors of low carbon steels with different Nb contents were investigated in the temperature range 900oC to 1100oC and strain rates from 0.05s-1 to 2s-1 by single pass deformation. Multi-pass compressive deformation processes were also carried out to examine strain accumulation under different Nb contents. In single pass deformations, dynamic recrystallization (DRX) can be observed in the case of low strain rate and high temperature, and the higher Nb steel exhibits higher deformation activation energy (Qdef) and critical strain value (εc) for the onset of DRX. However during multi-pass compression process (interval time of 3-4s), the higher Nb steel has larger strain accumulation between passes, so it is easier for high Nb steel that DRX happens during hot strip rolling process, which starts at relative high rolling temperature.

Abstract: In recent years, there has been an increasing interest in magnetic shape memory alloys (MSMAs) due to their unique ability to produce very large output strains and rapid response frequency. NiMnCoIn is a new-type MSMAs in which a reversible magnetic-field-induced phase transformation is observed. The microstructural evolution in the process of dynamic recrystallization in polycrystalline Ni45Co5Mn36.7In13.3 was studied in the present paper. The experimental results showed that the high deformation temperature and slow strain rate were necessary to achieve perfect dynamic-recrystallizing microstructure in Ni45Co5Mn36.7In13.3 alloy. Precipitates with two sizes were observed. The content of Co in precipitates was higher than that in the matrix alloy, while the content of In was lower than that in the matrix alloy.

Abstract: Dynamic recrystallization behavior of Co-29Cr-6Mo-0.16N alloy was analyzed in details. Compression tests were carried out in a computer aided Thermecmaster- Z hot forging simulator. The results showed that uniformly distributed superfine grain size could be obtained by continuous dynamic recrystallization (DRX) process; Texture-free microstructure with uniformly distributed equiaxed fine grains was obtained. The formation of profuse stacking faults and their subsequent intersections are considered to be the principle mechanisms of DRX.