Authors: Fu Zhen Xuan, Bo Zhang, Shan Tung Tu
Abstract: An interfacial resistance measuring method was proposed to evaluate the quality of
diffusion bonded joints. To study the feasibility of the method, a finite element (FE) model with
periodically distributed interfacial microdefects was presented. The influences of bonded area
fraction, width and length of microdefects on increments of resistance were analyzed by applying the
electromagnetic module in ANSYS software. Results indicated that the evolution of resistance
increment along with the interfacial bonded area fraction could be described by a hyperbolic function.
Based on the FE results, a modified theoretical solution was developed referred to Lodge’s work to
accommodate the size effects of interfacial microdefect and thus could lead to a more precise quality
evaluation for diffusion bonded joints.
1944
Authors: Keitaro Yamashita, Akira Shimamoto
Abstract: The method of generating the most practicable shape recovery force in smart composite
materials which embedded shape-memory alloy (SMA) fiber under the resin matrix is electric
heating. However, because the calorie for the heating of the resin matrix increases in the low
temperature environment, it is necessary to control the electric heating corresponding to an ambient
temperature to obtaining a steady shape recovery force. Then, the method of self-detecting the
temperature without using a special temperature sensor by measuring the electrical resistance of the
SMA fiber in the composite material was examined.
965
Authors: Hiroki Inoue, Keiji Ogi
Abstract: This paper describes the piezoresistance behavior in CFRP cross-ply laminates with
transverse cracking loaded in tension. The resistance change due to transverse cracking and the gage
factor (the rate of resistance change per mechanical strain) for each transverse crack density were
experimentally measured during loading/unloading cycles. The resistance change-strain curves in the
unloading/ reloading processes show the bilinear behavior where two gage factors are defined as the
slopes of the bilinear curve. The residual resistance change after full unloading increases almost
linearly with the mechanical strain while the gage factors do not always increase with the strain. The
residual resistance change and gage factors are associated with transverse crack density on the basis of
an equivalent resistance circuit.
961
Authors: Seung Hyun Baik, Byeong Soo Lim, Seung Jin Ryu, Dae Hyun Choi, Bum Joon Kim, Se Young Oh, Byung Ho Sung, Jee Hoon Choi, Chul Ju Kim
Abstract: Carbon nanotubes have received considerable attention because of their excellent
electrical and mechanical properties. In this study, carbon nanotube - copper nanocomposites with
homogeneously dispersed nanotubes within the copper matrix have been fabricated by two different
methods; a mechanical mixing process and a molecular-level mixing process, which consists of
mixing copper ions with functionalized nanotubes in a solvent. Small punch creep tests showed
significantly improved mechanical properties of the nanocomposites. The electrical resistance of the
nanocomposites also decreased.
285
Authors: Akira Todoroki, Kazuomi Omagari, Masahito Ueda
Abstract: For a cryogenic fuel tank of a next generation rocket, a Carbon Fiber Reinforced Plastic
(CFRP) laminated composite tank is one of the key technologies. For the fuel tank made from the
laminated composites, matrix cracks are significant problems that cause leak of the fuel. In the
present paper, electrical resistance change method is adopted to monitor the matrix cracking of the
CFRP laminate. Previous studies show that tension load in fiber direction causes electrical
resistance increase due to the piezoresistivity of the carbon fibers, and fiber breakages also cause
the electrical resistance increase of the CFRP laminates. In order to distinguish the electrical
resistance changes due to matrix cracking from those due to the piezoresistivity and the fiber
breakages, residual electrical resistance change under the complete unloading condition is employed
in the present study. Experimental investigations were performed using cross-ply laminates in
cryogenic temperature. As a result, it can be revealed that the residual electrical resistance change is
a useful indicator for matrix crack monitoring of the cross-ply CFRP laminates.
873
Authors: V.V. Ustinov, L.N. Romashev, M.A. Milyaev, T.P. Krinitsina, A.M. Burkhanov
Abstract: The magnetic and magnetoresistive properties of nanostructured Fe/Cr multilayers with
ultra-thin Fe layers (the nominal Fe thickness tFe is down to 0.3 Å) have been investigated at low
temperatures (down to 2 K) in magnetic fields up to 90 kOe. Nanostructures were MBE grown in
ultrahigh vacuum on single crystal MgO substrates. It is shown that Fe layers in nanostructures with
tFe < 2 Å are not continuous but consist of separate ferromagnetic clusters. Such cluster-layered
nanostructures exhibit superparamagnetic properties and the Kondo-like behavior of resistivity.
75
Authors: Minoru Takahashi, Koichiro Adachi, Ruben L. Menchavez, Masayoshi Fuji
Abstract: In this study, we propose a new process to fabricate electrically conductive alumina by
gelcasting and reduction sintering. The process used the conventional gelcasting method except for
varying amounts of monomer at 2.8, 5.5, and 8.0 wt.% relative to the weight of the slurry. In the plastic
mould, the slurry was under in situ solidification for 3 hrs at 25oC to achieve gelation. The freshly gelled
bodies were demolded, carefully dried, and then sintered at 1100oC, 1300oC, and 1550oC in nitrogen
atmosphere. The holding times at 1100oC and 1300oC was 2 hours, while at 1550oC were 2, 4, and 6 hrs.
The sintered alumina body was characterized by electrical property, X-ray diffraction, and scanning
electron microscopy. Results showed that monomer additions and sintering schedule significantly affect
in lowering electrical resistance. The low value was 3.6×106 +cm at 8.0wt.% monomer addition and
sintering at 1550oC for 2 hrs. The effect of physical properties on electrical conductivity and the
corresponding reaction mechanism were discussed in details.
657
Authors: Teruto Kanadani, Keiyu Nakagawa, Norio Hosokawa, Akira Sakakibara, Koji Murakami, Makoto Hino
Abstract: The aging of Al-Zn alloys has been vastly studied for decades. In the previous paper, 0hta
et al. studied carefully the hardness of the alloy during aging and revealed the existence of softer
regions near the surface and the grain boundary than the interior of the specimen even after aging
for a long time. Electrical resistivity measurement and X-ray small angle scattering experiment
together with hardness test suggested that in these regions vacancy decay to the surface and grain
boundaries was severe, thus the growth of GP zones were suppressed and therefore age hardening
was retarded. Also, it is well-known that an addition of a small amount of Ag raised solvus
temperature of GP zones. In this paper, soft surface layer formed in an Al-12mass%Zn alloy is
studied by adding small amount of Ag by means of hardness test and resistometry. Addition of Ag
more than 0.1% decreases the thickness of soft surface layer as well as accelerates age hardening
rate and suppresses the formation of soft region near the grain boundaries. Higher quenching
temperature also reduces the thickness of soft surface layer. Together with the behavior of aging
curves of the specimen with various thicknesses, the origin of the soft surface layer is confirmed to
be the effective role of surface as sinks for vacancies.
1883
Authors: Raluca Savu, Ednan Joanni
Abstract: Nanocrystalline indium tin oxide (ITO) thin films were deposited on Si/SiO2 substrates by laser ablation from a ceramic target with a composition of 0.9 In2O3 . 0.1 SnO2. Samples were prepared in the pressure range from 10-1 to 5mbar, either in-situ at 500°C or at room temperature and heat-treated in air at 500°C. X-ray diffraction results show that the films are not oriented, except the ones made at high temperature which exhibit strong (400) orientation. AFM pictures show that
the grains are round shaped and the sizes are in the range between 50 and 200nm, except for films made in-situ at 10-1mbar which are elongated and faceted. For higher pressures the grains tend to be small and to form agglomerates. The porosity of the films increases with the deposition pressure and the thicknesses reach a maximum of 2.8µm at 1mbar for the films made at room temperature and of 1.2µm at 2mbar for the ones made in-situ; for higher pressures the growth rate drop
drastically, as revealed from SEM observations of cross-sections. The electrical resistance increases with the deposition pressure due to the increase in porosity, changing from 3.3k to 38.9M for films deposited at room temperature and from 20 to 265k for the ones made in-situ.
1161
Authors: Ruben L. Menchavez, Koichiro Adachi, Masayoshi Fuji, Minoru Takahashi
Abstract: This work demonstrated an in-situ pyrolysis of gelcast alumina under reduction sintering to
make alumina and carbon composite in providing semi-electrical conductivity. To increase the carbon
content, the monomer was varied in the premix solution with reduction sintering in nitrogen gas.
Two-probe method was used to measure electrical resistance of the sintered samples. The results
revealed that the increase of monomer addition and sintering treatment were effective in reducing
electrical resistance. The lowest value was 3.6×106-cm, which is a potential candidate for
electrostatic shielding application. The reduction-sintered sample was re-sintered in an air in order to
gain insight on the conductive path due to carbon network. Further tests such as XRD, TGA/DTA,
and scanning electron microscopywere used to explain the semi-conductive property of the material.
493