Authors: Daniella Gomes Rodrigues, Tarcísio Reis Oliveira, Dogoberto Brandão Santos, Berenice Mendonça Gonzalez
Abstract: The cold rolled band of the niobium stabilized type ASTM 430 ferritic stainless steel with 85 % thickness reduction was annealed with heating rates of 0.10, 6.8, 23.5 and 41.5 °C/s and a soaking time of 24 s. The changes in microstructure and texture were followed by interruptions in the annealing cycle at temperatures of 780, 830 and 880 °C. Annealing at the lower heating rate was more effective for the development of γ-fiber than the annealing performed with high heating rate. The increased rate of heating provided an increase in the onset recrystallization temperature, a reduction in average grain diameter and a more homogeneous distribution throughout the thickness. The specimens with higher volume fraction of the γ-fiber annealed with low heating rate showed a high average coefficient of anisotropy R =1.99.
217
Authors: Huai Yi Chiu, Chen Ming Kuo, Huei Sen Wang
Abstract: In order to investigate the creep behavior and understand its deformation mechanism of automotive exhaust pipe materials, this study conducted creep experiments of 409L and 436 ferritic stainless steels at both 600°C and 750°C under different stress levels. After creep tests, crept specimens were analyzed on the microstructure and fracture surfaces by the use of scanning electron microscopy. From creep data, two important material coefficients, namely, M of Monkman-Grant relationship and K of Coble creep equation are calculated for predicting the material creep life. Results show the creep resistance of 436 stainless steel is better than that of 409L stainless steel, because the 436 stainless steel has more Ni, Cr, and Mo contents. As the creep mechanism, all tests show grain boundary diffusion or Coble creep is the dominate deformation mechanism, except at higher temperature 750 °C and higher stress levels.
252
Authors: Xiao Liu, Jing Long Liang
Abstract: The effect of RE on modifying inclusions of 430 ferrite stainless steel was studied by metallographic examination, SEM and electron spectroscopy. Thermodynamic calculation was used to analyze the formation of RE inclusions in 430 ferrite stainless steel. The result shows that sulfide and other irregular inclusions are modified to round or oval-shaped RE2O2S and RES.
441
Authors: Tae Soo Kim, Min Seung Kim
Abstract: Based on the existing test results of single shear bolted connection fabricated with cold-formed ferritic stainless steel, in this study, the experiment for double shear bolted connections with bolt arrangements(1×2, 2×2) and end distance parallel to the loading direction as main variables has been performed. Specimens were planed with a constant dimension of edge distance perpendicular to the loading direction, bolt diameter, pitch and gauge. Ultimate strength and fracture mode obtained from test results were compared with those predicted by current American and Japan design codes such as AISI and AIJ.
976
Authors: Matias de Angelis Korb, Raimundo Nonato Ferreira Linhares Junior, Eduardo Etzberger Feistauer, Ledjane Silva Barreto, Vânia Caldas de Sousa, Iduvirges Lourdes Müller, Célia de Fraga Malfatti
Abstract: Ferritic stainless steels have been used to produce interconnects for intermediate temperature solid oxide fuel cells (ITSOFC) due to their appropriate properties. Ferritic stainless steel presents mechanical stability, much higher thermal and electronic conductivities; significantly lower cost, and mechanical resistance than austenitic steels. Besides, it presents a thermal expansion coefficient compatible with the other materials of the cell components. However, in the range of this device operating temperature (600 °C 800 °C) it can occur the formation of poorly conducting oxide (Cr2O3) reducing the fuel cell performance. The aim of this work was to obtain oxide coatings starting with La, Sr and Co nitrates applied by spray-pyrolysis technique on a stainless steel AISI 430 substrate. The coatings obtained were characterized by X-ray diffraction and scanning electron microscopy/energy dispersive spectroscopy. The oxidation resistance of the ferritic stainless steel, coated with a perovskite (La0,6Sr0,4CoO3) film, was investigated by isothermal oxidation. The results showed that the coating obtained promoted the increase of the ferritic stainless steel oxidation resistance. However, after the oxidation test, it was observed a Cr enrichment and a very pronounced Sr enrichment, near to the alloy/coating interface, which can be associate to the decomposition of La0,6Sr0,4CoO3 film.
522
Authors: Jiang Ning Deng, De Chao Xu, Lei Su, Gang Dong, Yan Dong Liu
Abstract: In this paper, the welding microstructure of Ferritic Stainless Steel sheet with different Ti, Nb elements were studied. The experiment results shows that the addition of alloying element Ti +Nb stabilization steel causes the precipitation of Nb(CN) and TiN. This can reduce the C content, so the temperature of Ac1 increases, then it would be difficult to get martensite. Due to Martensite is harmful for toughness, so Ti+Nb elements are in need.
1473
Authors: Jolanta Baranowska, Paweł Kochmański, Jarosław Bielawski
Abstract: This paper presents results of investigations on gas nitride layers of stainless steel. Steel with ferritic structure, containing different chromium and nickel content was used in the experiments in order to compare the influence of these two main alloying elements on layer growth kinetics and layer structure. Particular attention was paid to formation of Sphase and expanded martensite which usually are formed during lowtemperature nitriding of stainless steel. It was observed, that chromium and nickel content does not have a significant influence on layer growth kinetics but the treatment temperature does. It was also stated that Sphase formation is possible both in nickel alloyed and nickelfree steel depending on treatment parameters.
297
Authors: Dong Hua Guo, De Wen Ma, Zhi Yong Zhang, Xue Feng Ma
Abstract: This paper explains the economy and mechanical properties of the ferritic stainless steel used as the materials of the traffic sign substrate plate, analyzes the relationship between the density of the ferritic stainless steel and the thickness of the substrate plate, proposes a method to determine the quality of the welding, and describes the corrosion mechanism and processing performance of the ferritic stainless steel substrate plate while proposing the related improving ways. The results showed that: by reducing the thickness, ensuring the overall load, adopting the tempering control to reduce the contents of the C, N and other impurities, adding the alloy elements such as the Cr, Mo, Ti, Nb to lower the corrosion, and reducing the C, N, S, P, O and other impurity elements to improve the welding performance, the ferritic stainless steel can be a good material for the traffic sign substrate plate.
227
Authors: Antônio Claret Soares Sabioni, Emiliane Advíncula Malheiros, Vincent Ji, François Jomard
Abstract: In order to investigate the role of oxygen diffusion in the oxidation process of the AISI 439 ferritic stainless steel, oxygen ion diffusion coefficients were determined, for the first time, in oxide films formed by the oxidation of this steel. Steel samples were firstly oxidized from 750o C to 900o C, in synthetic air, in order to grow oxide films mainly made up of chrome oxide; the oxygen diffusion experiments were then performed using the stable isotope 18O as oxygen tracer. The introduction of the 18O in the oxide film was performed by means of the gas-solid isotopic exchange method, in the temperature range of 750-900o C, in Ar+21%18O2 atmosphere. The 18O diffusion profiles were established by secondary ion mass spectrometry (SIMS). Parabolic oxidation constants calculated by means of Wagner´s theory, using the oxygen ion diffusion coefficient determined by our experimental process, are greater than oxidation constants previously determined in oxidation experiments from 850 to 950º C, in air, which indicates that the oxygen ion diffusion is large enough to assure the growth rate of the oxide film formed by the oxidation of the AISI 439 steel in these temperatures.
339
Authors: Anna P. Kisko, Pasi P. Suikkanen, C. Isaac Garcia, K. Cho, M. Hua, L. Pentti Karjalainen, Anthony J. DeArdo
Abstract: The annealing behavior of cold rolled Type 430 ferritic stainless steel is the subject of this paper. The steel was cold rolled 79%, then heated at 6 °C/s to the soaking temperature of 841 °C, which is just below the Ae1 temperature. During heating, specimens were quenched from selected temperatures between 650 and 841 °C and after various times at 841 °C. These quenched samples underwent metallographic examination and micro-hardness determination. The results indicated that under the prevailing experimental conditions, the hardness appeared to correlate strongly with the extent of recrystallization. The kinetics of recrystallization appeared to originate in the cold worked state, where three kinds of grain were found: (i) smooth elongated, featureless of α-fiber orientation {001}<100>; (ii) irregular fishbone grains of the γ-fiber orientations {111}<112> plus {111}<110>; and (iii) twisted grains of the η-fiber orientation {001}<100>. It was found that the twisted grains of the η-fiber were the first to recrystallize, with the fishbone grains of the γ-fiber second, and the smooth elongated, featureless grains of the α-fiber last. It was found that the grains of the α-fiber orientation {001}<100> and the η-fiber orientation {001}<100> were replaced with grains of the γ-fiber orientations as recrystallization progressed. These results are discussed in terms of recrystallization and texture development.
437