Papers by Keyword: Globularization

Abstract: Microstructure evolution and mechanical behavior of alpha/beta Ti-6Al-4V and Ti-6Al-4V-0.75Mo-0.5Fe titanium alloys during uniaxial compression to a height strain of 70% was studied. The plastic-flow response for both alloys is characterized by successive stages of strain hardening, flow softening, and steady-state flow. During compression the lamellae spheroidized to produce a globular microstructure with higher rate of globularization in Ti-6Al-4V-0.75Mo-0.5Fe. The globularization kinetics in Ti-6Al-4V-0.75Mo-0.5Fe was also found to be much faster than that in Ti-6Al-4V. This difference can be partially associated with different interphase energy due to doping of β-stabilizing elements.

Abstract: Ti6Al4V samples were isothermally compressed using a Gleeble^(TM) 1500D thermo-mechanical simulator. Differential scanning calorimetry (DSC), microstructural analyses, and thermodynamic calculations were used to investigate the sequence of transformation of β into α or vice-versa and the presence of different phases in the compressed Ti6Al4V sample. Globular alpha phase was revealed in the isothermally compressed sample in addition to martensitic and lamellar α/β structures. The transition temperature range of β into α-phase was determined using the DSC thermograms and thermodynamic calculated diagrams. The fraction of α-phase globulized increased as the strain rate decreased from 0.01s^-1 to 10^-3s^-1, and the spheroidization of the α-phase is only possible in a specific range of deformation temperatures.

Abstract: Microstructure evolution and mechanical behavior of alpha/beta Ti-6Al-4V titanium alloy with initial α-colony microstructure during uniaxial compression at 600 and 800°C to a height strain of 70% were studied. It was shown that decrease in deformation temperature considerably influences on the kinetics of globularization of a lamellar microstructure. At the lower temperature stages of strengthening and softening extend that associates with inhibition of globularization. Deformation at 600°C is also associated with a smaller fraction of high-angle boundaries during deformation, smaller fraction of globular grains, increased contribution of shear deformation and more intensive rotation of α-lamellae towards the metal flow direction. In contrast to 800°C, the rate of thinning of α-lamellae at the lower temperature is noticeably higher. The results obtained are related to the change of the type of dislocation slip in α-lamellae due to inhibition of dynamic recovery with decreasing deformation temperature.

Abstract: The effect of initial lamellar structure of β heat treated Ti-6Al-4V alloy on the globularization behavior during the multi-step forging was investigated. Specimens of different lamellar thicknesses were upsetted and stretched by side pressing repeatedly, i.e. multi-step forging, at the sub-transus temperature to break down the lamellar structure. The microstructural changes after multi-step forging were analyzed in the light of globularization behavior. The results showed that the thick lamellar structure was more difficult to be transformed to homogeneous equiaxed structure than thin lamellar structure.

Abstract: Semi-solid slurry for a rheocasting process requires a fine and globular structure of primary solid phase. In the present study, in order to find an optimum preheating temperature of a multiplex-type slurry cup in the slurry maker that we recently developed for the rheocasting process, the semi-solid slurry was held for a various time of up to 60 min. in a multiplex-type slurry cup preheated at a different temperature. A size and morphology of primary solid phase of the semisolid slurry was measured and analyzed with the difference of the recorded cooling curve during the solidification with respect to a preheating temperature of the slurry cup. Also, a microstructural evolution and globularization mechanism occurred during the isothermal holding were discussed. Finally, as considering the effect of a different casting condition on the morphology of primary solid phase the optimum manufacturing condition of the semi-solid slurry for the rheocasting process was proposed.

Abstract: Forming of alloy and composite within a solid-liquid region, i.e. thixo-forming and rheo-forming, has been recognized as a technology offering several potential advantages over casting and forging such as a low forming pressure, reduction of macrosegregation, and reduction of porosity. In this paper, a globularization for primary solid phase by a forced fluid flow in melt due to electromagnetic stirring during solidification and isothermal stirring at solid-liquid region, was examined to produce Al alloy having a globular solid phase to get a thixotropic behavior. The electromagnetic stirrer was specially designed and manufactured to create all kind of fluid flow pattern such as a circumferential, vertical, helicoidally and contra-rotating flow pattern during the solidification of a melt. The size and roundness of primary solid phase of the quenched sample after isothermal stirring at solid-liquid region were measured with respect to a stirring time and frequency. The globularization of solid phase was enhanced with incresing the stirring time and electromagnetic flux density, i.e. stirring strength.

Abstract: Microstructure evolution in alpha-beta Ti-64 alloy samples with lamellar structure deformed to a height reduction of 70% at temperatures between 450 and 800°C has been investigated. The deformation led to a distinctly globularized structure of α- and β-phase in the whole temperature interval. The dependence of globular grain size on deformation temperature is of a linear character up to the temperature of warm deformation at which formation of an SMC structure takes place. Continuous recrystallization was observed in the α-and β-phases. Different types of defects responsible for splitting of α-lamellae such as low and high angle boundaries, shear bands and twins were found. An investigation of boundary misorientation spectra in the α-and β-phases deformed to different strains at 550 and 800°C was carried out. Typical boundary misorientation spectra for single phase metals with the same lattice were obtained. The boundary misorientation spectrum depends weakly on strain and deformation temperature. The results of this study show the importance of transformation of semi-coherent interphase boundaries to non-coherent ones for globularization of lamellar microstructures.

Abstract: Prediction of final microstructures after high temperature forming of Ti-6Al-4V alloy was´attempted in this study. Using two typical microstructures, i.e., equiaxed and Widmanstätten microstructures, compression test was carried out up to the strain level of 0.6 at various temperatures (700 ~ 1100°C) and strain rates (10^-4 ~ 10²/s). From the flow stress-strain data, parameters such as strain rate sensitivity (m) and activation energy (Q) were calculated and used to establish constitutive equations for both microstructures. Then, finite element analysis was performed to predict the final microstructure of the deformed body, which was well accorded with the experimental results.