Papers by Keyword: Grain Growth

Abstract: A new efficient numerical solver inspired by front-tracking concepts is implemented within the DIGIMU® framework to accelerate full-field simulations of microstructural evolution. The solver is applied to AISI 304L stainless steel and compared with the conventional level-set formulation under laboratory hot-torsion tests and industrial multi-pass hot rolling conditions. After a limited recalibration of grain boundary mobility and solute drag parameters, both solvers provide comparable predictions of recrystallization kinetics, grain size evolution and final microstructures. The new solver achieves a reduction in computational cost close to two orders of magnitude, while preserving the predictive capabilities of DIGIMU®, thereby enabling more efficient industrial-scale simulations. Simulated predictions will be compared to Ugitech experimental work on lab torsion tests and industrial extrusion processes.

Abstract: This paper presents experimental results on the processing of complex concentrated alloy with a nominal composition of A_0.35CoCrFeNi. The alloy was produced by vacuum induction melting and tilt casting. The microstructure of the as-cast CCA consists of dendritic and interdendritic regions homogenized by heat treatment at 1360 °C. After rotary swaging at room temperature, the microstructure is characterized by an abundance of dislocations and continuously intersecting slip bands. Annealing experiments were carried out in the temperature range of 1150 °C – 1300 °C and different holding times to determine the parameters of grain growth kinetics. Phase and chemical analysis were investigated using XRD and EDS methods. The activation energy of recrystallization in the studied composition was 458 kJ mol^-1. The influence of grain size on room temperature mechanical properties and tensile properties was determined. The hardening coefficients k_h and k_σ, calculated using the Hall-Petch relation, were 277.5 HV µm^-1/2 and 655 MPa µm^-1/2, indicating the effectiveness of grain boundary hardening in the studied single-phase CCA.

Abstract: Extensive simulations applying the Monte Carlo Potts model were carried out on a twodimensional square lattice to evaluate the influence of higher lattice temperatures on grain growth kinetics and the Zener limit. A wide range of simulation temperatures (KTs) were applied on a matrixof size 1000² with Q-state 64. They were then dispersed with a wide range of second-phase particles and ran to 100,000 Monte Carlo steps. The critical temperature for a square lattice with eight nearest neighbors (8 NN) was established as KTs = 0.4, after evaluating several growth parameters, undersimulated thermal conditions. Simulations were then next run to stagnation, for higher temperatures up to the critical value of KTs, and various growth parameters were computed in the pinned state. The Zener limit was found to scale with the square root of the surface fraction of second-phase particleswhile varying exponentially with its fraction lying on the grain boundaries.

Abstract: Owing to their several attractive features such as high hardness, high elastic modulus, light weight, high strength to weight ratio, high thermal conductivity, and high temperature strength, composites from Al-Mg₂Si family offers promise towards deployment in several industries such as automobile, aerospace, marine, defence and electronic. The present molecular dynamics (employing LAMMPS) based simulation study is one of the first attempt to investigate the nucleation and grain growth mechanisms of Mg₂Si phase at atomic level in case of novel Al-15Mg₂Si-4.5Si composite, during semi-solid processing. Modified embedded atom method (MEAM) potential has been used to study the atomic interactions in the composite. Reaching the melt state at 1000 K, the temperature of the system is first decreased from 1000 K to 853 K and then the system is held at 853 K for 100 ps. The simulations are performed with three different cooling rates. With lowering of temperature, randomly distributed Mg and Si atoms form atomic clusters at arbitrary locations within the system, which is the nucleation stage for Mg₂Si phase formation. Cluster size, radial distribution function has been used to investigate the structural evolution of Mg-Si clusters. Cooling rate significantly influences the grain size as well as the grain growth kinetics. The information about the thermodynamic state of the system has been revealed by extracting the values of internal energy, enthalpy, specific heat. during the slurry preparation and isothermal holding stages. The growth mechanism of Mg₂Si nucleus has been characterized from the temporal variation of (Mg + Si) atoms taking part in the cluster formation. Power-law variation is observed in the cooling stage whereas a linear variation is observed in the isothermal stage.

Abstract: While the role of Nb in flat rolling of low carbon steels has been investigated in many works, the information about the use of Nb in rebar rolling of higher carbon grades is more limited. Rebar rolling presents differences relative to flat rolling that can affect the role of Nb, such as the application of higher number of rolling passes, higher strain rates, lower interpass times, and, consequently, enhanced adiabatic heating. Increasing the number of passes can contribute to austenite grain refinement. However, the high finishing temperatures in rebar rolling can lead also to significant austenite grain growth and microstructural heterogeneity development before phase transformation. This phenomenon will directly influence the final grain size and can also lead to the appearance of second hard phases in the final product. One of the options to avoid austenite grain growth is to add microalloying elements that retard grain growth kinetics, either in solid solution or as precipitates. This can open new roles for the application of Nb in rebar rolling. To analyze this, in this work laboratory torsion tests were performed with two 0.2%C steels microalloyed with two different Nb contents (0.029% and 0.015%). Soaking temperatures from 1100°C to 1250°C were applied to obtain different amounts of Nb in solid solution before grain growth study. The study shows that not only finish rolling temperature and cooling time, but also reheating temperature and the amount of Nb remaining in the form of undissolved precipitates are important factors controlling austenite grain growth.

Abstract: High-pressure torsion (HPT) was conducted under 6.0 GPa on commercial purity titanium up to 10 turns. An ultrafine-grained (UFG) pure Ti with an average grain size of ~96 nm was obtained. The thermal properties of these samples were studied by using differential scanning calorimeter (DSC) which allowed the quantitative determination of the evolution of stored energy, the recrystallization temperatures, the activation energy involved in the recrystallization of the material and the evolution of the recrystallized fraction with temperature. The results show that the stored energy increases, beyond which the stored energy seems to level off to a saturated value with increase of HPT up to 5 turns. An average activation energy of about 101 kJ/mol for the recrystallization of 5 turns samples was determined. Also, the thermal stability of the grains of the 5 turns samples with subsequent heat treatments were investigated by microstructural analysis and Vickers microhardness measurements. It is shown that the average grain size remains below 246 nm when the annealing temperature is below 500 °C, and the size of the grains increases significantly for samples at the annealing temperature of 600 °C.

Abstract: Fatigue crack growth resistance of ultrafine grained Cu processed by equal channel angular pressing (ECAP) was investigated. Particular emphasis was devoted to the effects of microstructure evolution on fatigue crack growth in the near-threshold regime. The ultrafine grained Cu exhibits a lower fatigue threshold than coarse-grained Cu at stress ratios of 0.1 and 0.7. Fatigue induced coarsening of the UFG structure near the fatigue crack and intergranular fatigue crack growth are observed.

Abstract: In this present study, molecular dynamics simulation of creep for ultrafine grain NC Ni specimens with different grain sizes have been carried out under a constant 1 GPa applied load for various creep temperatures to study the dependence of grain growth on creep temperature and grain size during creep process and its influence on creep properties. It is observed that the extent of grain growth in ultrafine grain NC Ni during creep deformation process is more if creep in creep temperature is higher. A noteworthy anomaly, that is NC Ni with smaller grain exhibits better creep property compared to NC Ni with larger grain, is observed in case of higher creep temperatures (i.e. around or greater than 1400K).

Abstract: The high strength silicon steel HY-TUF, applied for manufacturing of the heavy loaded aerospace and engineering parts, was investigated. The effect of the heating temperature in the range 900...1000 °C on the austenite grain size was studied. The steel under consideration had a significant scatter of the austenite grain size. The most intensive growth of the austenite grains was observed in the temperature range 975...1000 °C.

Abstract: Nowadays, by increase in using structural materials, the high temperature properties of these materials are became an important issue within different aspects of engineering. The new Oxide Precipitation Hardened (OPH) steel generated by the authors based on Fe-Al-O matrix which prepared by mechanical alloying and hot consolidation. These new OPH steels showed a better oxidation resistant and creep, compare to similar ones. In order to investigate the thermomechanical and microstructure of these materials, a series of different tests were performed on three different OPH steels variant which developed and manufactured by the authors. The results show that the heating temperature has a significant influence on these properties while almost total recrystallization of grains and subgrains were observed during the investigation.