Authors: Ruo Han Chang, Zhong Yi Cai, Chao Jie Che
Abstract: The true stress-strain data from isothermal hot compression tests on Gleeble-1500D thermo mechanical simulator, in a wide range of temperatures (350-450°C) and strain rates (0.001-1s-1), was employed to establish the PSO-BP network prediction model and 3D processing map of Mg-Sm-Zn-Zr alloy. It was found that the PSO-BP model could be efficient and accurate in predicting flow stress, most of relative errors were in the range of -4% to 6%, and the average relative error was found to be 1.52%. Then considering the effect of strain, the 3D processing map was established to characterize the hot workability of the alloy. The 3D processing map exhibited the maximum efficiency domain and the instability domain, which could be used to determine the optimal deformation conditions. The optimum processing parameters of Mg-Sm-Zn-Zr alloy were deformation temperatures of 400-450°C and strain rates of 0.003-0.1s-1.
252
Authors: Guo Bao Yang, Ze Kun Yao, Yan Hui Liu, Yang Nan, Yong Quan Ning
Abstract: Isothermal compression tests were carried out on GH4133B superalloy at 940–1060°C (below nominal γ΄-transus temperature of 1080°C) and 0.001–1.0s-1. The processing maps were constructed to evaluate the efficiency of power dissipation (η) and recognize the flow instability regimes. Our investigations demonstrate that true strain takes great effect on processing maps' evolution. At 1020°C/1.0s-1, the efficiency value η undergoes a small decline at low strains, and then increases linearly from 0.26 to 0.58 at high strains. However, the efficiency value remains high constant (η=0.40) with the increased strain under the condition of 980°C/0.001s-1. As a result, hot deformation can be carried out firstly at 980°C/0.001s-1 with small strain about 0.35 and then carried out at 1020°C/1.0s-1 to get fine homogeneous microstructure. There are two instability regimes respectively located around 940°C/1.0s-1 and 1060°C/0.001s-1 when the strains are 0.05–0.40. Moreover, there is another instability regime located around 1060°C/1.0s-1 when the strains are 0.45–0.69.
1459
Authors: N. Gonzalez, M.C. Revilla, Beatriz López, J.M. Rodriguez-Ibabe
Abstract: Free cutting steels belong to a family associated with hot workability problems. This study has focused on the analysis of microstructural features located near the surface of the billet before and after reheating and how they can affect the nucleation/propagation of damage during initial hot working operations. The work has been done with free cutting steels containing sulfur contents ranging from 0.32 to 0.42%. The relevance of clustering of inclusions, their location at grain boundaries or triple points and the influence of softening mechanisms (as recrystallization) have been considered with the help of several parameters determined by image analysis techniques.
777
Authors: Carlo Alberto Biffi, Paola Bassani, Riccardo Casati, Maurizio Vedani, Ausonio Tuissi
Abstract: In the present work an investigation on primary processing of CuZr based shape memory alloys is proposed. In particular, the study addresses the effect of hot rolling process on the properties of CuZr shape memory alloys, in which the addition of some elements, such as Cr, Co and Ni, is taken into account. These alloys are produced by means of vacuum arc melting furnace under non contaminating conditions. Considering the high reactivity of these alloys, due to Zr element, hot working was undertaken after sealing the ingot cigars in a stainless steel protective can. The characterization of the rolled alloys is performed using DSC in terms of evolution of martensitic transfor-mation temperatures. The analysis is completed with mechanical and the microstructure investigations by means of microhardness and scanning electron microscopy (SEM) observations, respectively. The main result of this work is the evaluation of hot workability property of this system, which can be improved by adding metallic elements to the binary CuZr intermetallic system. Moreover, interesting characteristics, such as high transformation temperatures, thermal stability and reduced thermal hysteresis, can be also improved by means of the addition of Ni and Co at the same time.
534
Authors: Sunil Nair, Dominic Savio, Y. M. Srinivas, K.R. Srinivasan
Abstract: Specialty stainless steels designed with higher levels of Chromium, Nickel and Molybdenum than the general austenitic grades AISI 304 and AISI 316 have distinctly superior corrosion resistance properties. The commercial production of such high alloyed stainless steels came with advent of improved steel melting, refining and casting technologies. These technological improvements made it possible to produce such steels with low carbon levels and close control of chemical composition necessary to achieve the desired phase balance and avoid formation of undesirable intermetallic phases. Further, ability to achieve low sulphur levels combined with freedom from undesirable level of tramp elements improved the hot workability characteristics. Thermodynamic aspects of steelmaking and refining in Vacuum Oxygen Decarburization ( VOD) process for manufacture of specialty grades 904L (24% Ni, 20% Cr, 4% Mo, 1.2%Cu) , 317LM ( 19% Cr, 14.5% Ni, 4% Mo,) , 2205 ( 22.5% Cr, 5% Ni, 3% Mo) at Mukand through the Triplex process route ( Ultra High Power Furnace Oxygen Top and Bottom Blown Convertor VOD) are outlined. The effects of undesirable intermetallic phases, particularly sigma phase, on mechanical and corrosion properties are discussed. Application areas for such specialty grades are reviewed. Keywords: High alloyed Stainless steels, triplex process, sigma phase, intermetallic phases, tramp elements, hot workability, corrosion properties, vacuum oxygen decarburization.
90
Authors: Woo Young Jung, Tae Kwon Ha
Abstract: The hot deformation behavior of a high strength low alloy (HSLA) steel for construction application under hot working conditions in the temperature range of 900 to 1100 and strain rate range from 0.1 to 10 s-1 has been studied by performing a series of hot compression tests. The dynamic materials model has been employed for developing the processing maps, which show variation of the efficiency of power dissipation with temperature and strain rate. Also the Kumars model has been used for developing the instability map, which shows variation of the instability for plastic deformation with temperature and strain rate. The efficiency of power dissipation increased with decreasing strain rate and increasing temperature. High efficiency of power dissipation over 20 % was obtained at a finite strain level of 0.3 under the conditions of strain rate lower than 1 s-1 and temperature higher than 1050. Plastic instability was expected in the regime of temperatures lower than 1000°C and strain rate lower than 0.3 s-1.
178
Authors: Wei Jie Lu, Jun Qiang Lu, Di Zhang, Hong Liang Hou
Abstract: Ti-6Al-4V matrix composite (TMC) reinforced with TiB plus TiC was prepared and hydrogenated. Isothermal compression tests and high temperature tensile tests were carried out to study the effect of the hydrogen on hot deformation and superplastic deformation. The flow behaviour and microstructure evaluation of hot deformation was investigated. The results show hydrogen can reduce the flow stress and decrease the deformation temperature or increase the strain rate at the same flow stress level in hot deformation. Hydrogen increasing β phase and promoting dynamic recrystallizaiton (DRX) was considered as the main reasons for hydrogen-induced plasticity in hot deformation. The results of superplastic deformation indicate hydrogen can decrease the superplastic temperature 100°C or increase strain rate one order of magnitude at the same elongation level in superplastic deformation. Hydrogen promoting DRX were considered as the main reason for improvement of superplastic elongation.
835
Authors: Kamineni Pitcheswara Rao, Yellapregada Venkata Rama Krishna Prasad, Norbert Hort, Karl Ulrich Kainer
Abstract: The hot working behavior of Mg-3Sn-2Ca alloy has been investigated in the temperature range 300–500 oC and strain rate range 0.0003–10 s-1, with a view to evaluate the mechanisms and optimum parameters of hot working. For this purpose, a processing map has been developed on the basis of the flow stress data obtained from compression tests. The stress-strain curves exhibited steady state behavior at strain rates lower than 0.01 s-1 and at temperatures higher than 350 oC and flow softening occurred at higher strain rates. The processing map exhibited two dynamic recrystallization domains in the temperature and strain rate ranges: (1) 300–420 oC and 0.0003–0.003 s-1, and (2) 420–500 oC and 0.003–1.0 s-1, the latter one being useful for commercial hot working. Kinetic analysis yielded apparent activation energy values of 161 and 175 kJ/mole in domains (1) and (2) respectively. These values are higher than that for self-diffusion in magnesium suggesting that the large volume fraction of intermetallic particles CaMgSn present in the matrix generates considerable back stress. The processing map reveals a wide regime of flow instability which gets reduced with increase in temperature or decrease in strain rate.
3616
Authors: V.M. Imayev, Renat M. Imayev, Timur G. Khismatullin, T. Oleneva, Volker Gühter, Hans Jörg Fecht
Abstract: Microstructure and hot workability have been considered for a number of -TiAl alloys including -solidifying TNM alloys. All TNM alloys under study showed improved hot workability in cast condition. As was shown for the Ti-45Al-5Nb-1Mo-0.2B alloy, a critical issue of TNM alloys is room temperature ductility in the conditions with lamellar structure.
235
Authors: Tae Kwon Ha, Hyo Tae Jeong, Jae Young Jung
1365