Papers by Keyword: Hot Working

Abstract: Three main rheological laws are found in the literature to describe the strain hardening of materials at high temperatures. The choice of the most suited law to describe a flow stress curve is often discussed as a function of the nature of the material; but it still remains difficult to choose the most appropriate one. These semi-empirical laws systematically comprise two main terms linked either to the dislocations generation or their annihilation.The objective of this paper is to determine by an inverse method which law appears to be the most suited. It is finally demonstrated that the application of one law is mostly equivalent to another. The various laws are overall equivalent and do not help to describe some peculiar physical mechanism of plasticity.

Abstract: Some feature of discontinuous dynamic recrystallization (DRX) in an Fe-0.4%C-18%Mn austenitic steel during isothermal compression tests at temperatures of 973-1373 K and strain rates of 10^-3-10^-1 s^-1 were studied. The DRX microstructures consisted of various grains, i.e., DRX nuclei, growing DRX grains, and work-hardened DRX grains, which differentiated with the grain orientation spread (GOS). DRX was commonly promoted by a decrease in temperature-compensated strain rate, i.e., Zener-Hollomon parameter (Z), corresponding to an increase in deformation temperature and/or a decrease in strain rate. In contrast, the GOS distribution varied non-monotonously with Z. The large area fraction of DRX grains with small GOS below 1° appeared at definite temperature/strain rate conditions. The large fraction above 0.6 of DRX grains with small GOS was observed in DRX microstructures with a large ratio of CSL Σ3 boundary fraction to low-angle subboundary fraction. The GOS distribution in the DRX microstructures is discussed in terms of the DRX grain nucleation and growth rates.

Abstract: This present work examines the influence of niobium in solid solution on the microstructural evolution of pure nickel at various deformation conditions. On this purpose, high-purity nickel and six model nickel-niobium alloys (Ni–0.01, 0.1, 1, 2, 5 and 10 wt. % Nb) were subjected to hot torsion test to large strains within the temperature range from 800 to 1000 °C at strain rates of 0.03, 0.1 and 0.3 s^–1. Microstructural analyses were carried out using both optical and scanning electron microscopy-based electron back-scattered diffraction technique. The overall results showed the key role played by the Nb amount when coupled with various DRX mechanisms involved, i.e. DDRX, CDRX, and GDRX with respect to the prescribed deformation conditions, in reducing grain size and retarding DRX kinetics from which the microstructures of the examined materials such as Ni 2 and 10 wt. % Nb were seen evolving in different ways. In all these deformed materials, a transition from discontinuous dynamic recrystallization to continuous dynamic recrystallization was observed at low temperature and high strain rate whereas only discontinuous dynamic recrystallization occurred at high temperature.

Abstract: Refinement and uniform austenite grains are essential to obtain excellent and homogenous properties for non-quenched and tempered steel, which is mainly affected by static recrystallization of the rolling process. Using the Gleeble-3500 thermal simulation test machine, 20% compression test was carried out for two passes at 850~1050 °C (interval of 50 °C) and different pass interval time conditions to study the static softening and recrystallization behavior of 38MnSiVS non-quenched and tempered steel during deformation process. The effects of strain rate, deformation temperature and interval time on static softening rate and austenite recrystallization fraction were analyzed. The results showed that the increase of deformation temperature and the increase of pass interval time had more significant impact on the static recrystallization volume fraction of 38MnSiVS steel, while the influence of strain rate was relatively smaller. When the deformation temperature was 950 °C or higher, the non-conditioning steel 38MnSiVS could undergo complete recrystallization, and partial recrystallization occurred in the temperature range of 850-950 °C. A static recrystallization volume fraction model of non-regulatory steel 38MnSiVS was established. The static recrystallization activation energy was 296.7 kJ·mol^-1, and the static recrystallization volume fraction model had a relative error of 2%.

Abstract: The macroscopic strain rate sensitivity m and apparent activation energy Q are derived from their microscopic counterparts associated with strain hardening, grain boundary mobility, and nucleation rate in the case of steady state discontinuous dynamic recrystallization (DDRX). The case of solid solutions, involving effects of the solute concentration on strain hardening and boundary mobility, is also taken into consideration. Moreover, three distinct Derby exponents are introduced to refine the correlation between steady state flow stress and average grain size. Hot torsion data and micrographic observations on a set of nickel-niobium alloys are used to assess the predictions of this tentative approach.

Abstract: The modeling of the forming of materials at high homologous temperatures allows obtaining optimum forming parameters, reduced costs and improving final properties of the finished product. In this work, the behavior of the ZK30 Magnesium alloy was characterized by means of compression tests at temperatures 300 to 450oC and strain rates between 0.1 and 8.7 s^-1. Using data from these tests, the parameters of the Garofalo equation are calculated. In addition, by means of the second Lyapunov stability criterion, the optimum temperature at a given temperature is determined which should minimize the appearance of deformation bands and cracks during hot working. This temperature was found to be 641 K (368oC) at 8.7 s^-1.

Abstract: Ductility is the property of a given material to deform without fracture. In other words, is the capacity to maintain a structural stability under stresses. It is an important property that is difficult to predict since many microstructural and experimental factors play a role. A review of the most important approaches on ductility is given in this work with special emphasis in the high temperature deformation and the deformation mechanisms. The stability of materials is also analyzed and new concepts on the conditions for hot working are included. Stability maps are analyzed and conclusions on the various stability criteria are given on the base of magnesium alloys.

Abstract: The aim of this research is to investigate the effect of annealing treatment on mechanical properties and deformability of titanium alloy to form mini gear in squeezing process. Diameter of experimental specimen was 5mm of Grade 2 Ti alloy. It was annealed with temperature in a range of 500 to 1000 °C, resulting in different initial grain sizes. The mechanical properties and hardness of annealed specimens were obtained by means of tensile and micro-hardness test. In addition, a modulus of mini gear die was 0.92 and made of h13 steel. The annealed specimens were inserted in die and squeezed into mini gear. The experimental results show that microstructure of α-phase precipitates when annealing temperature reaches to 600 °C and hold time was 3 hours. The specimen which annealed with a temperature of 700 °C has the maximal elongation and die filling rate. The microstructural of β-phase precipitates when annealing temperature reaches to 1000 °C resulting in brittle behavior and the lowest die-filling rate.

Abstract: During hot rolling, austenite recrystallization determines the grain size evolution and the extent of strain accumulation, and therefore, it can be used to tailor the microstructure and mechanical properties of the final product. However, at the moment, models describing the recrystallization kinetics of high-Mn steels are scarce and they do not take into account the effect of the alloying elements present in these steels. The aim of this work is to provide a quantitative model for the determination of the static recrystallization kinetics valid for a wide range of high-Mn steel compositions. Softening data determined for steels with different Mn (20 to 30%), Al (0 to 1.5%) and C (0.2 to 1%) levels at different strain, strain-rate and temperature conditions were analyzed. Static recrystallization of the investigated high-Mn steels follow Avrami’s law, with n Avrami exponents which are temperature dependent and lower than those determined for low C steels. A dependence of the t0.5 (time for 50% fractional softening) on the carbon content has been also observed and it was incorporated into an equation for the calculation of this parameter.

Abstract: Semi-empirical models for predicting the austenite static recrystallization behavior are widely used in designing thermomechanical treatments to improve final mechanical properties. However, a problem with these models is that their utility can be limited to the range of deformation conditions and chemical compositions they were developed for. This work focuses on the study of the applicability of current recrystallization models to the range of low strain conditions and/or high Nb microalloying additions (≈0.1%). To do so, the recrystallization behavior of two low carbon Nb-Ti microalloyed steels (0.04 and 0.11% Nb and ≈0.01% Ti) has been investigated by torsion tests. Experimental results for recrystallization time and recrystallized grain size have been compared to previously developed equations. It has been observed that at low strains (ε = 0.1) the predictions fail. A dependence of the n Avrami exponent both on temperature and applied strain was also found.