Papers by Keyword: Mechanical Treatment

Abstract: The present work summarizes and presents separate results obtained by the authors when investigating mesoscopic and microscopic internal stresses formed under the conditions of thermal and mechanical treatment of martensitic, pearlitic and austenitic steels. Internal stresses were investigated using the method based on the analysis of bend extinction contours. The results obtained on industrial steels were presented. The sources were described and examples of internal stresses induced by these sources were given. The nature of bending-torsion of the crystal lattice depending on the averaging volume was determined. It has been shown that in martensitic steels along with the increase in the averaging volume (carbide particle → separate martensitic lath → martensite packet→ martensitic plate → grain) the amplitude of bending-torsion of the crystal lattice decreases. The nature of distortions also changes. At large amplitudes and low volumes of averaging they are completely or partly elastic, at large volumes of averaging they are completely plastic. Thereby, distortions are fully driven by the excess dislocation density.

Abstract: In this work, bacterial cellulose was obtained from nata de coco. Initially, the samples were subjected to three types of different condition which were raw, chemical treatment and mechanical treatment. Bacterial cellulose was characterized by Fourier Transform Infrared Spectroscopy (FTIR), X-Ray Diffractometer (XRD) and Field Emission Scanning Electron Microscopy (FESEM). Bacterial cellulose met the specifications of pure cellulose either using chemical or mechanical treatments proved by IR spectra reading. XRD results indicated that the crystallinity of chemical treatment bacterial cellulose is higher than the mechanical treatment bacterial cellulose which was 68.6% and 59.5% respectively. The FESEM analysis shows that the size of the bacterial cellulose that obtained from chemical treatment is smaller than mechanical treatments which were 19.42μm and 50.35μm.

Abstract: For operating under outer space conditions besides providing originally specified protective function, coating should often ensure accomplishment of functional properties, for instance conductivity of electric current. The solution of this problem can be reached by adding powder fillers with specified functional properties into powder paint. The paper deals with development of technique for formation of protective conducting coatings by filling powder paints and treatment in planetary ball mill. For protection of magnesium alloy shells the technique is offered which combines formation of the oxidized sublayer, introduction of electroconductive filler, treatment of the powder mixture in the planetary ball mill and electrostatic deposition of sifted mixture of definite dispersion. This allows sinking of static electricity from cabinets of the equipment for the space-crafts applications in conditions of the outer space.

Abstract: Effects of mechanical treatment, pre-strain and pre-deformation temperature on shape recovery stress of Ti₅₀Ni₄₇Fe₃ shape memory alloys were investigated. Mechanical treatment, consisting of hot-rolling and hot-forging, improved σrmax σrmax (maximum recovery stress), dσr/dT (rate of recovery stress with temperature) and T_s (the temperature at which recovery stress rises sharply). Martensitic transformation and reverse transformation temperatures also increased with increasing the hot-rolling deformation. σrmax and dσr/dT increased with increasing pre-strain at first and then decreased with further increasing of pre-strain, and the maximum values of σrmaxand dσr/dT were obtained at a pre-strain of 10%. On the other hand, σrmaxand dσr/dT decreased with increasing pre-deformation temperature. Upon a hot-rolling of 88% area reduction and pre-deformation of 10% at-150°C, the Ti₅₀Ni₄₇Fe₃ alloy exhibited excellent recovery stress property with the σrmax of 391MPa in combination with dσr/dT of 5.09.

Abstract: The disposal of PV systems will become a problem in view of the continually increasing production of PV modules. Development for waste PV modules recycling would be extremely effective in coping with this problem. In Europe, the thermal method and chemical method for PV recycling were deeply developed. The thermal treatment was to separate the module components under 600°C. The chemical treatment is to recover silicon wafers out of solar cells, which can be used again in modules. But automated separation of components and advanced chemical process needs to be studied on. In China, mechanical treatment research for PV recycling has just started. PV modules were separated and recycled by abrasive machining under the cryogenic condition and electrostatic separation. The mechanical treatment can't recycle silicon to reprocess new wafers for its low purity. Compared to the advanced technology in Europe, PV recycling in China is primary and badly in need of improving to face the huge PV module recycling demands in future.

Abstract: The wasted cement mortar and internal cracks induced by the secondary breaking process existing on/in recycled aggregates lead to significant reductions in the apparent density, strength and durability of recycled aggregate concrete compared to those of natural aggregate concrete. In this study, recycled aggregate intensification approaches was proposed by removing the old cement mortar from recycled aggregate surface through mechanical agitation, and immersing the recycled aggregate in chemical solutions. A series of laboratory experiments were carried out to validate that the proposed approach could improve various performances of the recycled aggregate, as well as the concrete made of it. The testing results showed that through the combination treatment or modification of mechanical and chemical intensification, both of the compressive and flexural strength of the recycled aggregate concrete could be increased to some extent.

Abstract: AlN ceramics used in electronic substrates and packages are fabricated by the densification of green bodies with sintering aids such as rare-earth oxides. The homogeneous dispersion of the sintering aids, achieved with the help of the mechanochemical bonding of several types of fine powders, is the key process for obtaining a good sinterability and high performance. In this study, we fabricated the AlN ceramics using AlN and nano-Y2O3 composite particles prepared by mechanical treatment. The AlN powder and nano-Y2O3 powder were ball-milled with Al2O3 balls and a dispersant in ethanol in a plastic pot. The powder mixture of AlN and Y2O3 was composited by mechanical treatment. The composite powder was granulated and pressed to obtain a green body. After dewaxing, the AlN green body was fired at 1800°C in 0.6 MPa N2. The sintered body possessed a fracture toughness of 3.6 Pa•m1/2, higher than that, 3.1 Pa•m1/2, of the AlN ceramics fabricated without the mechanical treatment. An observation of the fractured surface revealed that grain boundary reinforcement enhances the fracture toughness of the AlN ceramics made of composite particles.

Abstract: TiN nanoparticle-dispersed Si3N4 ceramics is one of the typical ceramics used for bearing applications. Because larger TiN particles considerably damage the mating metallic materials, smaller TiN particles must be dispersed in Si3N4 ceramics. In this study, we fabricated TiN nanoparticle-dispersed Si3N4 ceramics from Si3N4–nano TiO2 composite particles prepared by mechanical treatment. The mechanical properties of the fabricated TiN nanoparticle-dispersed Si3N4 ceramics were evaluated. At first, TiO2 nanoparticles were dispersed in ethanol using polyethylene imide as a dispersant with a lower molecular weight. Si3N4 powder was mixed with this slurry to obtain a powder mixture. In this case, the reaggregation of the TiO2 nanoparticles during the drying process is the problem that has to be solved. In this study, TiO2 nanoparticles and Si3N4 particles were mechanically joined by a particle composer to fabricate the composite particles from the powder mixture. TiN nanoparticles were uniformly dispersed in Si3N4 ceramics by using composite powder. The bending strength of the developed Si3N4 ceramics with TiN nanoparticles was improved, and its distribution was narrow due to the homogeneous dispersion of TiN nanoparticles.