Papers by Keyword: Metadynamic Recrystallization

Abstract: The present work provides a summary of the recent findings obtained from the experimental investigation of the grain structure, crystallographic texture and dislocation substructure evolution in an austenitic Ni-30%Fe model alloy during dynamic recrystallization (DRX) and post-dynamic annealing. It has been found that the DRX texture characteristics become increasingly dominated by the low Taylor factor grains during DRX development, which presumably results from the preferred nucleation and lower consumption rates of these grains. The substructure of DRX grains is random in character and displays complex, hierarchical subgrain/cell arrangements characterized by accumulation of misorientations across significant distances. The stored energy within DRX grains appears to be principally consistent with the corresponding Taylor factor values. The changes observed within the fully dynamically recrystallized microstructure during post-dynamic annealing have provided a basis to suggest a novel mechanism of metadynamic softening for the current experimental conditions. It is proposed that the initial softening stage involves rapid growth of the dynamically formed nuclei and migration of the mobile boundaries. The sub-boundaries within DRX grains progressively disintegrate through dislocation climb and dislocation annihilation, which ultimately leads to the formation of dislocation-free grains, and the grain boundary migration gradually becomes slower. As a result, the DRX texture largely remains preserved throughout the annealing process.

Abstract: The current work investigates the microstructure evolution and softening processes that take place during annealing of an austenitic Ni-30Fe model alloy subjected to hot deformation in the dynamic recrystallization (DRX) regime. The substructure of the deformed matrix grains largely comprised organized microband arrays, though that of the DRX grains consisted of more random, complex subgrain/cell arrangements. This substructure disparity was also reflected by the distinct difference in the mechanism of post-deformation softening taking place during annealing of the deformed matrix and DRX grains. In the former, the recrystallization process took place through nucleation and growth of new grains fully replacing the deformed structure, as expected for the classical static recrystallization (SRX). The corresponding texture was essentially random, in contrast to that of the DRX grains dominated by low Taylor factor components. The microbands originally present within the deformed matrix grains displayed some tendency to disintegrate during annealing, nonetheless, they remained largely preserved even at prolonged holding times. During annealing of the fully DRX microstructure, a novel softening mechanism was revealed. The initial post-dynamic softening stage involved rapid growth of the dynamically formed nuclei and migration of the mobile boundaries in correspondence with the well-established metadynamic recrystallization (MDRX) mechanism. However, in contrast to the deformed matrix, SRX was not observed and the sub-boundaries within DRX grains rapidly disintegrated through dislocation climb and dislocation annihilation, which led to the formation of dislocation-free grains already at short holding times. Consequently, the DRX texture initially became slightly weakened and then remained largely preserved throughout the annealing process.

Abstract: The texture and substructure development during post-dynamic annealing of an austenitic Ni-30%Fe model alloy after complete dynamic recrystallization was investigated using electron back-scattered diffraction (EBSD) and transmission electron microscopy (TEM). A novel mechanism of metadynamic softening is proposed based on the experimental investigation of the grain structure, crystallographic texture and dislocation substructure evolution. The initial softening stage involved rapid growth of the dynamically formed nuclei and migration of the mobile boundaries. The subboundaries within DRX grains progressively disintegrated through dislocation climb and dislocation annihilation, which ultimately led to the formation of dislocation-free grains, while the grain boundary migration gradually became slower. As a result, the DRX texture was largely preserved throughout the annealing process.

Abstract: During hot working of the recently developed nickel based alloy Allvac 718PlusTM softening kinetics like dynamic, metadynamic as well as static recrystallization govern the microstructure evolution during and after hot forming and hence the final mechanical properties. In this work the metadynamic recrystallization was investigated using double hit compression tests. The classical methodology of offset stress comparison was not usable because of discontinuous yielding of this material. Thus a new method to describe the softening during metadynamic recrystallization was developed, which compares the deformation energy at equal strains, i.e. the area beneath the true strain vs. true stress curve, of the first and second hit as well as at steady state.

Abstract: The kinetics of interpass softening and the strain (ε*) at which they become strain-independent were determined by means of double-hit hot compression tests. For this purpose, interrupted compression tests were conducted at strain rates of 0.01 and 0.1 s-1 to initial strains ranging from that corresponding to the initiation of DRX (εc) to the onset of steady state flow (εs.). Test temperatures between 1000 and 1100 °C (inclusive) were employed. Interpass times were varied from 0.3 to 1000 seconds. The fractional softening was determined using the 0.2% offset method. It is clear from the results that there is a transition strain (ε*) that separates the straindependent range of post-dynamic softening from the strain-independent range. The value of ε* obtained in this work was ε* = 4/3 εp. It was also found that the strain hardening rate was identical at all the critical strains (ε*) and took the value -22 MPa.

Abstract: In Alloy 718 ingot cogging process, dynamic and metadynamic recrystallizations, and static grain growth occur, and also the presence of δ phase plays a key role in controlling the grain size. In this study, the evolution of grain structure in VIM/VAR-processed Alloy 718 ingots during post-cogging heat treatments is dealt with. Compression tests were made on VIM/VAR-processed Alloy 718 ingot at temperatures between 900oC ~ 1150oC. Heat treatments were made on the compression-tested specimens, and the variation of grain size was evaluated. Constitutive equations for the grain growth are established to represent the evolution of microstructures. Special attention is paid to the evolution of grain structure under the condition of dynamic and metadynamic recrystallizations, and grain growth. The grain growth rate depends mainly on the presence of δ-phase below the δ-solvus temperature, and on the difference in the grain boundary characteristics above it.

Abstract: Experiments were carried out in which the dependence of the fractional softening on temperature, time and strain rate was determined in a 304H stainless steel. Three prestrain ranges were identified pertaining to three different post-deformation softening behaviors: 1) prestraining to below the DRX critical strain: strongly strain dependent softening by SRX alone with softening kinetics controlled by growth rate of the nuclei; 2) prestraining to above the DRX critical strain: SRX + MDRX softening with weaker strain dependence of the kinetics but still controlled by grain growth; 3) at a prestrain of ε* and beyond: nucleation-controlled MDRX softening with the full inhibition of SRX. The transition prestrain ε* can exceed the peak strain if the DRX grain refinement ratio g = D0/DDRX > 4. The transition to MDRX-dominated softening can be attributed to a constant value of the normalized strain hardening rate independent of the preloading temperature and strain rate. The softening data from the compression tests show that at ε*, the time for half softening t50 exhibits a minimum. These data differ somewhat from observations obtained in the torsion testing of solid bars, in which no strain dependence of t50 was detected at ε* and beyond. Whether or not the strain dependence of t50 vanishes in the MDRX range is sensitive to the test method employed to study the post-deformation softening.

Abstract: We have investigated the static and metadynamic behaviour of the interstitial free steels and in particular the effects of the steeling elements (phosphorous and boron) on kinetics of recrystallisation. The results showed that the strain for the initiation of strain independent softening (often referred to as metadynamic recrystallisation) varies with the Zener-Hollomon parameter and steel composition. Strain rate had a strong influence on kinetics of metadynamic recrystallisation. An increase in temperature from 930oC to 1100oC led to a decrease in time for 50% softening (about one order of magnitude) in the SRX region. However, for the same temperature range, the time for 50% MDRX did not change significantly.

Abstract: The stress relaxation method has been applied to the nickel-based alloy 80A to predict meta-dynamic (MDRX) and static recrystallization (SRX) kinetics. Compression tests were performed on a Gleeble 3800 system atr different temperatures (950-1200°C). The strain rate was varied in the case of MDRX and the pre-strain in the case of SRX. To investigate MDRX, the prestrain was set to twice the peak strain in order to reach steady state before holding. To focus on the interaction of MDRX and SRX, the pre-strain was set to the peak strain, where dynamic recrystallization (DRX) starts but does not yet reach steady state. Avrami type equations for the prediction of both the MDRX and SRX were adapted to feed a semi-empirical grain structure model.