Authors: Rajabi Javad, Norhamidi Muhamad, Abu Bakar Sulong, Aziz Hasyimah, Abdolali Fayyaz, Hafizawati Zakaria
Abstract: Micro metal injection molding has become the promising method in powder metallurgy research in order to fabricate small-scale intricate parts in an influential process and competitive cost of mass production. Stainless steel 316 L powders with powder size of 150 nm and 5 μm were mixed with a binder with a water soluble component which consisted of a major fraction of water soluble Polyethylene Glycol (PEG), a minor fraction of polymethyl-methacrylate (PMMA) and some stearic acid has been used as a surfactant. This work aims to investigate the rheological properties of a feedstock which are efficiently characterised by capillary Rheometry to measure apparent viscosities at different temperatures and shear rates. Results obtained by the varying feedstock characteristics, when viscosity decreases by increasing of shear rate at certain temperature feedstock should have a pseudoplastic behaviour. Melt viscosity of the feedstock was decreased by adding nanoscale powders. The reduced (n) values at high temperature with addition of nanoparticles indicated a possible increase in the shear-thinning behavior.
174
Authors: Rajabi Javad, Norhamidi Muhamad, Abu Bakar Sulong, Aziz Hasyimah, Abdolali Fayyaz, Hafizawati Zakaria
Abstract: Micro metal injection molding has become the promising method in powder metallurgy research in order to fabricate small-scale intricate parts in an influential process and competitive cost of mass production. Stainless steel 316 L powders with powder size of 150 nm and 5 μm were mixed with a binder with a water soluble component which consisted of a major fraction of water soluble Polyethylene Glycol (PEG), a minor fraction of polymethyl-methacrylate (PMMA) and some stearic acid has been used as a surfactant. This work aims to investigate the rheological properties of a feedstock which are efficiently characterised by capillary Rheometry to measure apparent viscosities at different temperatures and shear rates. Results obtained by the varying feedstock characteristics, when viscosity decreases by increasing of shear rate at certain temperature feedstock should have a pseudoplastic behaviour. Melt viscosity of the feedstock was decreased by adding nanoscale powders. The reduced (n) values at high temperature with addition of nanoparticles indicated a possible increase in the shear-thinning behavior.
36
Authors: Mohd Halim Irwan Ibrahim, Norhamidi Muhamad, A.B. Sulong
Abstract: Due to its versatility, micro metal injection molding has become an alternative method in powder metallurgy where it can produce small part with a minimal number of waste. The success of micro MIM is greatly influenced by feedstock characteristics. This paper investigated the characterization and optimization which both of them plays an important characteristic in determining the successful of micro MIM. In this paper, stainless steel SS 316L was used with composite binder, which consists of PEG (Polyethelena Glycol), PMMA (Polymethyl Methacrilate) and SA (Stearic Acid). The rheology properties are investigated using Shimadzu Flowtester CFT-500D capillary rheometer. The geometry of water atomised stainless steel powder are irregular shape, therefore it is expected significant changes in the rheological results that can influence the microcomponent, surface quality, shape retention and resolution capabilities. From rheological characteristics, feedstock with 61.5% shows a significant value with several injection parameters were optimized through screening experiment such as injection pressure (A), injection temperature (B), mold temperature (C), injection time (D) and holding time (E). Besides that, interaction effects between injection pressure, injection temperature and mold temperature were also considered to optimize in the Taguchis orthogonal array. Result shows that 61.5%vol contributes a significant stability over a range of temperature and the best powder loading from a critical powder volume percentage (CPVP) and rheological point of view. Furthermore interaction between injection temperature and mold temperature (BxC) give highest significant factor followed by interaction between injection pressure and mold temperature (AxC).
992
Authors: Lin Liu, Ngiap Hiang Loh, Bee Yen Tay
Abstract: Constitutive model is useful to predict the final shape of sintered microsize structures. In this paper, the contribution of lattice diffusion (Nabarro-Herring creep) is considered and a constitutive model is established to simulate densification of 316L stainless steel microsize structures fabricated by micro metal injection molding. The predictive capability of the model is verified by comparing the theoretical calculations with the experimental results. The influences of boundary energy on modeling results are discussed. It is found that the modeling results agree reasonably well with the experimental results.
846
Authors: Mohd Halim Irwan Ibrahim, Norhamidi Muhamad, Abu Bakar Sulong, Khairur Rijal Jamaludin, Nor Hafiez Mohamad Nor, Sufizar Ahmad
Abstract: Micro metal injection molding which is a new develop technology has attract most researcher where it becomes among the promising method in powder metallurgy research to produce small-scale intricate part at an effective process and competitive cost for mass production. Due to highly stringent characteristics of micro MIM feedstock,the study has been emphasized in investigating the optimization of highest green strength which plays an important characteristic in determining the successful of micro MIM. Stainless steel SS 316L with D50 = 5.96μm was used with composite binder, which consists of PEG, PMMA and Stearic Acid. From rheological characteristic and highly significant parameter through screening experiment, feedstock with 61.5% with several injection parameters were optimized such as injection pressure(A), injection temperature(B), mold temperature(C), injection time(D) and holding time(E). Besides that, interaction effects between injection pressure, injection temperature and mold temperature were also considered to optimize in the Taguchi’s orthogonal array. Analysis of variance (ANOVA) in terms of signal-to-noise ratio (S/N-larger is better) for green strength was also presented in this paper. Result shows that interaction between injection temperature and mold temperature(BxC) give highest significant factor followed by interaction between injection pressure and injection temperature(AxB). Single factor that also contributes to significant optimization are mold temperature(C), injection time(D) and injection pressure(A). This study shows that Taguchi method would be among the best method to solve the problem with minimum number of trials.
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Authors: Mohd Halim Irwan Ibrahim, Norhamidi Muhamad, Abu Bakar Sulong
Abstract: This paper investigates the performance of feedstock characteristics for micro metal injection molding (μMIM) by using optimum power loading variation and rheological characterization. The study has been emphasized on the powder and binder system in which stainless steel SS316L powder are mixed with composite binder, which consists of PEG (Polyethelena Glycol), PMMA (Polymethyl Methacrilate) and SA (Stearic Acid) by variation of powder loading concentration. The rheology properties are investigated using Shimadzu Flowtester CFT-500D capillary rheometer. As the geometry of water atomised stainless steel powder are irregular shape, therefore it is expected significant changes in the rheological results that can influence the microcomponent, surface quality, shape retention and resolution capabilities. The optimization of the μMIM rheological properties as a function of stainless steel powder loading concentration are evaluated by flow behavior exponent, activation energy and moldability index. From the results, it shows that 61.5%vol contributes a significant stability over a range of temperature and the best powder loading from a critical powder volume percentage (CPVP) and rheological point of view.
129
Authors: Mohd Halim Irwan Ibrahim, Norhamidi Muhamad, Abu Bakar Sulong, Khairur Rijal Jamaludin, Nor Hafiez Mohamad Nor, Sufizar Ahmad, Mohd Ruzi Harun, Hafizawati Zakaria
Abstract: Nowadays, micro metal injection molding has become among the promising method in powder metallurgy research to produce small-scale intricate part at an effective process and competitive cost for mass production. This paper investigated the optimization of highest green strength which plays an important characteristic in determining the successful of micro MIM. In this paper, stainless steel SS 316L with D50 = 5.96µm was used with composite binder, which consists of PEG (Polyethelena Glycol), PMMA (Polymethyl Methacrilate) and SA (Stearic Acid). Feedstock with 61.5% with several injection parameters were optimized which highly significant through screening experiment such as injection pressure(A), injection temperature(B), mold temperature(C), injection time(D) and holding time(E). Besides that, interaction effects between injection pressure, injection temperature and mold temperature were also considered to optimize in the Taguchi’s orthogonal array. Analysis of variance (ANOVA) in terms of signal-to-noise ratio (S/N-larger is better) for green density was also presented in this paper. Result shows that interaction between injection temperature and mold temperature(BxC) give highest significant factor followed by interaction between injection pressure and mold temperature(AxC). Single factor that also contributes to significant optimization are mold temperature(C) and injection time(D). This study shows that Taguchi method would be among the best method to solve the problem with minimum number of trials.
705
Authors: Hideshi Miura, Shigeo Tanaka, Toshiko Osada, Makoto Uemura
Abstract: In this study, gas nitriding was processed for various sizes of Ti specimens which were
produced by metal injection molding (MIM) process, for the sake of enabling the high functionality at
low processing cost. It was shown by the nitriding treatment that the hardness of the surface increased
extremely and the microstructure changed to the TiN and acicular α-Ti phase. With respect to the
effect of the nitriding on the size of parts, micro dumbbell specimen had around five times higher
content of nitrogen than the block ones. It was suggested that the size of μ-MIM products is so small
that the surface treatment can contribute significantly to improve the properties, and then gas nitriding
process may be one of effective surface treatment methods for high functionality of μ-MIM Ti
products.
3667
Authors: Kazuaki Nishiyabu, Kenichi Kakishita, Shigeo Tanaka
Abstract: This study aims to investigate the effects of hybrid micro/nano powders in a micro metal
injection molding (μ-MIM) process. A novel type of mixing-injection molding machine was used to
produce tiny specimens (<1mm in size) with high trial efficiency using a small amount of feedstock
(<0.05cm3 in volume). Small dumbbell specimens were produced using various feedstocks prepared
by changing binder content and fraction of nano-scale Cu powder (130nm in particle size). The
effects of adding the fraction of nano-scale Cu powder on the melt viscosity of the feedstock,
microstructure, density and tensile strength of sintered parts were discussed.
381
Authors: Kazuaki Nishiyabu, Yasuhiro Kanoko, Shigeo Tanaka
Abstract: The production method of micro sacrificial plastic mold insert metal injection molding,
namely μ-SPiMIM process has been proposed to solve specific problems involving the
miniaturization of MIM. The sacrificial plastic mold (SP-mold) with fine structures was prepared by
injection-molding polymethylmethacrylate (PMMA) into Ni-electroform, which is a typical LIGA
(Lithographie-Galvanoformung-Abformung) process. Stainless steel 316L feedstock was injectionmolded
into the SP-mold which had micro structures with multi-pillars. The green compact was
demolded as one component with the SP-mold, which was decomposed along with binder
constituent of feedstock in debinding process. This study focused on the effects of metal particle
size and processing conditions on the shrinkage, transcription and surface roughness of sintered
parts, which were evaluated by SEM (Scanning Electron Microscope) observation.
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