Authors: Dorothée Dorner, Yoshitaka Adachi, Kaneaki Tsuzaki
Abstract: Compression tests were performed on Fe-3%Si specimens with few grains. The deformation
microstructure and microtexture were investigated by electron backscatter diffraction (EBSD)
and related to the initial crystal orientation and grain boundary characteristics. Groups of microbands
were found that are characterised by a periodic change in crystal orientation, shear at the
grain boundary, and the formation of new grains. It is supposed that these microband groups represent
an early stage of microshear band development.
873
Authors: Bradley P. Wynne, O. Hernandez-Silva, M. Lopez-Pedrosa, W. Mark Rainforth
Abstract: The effects of strain path reversal, using forward and reverse torsion, on the
microstructure evolution in the aluminium alloy AA5052 have been studied using high resolution
electron backscatter diffraction. Deformation was carried using two equal steps of forward/forward
or forward/reverse torsion at a temperature of 300°C and strain rate of 1s-1 to a total equivalent
tensile strain of 0.5. Sections of the as-deformed gauge lengths of both test specimens were then
annealed at 400°C for 1 hour in a salt bath in order to investigate their subsequent recrystallisation
response. In both strain path histories the deformation substructure in the grains analysed consisted
of microband arrays within an equiaxed dislocation cell structure. The material subjected to
forward/forward deformation did, however, have a slightly greater number of low angle boundaries,
i.e. boundaries < 15° misorientation, whilst the forward/reverse material had some grains containing
little evidence of substructure. On annealing both materials had significantly reduced levels of low
angle boundaries but only the forward/forward material had an increased number of high angle
boundaries and a reduced grain size, indicating recrystallisation had only occurred in this material.
This would suggest that the deformation microstructure within the forward/forward condition was
sufficient to initiate and maintain recrystallisation whilst the microstructure produced by the
forward/reverse test contained insufficient nuclei or internal energy to produce a recrystallised
material within 1 hour. Further work is now required at different annealing times in order to
determine if the major effect of strain path is on retarding nucleation, growth or both.
407
Authors: W. Bevis Hutchinson
Abstract: The paper surveys various types of dislocation substructure that are created by plastic
deformation in metals. Special reference is made to those substructures that accommodate sharp
misorientations as these are of fundamental importance to the nucleation of recrystallisation.
Several different mechanisms can give rise to high misorientations; these are discussed in terms of
the factors that control them and their relationships to orientation and texture. Different
mechanisms for nucleation of recrystallisation may occur depending on the type of substructure,
allowing some practical control over the final recrystallised texture.
13
Authors: Dorothée Dorner, Yoshitaka Adachi, Kaneaki Tsuzaki, Stefan Zaefferer
Abstract: A Goss-oriented single crystal was cold rolled up to 89 % thickness reduction, and
subsequently annealed at 550°C or 850°C. During deformation most of the initially Goss-oriented
material rotated into the two symmetrical {111}<112> orientations. In addition, Goss regions were
observed related to microbands or microshear bands. Goss regions in microshear bands formed
during straining, whereas Goss regions between microbands were retained from the initial Goss
orientation. The recrystallisation texture for annealing temperatures of both 550°C and 850°C is
characterised by a Goss texture. However, the origin of the Goss recrystallisation nuclei appeared to
be different for the different annealing conditions. In the material annealed at 550°C, the Goss
texture originated from the Goss regions in the microshear bands. In contrast, for an annealing
temperature of 850°C, the Goss grains between the microbands are likely to form recrystallisation
nuclei.
485
Authors: M. Lopez-Pedrosa, Bradley P. Wynne, W. Mark Rainforth
Abstract: The effects of strain path reversal on the microstructure in AA5052 have been studied
using high resolution EBSD. Deformation was carried out using two equal steps of forward/forward
(F/F) or forward/reverse (F/R) torsion at a temperature of 300°C and strain rate of 1s-1 to a total
strain of 0.5. In both cases the deformation microstructure in the majority of grains analysed
consisted of microband arrays clustering at specific angles to the macroscopic deformation axes. For
the F/F condition microbands clustered around -20° and +45° to the maximum principle stress
direction, whilst for the F/R condition significantly more spread in microband angle was observed.
This suggests that the microbands formed in the forward deformation have or are dissolving and any
new microbands formed are related to the deformation conditions of the final strain path. This leads
to the conclusion that instantaneous deformation mode determines the orientation of new
microbands formed whilst a non-linear strain path history influences the range of misorientation
angle in the material through the dissociation of previously formed microbands and the formation of
new microbands at the new straining condition, leading to a lower level of misorientation angle.
Analysis of material subjected to static annealing at 400°C for 1 hour appears to correspond with
these observations as the F/F material was completely recrystallised with a fine grain structure
whilst the F/R material had no major signs of recrystallisation.
223
Authors: Aurelie Wauthier, Hélène Réglé, Rénald Brenner
Abstract: The aim of this study is to acquire more quantitative data on the cold-deformed state, in
order to determine the key parameters for nucleation (like orientation gradient, dislocation density,
degree of fragmentation…) and to correlate these to parameters which can be predicted by a mean
field deformation model.
Experimentally, a Ti-IF hot band has been deformed by cold rolling up to 51%. The deformed
microstructures are finely characterised using EBSD inside the SEM. It appears then that the
heterogeneity of deformation inside the grains begins very early. Some grains undergo
fragmentation whereas some others deform very homogeneously. Misorientation and degree of
fragmentation are found to be orientation and rolling level dependent. These deformation
parameters are plotted against the Taylor factor, calculated in each grain.
205
Authors: Hui Gao, Xin Ming Zhang, Hui Zhong Li, Ying Liu
Abstract: 2519A aluminum plate was shot obliquely by an incendiary projectile with the diameter of
7.62mm at impact velocity of 818m/s. The penetration inhomogeneities of the crater of 2519A
aluminum target plate were investigated with optical microscopy (OM), scanning electron
microscopy (SEM). Melted substance, a mixture of the target material and the projectile was found at
the interface of target and projectile. Different microstructural characteristics were observed along
the crater depth. Grains were elongated near the entrance area, while severely kinked grains and
adiabatic shear bands were present in the middle region, and microbands, as well as abnormal grown
grains, appeared at the crater bottom. The failure form of target is mainly ductile expanding.
1049
Authors: Dorothée Dorner, Ludger Lahn, Stefan Zaefferer
Abstract: A silicon steel single crystal with initial Goss orientation, i.e. the {110}<001>
orientation, was cold rolled up to 89 % thickness reduction. Most of the crystal volume rotates into the two symmetrical equivalent {111}<112> orientations. However, a weak Goss component is still present after high strain, although the Goss orientation is mechanically instable under plane strain loading. Two types of Goss-oriented crystal volumes are found in the highly deformed material. We suggest that their origin is different. The Goss-oriented regions that are observed within shear bands form during the cold rolling process. In contrast, those Goss-oriented crystal volumes that are found inside of microbands survive the cold rolling.
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