Papers by Keyword: Misorientation

Abstract: During the early stages of the plastic deformation of a polycrystal, dislocations can pile-up against grain boundaries. Experimental results on large-grained materials have provided excellent verification of this phenomenon. Such a pile-up may activate dislocation slip in the neighbouring grain. Whether this occurs depends on the misorientation between the grains and the resolved shear stresses in the affected grain. Several approximate criteria have been proposed to predict the occurrence of this mechanism. Here, the problem will be assessed directly by calculating the Peach-Köhler force produced by a single dislocation pile-up in one grain on all the possible slip systems in the neighbouring grain, in combination with the effect of the applied external stress as obtained through calculation of the Schmid factor. It will be seen that the problem is significantly more complex than what is generally assumed in basic explanations of the Hall-Petch effect: highly localised stress concentrations are generated for certain misorientations, which are capable of punching out small dislocation loops which may then propagate into the neighbouring grain.

Abstract: From the lattice orientation of a sample, elements of the Nye-tensor can be determined. With the help of Nye’s tensor, dislocation density can be calculated for the certain sample. Since the measures were carried out with scanning electronmicroscope (SEM), just superficial orientations can be measured. Hence the Nye-tensor is an incomplete matrix, with five elements. Because of the absence of the other four elements just a quasi-dislocation density can be obtained. The algorithm of the calculation was programmed on the language C#.

Abstract: Low carbon bainitic steels are important in applications such as linepipe, and the details of the bainite microstructure control strength and toughness. The transformation of austenite to bainitic ferrite has been widely researched over the years, although recent use of electron backscatter diffraction techniques has provided opportunity to advance the characterization of various crystallographic aspects. In recent work, microstructures were characterized in a base steel containing 0.04 C and 1.7 Mn (wt. pct.) and two additional steels having modest carbon and manganese variations to influence the transformation behavior, with an interest in the MA (martensite-austenite) constituent and characteristics of the bainite developed at different transformation temperatures. Effects of austenite conditioning were also examined, as these steels contained an addition of 0.04 wt. pct. Nb. Microstructural details including crystallographic characteristics assessed using EBSD are presented, along with comments related to the implications of the results.

Abstract: Orientation changes during fatigue crack initiation in ferrite and ferritepearlite steel were evaluated by electron backscatter diffraction (EBSD). Ferrite steel with different grain sizes and ferritepearlite steel with different carbon contents were prepared. EBSD measurements and fatigue tests were alternately performed using a small specimen. The tests on both ferrite and ferritepearlite steel suggest that the initial cracks were observed in the ferrite matrix. Thus, crystal rotation induced by fatigue in ferrite matrix is quantitatively evaluated by two misorientation parameters: grain reference orientation deviation, which is the misorientation between measuring points and the average orientation in each grain, and crystal misorientation at the same point before and after fatigue testing.

Abstract: The microstructure of X80 pipeline steel in different directions were observed by SEM technique and its effective grain size and misorientation were statistically analyzed by EBSD system. Based on these results, the mechanical properties at 0°, 45° and 90° to the rolling direction of X80 pipeline steel were studied. The results show that, owing to finer grain size and less low-angle grain boundaries, strengths and impact toughness of X80 pipeline steel at 90° direction are optimal. While the pipeline steel possesses finer grain size, more high-angle grain boundaries and less low-angle grain boundaries, the crack propagation is effectively suppressed, then its impact toughness is improved.

Abstract: The Rotating Extrusion Alloying (REA) is a process which combined friction stir welding process and extrusion technology. In the REA process, dissimilar metals are mixed, cracked, and subjected to high speed, severe pressing deformation, and therefore rapidly alloy at a low temperature. The Al-Ti alloy has been prepared by REA. The result shows that during REA process, the original materials and the products after synthesis present high energy ball mill and from sintering the compound are avoided, and the contamination to the compound due to the contact with the surrounding atmosphere and high energy balls disappear. REA technology can be alloyed Al-Ti material. Its phases are mainly composed of Al and Al3Ti, which are distributed more evenly in the aluminum. After heat treatment, its phases’ types and pole figures have no significant change, but there is a trend of transition to the non-equilibrium stable phase. Small-angle grain boundaries decrease or even disappear.

Abstract: Superplastic-like forming takes advantages of both deep drawing and bulge forming. The use of non-superplastic grade materials enables it to be more compatible with existing forming process with less material and time cost. Here, a non-isothermal heating system was adopted to selectively heat up selected localized areas to form the workpiece more efficiently. Electron backscattered diffraction (EBSD) was then used to investigate the wide range of grains in the formed samples resulting from elevated-temperature and large-strain deformation. The crystallographic textures of the material before and after deformation were observed for comparison. Very little recrystallization was found in the midst of the deformed grains. Considerable amount of elongated grains with high angle boundaries were produced during deformation. Many subgrain boundaries have developed within the big grains due to dynamic recovery.

Abstract: The c- and a-lattice constants of nitrogen-doped 4H-SiC were measured in the wide temperature range (RT - 1100°C). The samples used in this study were heavily doped substrates and lightly-doped free-standing epilayers. The lattice constants at room temperature are almost identical for all the samples. However, the lattice contraction by heavy nitrogen doping was clearly observed at high temperatures, which indicates that the thermal expansion coefficients are dependent on the nitrogen concentration. The lattice mismatch (Δd/d) between a lightly-doped free-standing epilayer (N_d = 6x10¹⁴ cm^-3) and a heavily-doped substrate (N_d = 2x10¹⁹ cm^-3) was calculated as 1.7x10^-4 at 1100°C. The authors also investigated lattice constants of high-dose N⁺, P⁺, and Al⁺-implanted 4H-SiC. Reciprocal space mapping (RSM) was utilized to investigate the lattice mismatch and misorientation. The RSM images show the c-lattice expansion and c-axis tilt of the ion-implanted layers, irrespective of ion species. The authors conclude that the lattice expansion is not caused by heavy doping itself, but by secondary defects formed after the ion-implantation and activation-annealing process.

Abstract: A local curvature multi-vertex model was developed. This model is the straightforward two-dimensional topological network model based on the physical principles which are the curvatures of grain boundaries and the grain boundary tensions at triple junctions. The model was applied to the artificial random microstructure under some conditions of grain boundary characters. The misorientation distribution was changed very little under constant grain boundary energy and mobility, but it was change much under grain boundary character dependent on misorientation. Therefore, in order to discuss actual textures, it is important to take grain boundary characters into account.

Abstract: Misorientation can be calculated over large datasets and a theme of this paper is the usefulness of examining the results statistically. Comparing the statistics of misorientations calculated from neighbouring pixels (or grains) with those calculated from pairs of pixels (or grains) selected at random helps to indicate deformation and recrystallisation mechanisms. Taking boundary length into account provides a link to grain boundary energy, and boundary length versus misorientation data should be used to examine how boundaries with different misorientations evolve through time. Time lapse misorientation maps indicate how orientation changes through time at particular points in a microstructure during in situ experiments. The size of areas which have changed orientation by particular amounts can be linked to boundary length and boundary migration velocities. When dealing with different phases, the statistics of angular relationships, akin to intraphase misorientation analysis, can indicate orientation relationships in the absence of prior knowledge, which is advantageous in investigating the plethora of minerals that make up the Earth.