Authors: Andreas Storz, Thomas Schubert, Thomas Weißgärber, Christoph Seyboldt, Kim Rouven Riedmüller
Abstract: The paper describes a cost effective and innovative combination of direct pressure sintering and subsequent thixoforming to produce MMC-components in (near-) net shape quality and, thus, to make these interesting materials attractive to mass production.First results of some combinations of aluminium matrix alloys with different ceramic reinforcements, consolidated by fast pressure sintering show the efficiency of this technology.The further processing of the consolidated billets has been performed by thixoforging. It can be shown, that the homogeneous microstructure from the direct pressure sintering stage with uniformly distributed ceramic reinforcements can be maintained over the semi-solid state and a full densification can be achieved. Form filling was complete and surface quality was comparable to forgings from conventional alloys.This new process flow shows advantages regarding the material yield in each of the processing steps. The (near-) net shape quality of thixoforged components allows a reduced effort for machining, which is of special importance for composite materials with a high content of wear resistant hard phases like SiC-particles.
167
Authors: Rui Peng Guo, Lei Xu, Jie Wu, Zheng Guan Lu, Rui Yang
Abstract: Shima model and two different kinds of container designs were described. The final geometries of powder metallurgy (PM) preforms were predicted by using finite element method. Several PM Ti-6Al-4V parts were fabricated through a hot isostatic pressing route for comparison with the prediction from the modelling. FEM simulation can be used for shrinkage prediction of powder during HIPing process. The finite element calculations agreed well with the experimental data for shrinkage of the titanium alloy powder under HIPing. The simulation results is helpful to fabricate near-net-shape PM titanium parts.
610
Authors: Lei Xu, Rui Peng Guo, Jia Feng Lei, Rui Yang
Abstract: Net shape process from pre-alloyed powder has become a viable approach to manufacture high-performance, complex shaped titanium alloy components. In this work densification of Ti-5Al-2.5Sn powder compacts in mild steel containers by means of hot isostatic pressing was studied. Due to the shielding effect of the container, inhomogeneous deformation of Ti-5Al-2.5Sn powder compacts was observed during the experiment and this was also predicted by a finite element analysis. The mechanical properties of powder metallurgy (PM) Ti-5Al-2.5Sn alloy of different density were compared. Near-net-shape forming processes of PM titanium alloy parts are studied. By using metal capsules and metal internal tooling, near-net-shaping of PM parts with complex shapes was demonstrated. The design of capsules and tooling was found very important because of the different shrinkage ratio of the differently shaped regions of the component.
278
Authors: V.A.R. Henriques, A.C.S.M. Dutra, C.A.A. Cairo
Abstract: During the recent years, alloys based on the intermetallic compound TiAl have attracted a considerable interest as potential competitors to steels and superalloys. Gamma-TiAl alloys are potential replacements for nickel and conventional titanium alloys in hot sections of turbine engines, as well as in orbital platform vehicles. The alloy design and efficient routes of TiAl processing are important technological challenges. Powder metallurgy is a near net shape process that allows the parts production with complex geometry at low costs. In this work, samples of Ti-48Al-2Cr-2Nb (at.%) were prepared from elemental and pre-alloyed powders mixed for 2 h, followed by cold uniaxial and isostatic pressing and sintered between 800 up to 1400°C, for 1 h, under vacuum. After metallographic preparation, sintered samples were characterized by SEM (Scanning Electron Microscopy), density analyses and Vickers microhardness measurements. The results indicated the viability of the pre-alloyed route and the tendency of a full lamellar microstructure of alternating gamma and α2 phases in high sintering temperatures.
44
Authors: Xian Liang Zhou, Ai Hua Zou, Xiao Zhen Hua, Duo Sheng Li, Zhi Guo Ye
Abstract: SiCp/Z101 composites substrate can be successfully fabricated by pressureless infiltration of ZL101 alloy liquid into porous SiCp preform, the relative density are nearly up to 99%. This is mainly because that generated SiO2 phase on the surface after sintering of SiCp not only has joint function to the porous of SiC perform, but also obtains two-phase wetting between SiC and Al matrix through the interface reaction, resulting in promoting spontaneous infiltration. SiC preforms have almost no change of shapes and sizes after infiltration of Al liquid and can achieve near-net-shape of the composites for substrate. Volume fraction of SiC can be effectively improved by using binary mixture particles with the diameter ratio of 11:1, through which the properties of substrate can be controlled effctively. By the addition of SiCp, strength of the composites is improved remarkably, and its elastic modulus increases correspondingly about one time, the increase of SiC volume fraction can markedly reduce coefficient of thermal expansion (CTE) of composites , but meanwhile decrease thermal conductivity(TC) of composites, and its TC (at 50 °C ranges from 120.7 W/(m•k) to 99.4 W/(m•k) and its mean linear CTE (25°C to 50°C ) ranges from 9.47×10−6 k-1 to 7.05×10−6 k-1 as volume fraction of SiC ranges from 38% to 68%.
4459
Authors: Vinicius André Rodrigues Henriques, Cosme Roberto Moreira Silva, Carlos Alberto Alves Cairo, Eduardo T. Galvani
Abstract: Powder metallurgy (P/M) of titanium alloys may lead to the obtainment of components having weak-to-absent textures, uniform grain structure and higher homogeneity compared with conventional wrought products. The production of the Ti-13Nb-13Zr alloy by P/M starting from blended elemental (BE) powders is a cost-effective route considering its versatility and also for allowing the manufacture of complex parts. This alloy due its high biocompatibility and lower modulus of elasticity is a promising candidate for implants fabrication. Samples were produced by mixing of initial metallic powders followed by uniaxial and cold isostatic pressing with subsequent densification by sintering in order to identify the microstructural evolution. Sintered samples were characterized for phase composition, microstructure, microhardness and density. The surface topography of the samples was studied by means of atomic force microscopy (AFM). It was shown that the route is adequate to reach high densities with homogeneous microstructure. Representative AFM images allowed distinguishing a lamellar structure caused by the different phases that are present in the surface of the specimens.
112
Authors: Yukinori Yamamoto, Jim O. Kiggans, Michael B. Clark, Stephen D. Nunn, Adrian S. Sabau, William H. Peter
Abstract: This paper summarizes our recent efforts to develop the manufacturing technologies of consolidated net-shape components by using new low-cost commercially pure titanium (CP-Ti) and Ti-6Al-4V alloy powders made by the Armstrong process. Fabrication processes of net shape/ near net shape components, such as uniaxial die-pressing, cold isostatic pressing (CIP), sintering, roll compaction and stamping, have been evaluated. The press-and-sinter processing of the powders were systematically investigated in terms of theoretical density and microstructure as a function of time, pressure, and temperature. Up to 96.4% theoretical density has been achieved with the press-and-sinter technology. Tensile properties of the consolidated samples exhibit good ductility as well as equivalent yield/ultimate tensile strengths to those of fully consolidate materials, even with the presence of a certain amount of porosity. A consolidation model is also under development to interpret the powder deformation during processing. Net shape components made of the Armstrong powder can successfully be fabricated with clearer surface details by using press-and-sinter processing.
103
Authors: Peng Yu, Ma Qian, Dacian Tomus, Craig A. Brice, Graham B. Schaffer, Barry C. Muddle
Abstract: Electron beam (EB) direct manufacturing is an additive near-net shape digital fabrication process developed recently. The process offers a promising route for the fabrication of intricate speciality aluminium alloy parts for aircraft and aerospace applications because of the excellent energy coupling between an electron beam and aluminium. As part of a fundamental study on EB manufacturing of Al alloys, this work investigates the effect of the EB processing parameters on the development of the molten pool and the solidification characteristics of Al 2219 and Al 6061 alloys. The samples were processed using a 50kV electron beam gun over a wide range of beam currents (10-40mA) and welding speeds (0.3-0.86m/min) in both the static and oscillation focus modes. In the static focus mode, the molten pool is wedge-shaped; while in the oscillation focus mode, the molten pool is hemispherical, wider and shallower. In both cases, the depth and width of the molten pool increase with increasing beam current but they are less affected by the moving speed of the EB gun in the range 0.3-0.86m/min. Electron beam re-melted and subsequently re-solidified Al 2219 and Al 6061 alloys show microstructural features distinct from those obtained under sand casting and direct chill casting conditions. In particular, fine intermetallic precipitates in the size range 100-200nm are prominent in the equiaxed grains formed in the re-solidified weld beads of Al 6061 compared to the coarse intermetallic particles up to 10m in size prior to EB processing. EB processing offers opportunities for aluminium alloy development.
621
Authors: M. J. Jeong, Chang Hwan Seo, Yeong Hwan Song, K.J. Kang, Bo Young Hur
Abstract: Fabrication of Aluminum foam with near net shape has been investigated by powder
metallurgy method and conventional pouring method. PM method is good for fabrication of near net
shape foam, but it needs high cost compared with pouring method. More cost-effective methods are
needed to make near net shape al foam to be applied various field. Therefore, novel method for
fabrication Al foam was researched in this paper. In order to prepare near shape Al foams with
homogeneous pore structures, the so-called upward foaming method was designed and applied. By
using this method, two kinds of molds were designed, one is stainless mold used for melting and
foaming Al and another is the plaster mold with near net shape. The fabrication procedures of near net
shape Al foam are as following: (1) a quantity of Al ingot was melted in the stainless mold; (2) Ca
particles was added in the Al melt to increase its viscosity; (3) TiH2 was introduced in the thickened
Al melt to make melt being foamed; (4) the plaster mold was put on the stainless steel one to make
enlarging Al melt foam fill with the plaster one; (4) the plaster mold was removed and was cooled.
In this study, in order to get near net Al foam with relative good pore structures, the plaster molds
were designed with three different upside styles and their effects on the pore structures (pore size,
porosity and cell wall thickness) of Al foams were investigated. The results showed that the Al foam
had the relative good pore structures when the plaster mold with a void was applied.
269
Authors: F. Wang, Kai Feng Zhang, Wen Bo Han
Abstract: Superplastic extrusion of axial forcing and radial flowing under different conditions was
adopted to form a turbo-rotor, using hot-press sintered compact of zirconia (3Y)-toughened alumina
composite that was prepared at 1450 °C for 1 hour with relative density of higher than 96%.
Subsequent superplastic extrusion was attempted at temperature of 1500 °C-1650 °C. The results
indicate that 3Y-ZrO2 plays an important role as a second-phase pinning agent and inhibits grain
growth. The material shows good deformability and potential of near-net-shape forming. Comparing
with undeformed sample, extruded sample was observed apparent coarsening in grain size and the
remaining mechanical properties after deformation are not improved, irrespective of improved
density. The dominating deformation mechanism is grain sliding and rotation accommodated with
zirconia coordinated deformation.
501