Papers by Keyword: Nickel Coating

Abstract: The present research aimed to evaluate the effect of nickel-based electrochemical metallization (EMNi) on the quality and performance of electric motor components, compared to high-velocity oxy-fuel (HVOF) thermal spray coating, the most widely used coating in the mining industry. The experiment was conducted using motor components comprised of 4340 VCN steel, 4140 VCL steel, 1045 steel, and stainless steel, which underwent both treatments. The surface temperature of the components was monitored during the processing stage, followed by evaluations of their Rockwell hardness (HRC) and surface characteristics (taper, ovality, parallelism, finish, wear) at the onset (day 0) and after 2 years of use the results indicate that EMNi delivers electric motor components with superior finishes and extended warranty and service life in comparison to HVOF.

Abstract: A carbon fibre (CF) in the form of a rod (continuous fibre) was used as reinforcement due to its superior strength and modulus properties. Carbon fibre rod reinforced aluminium 6061 alloy metal matrix composite material was synthesized using the stir casting liquid metallurgy route. Aluminium based metal matrix composite materials are light in weight. Very few researchers were worked on carbon fibre rod reinforced metal matrix composites (MMC). Electroless nickel deposition on carbon fibre rods (2mm and 3mm diameter) were carried out for improvement in wettability. On carbon fibre rods, the effectiveness of electroless nickel coating was validated using SEM (scanning electron microscopy) and EDAX (Energy Dispersive X-Ray Spectroscopy) analysis. A further coating thickness of nickel was improved using nickel electroplating. In a cast iron mould, nickel-coated carbon fibre rods were arranged in a circular pattern. Completely degassed molten aluminium 6061 alloy was poured in cast iron mould at 600-700 °C. The enhancement in Tribological and mechanical properties is always a prerequisite for technological advancement in automobile sector. From synthesized composites (11.11% Vol. CF and 25% Vol. CF reinforcement) specimen were prepared for density tests, bulk and microhardness tests, friction and wear tests. Synthesized composite has low density, increased bulk and microhardness, low coefficient of friction and reduced wear rate in comparison with aluminium 6061 alloy. Keywords: Carbon Fibre (CF) rod, MMC, Nickel coating, Casting, Mechanical, Tribological

Abstract: The time-transition curve of open circuit potential (Eoc) during the single zincating process of aluminium alloy 7075 (AA7075) was recorded. Then, a suitable single zincating duration was selected from the Eoc slope, in order to get the optimum zincating duration. The evolution of surface morphology and composition of AA7075 substrate at various single zincating durations were characterized by scanning electron microscopy (SEM) and energy dispersive analysis of x- rays (EDX). The coating adhesions of single zincated samples produced at various durations were investigated using a scratch tester. SEM results showed that the substrates produced at a longer zincating duration were fully covered by a dense layer of zinc particles. The adhesion of the electrodeposited nickel on single zincated samples produced at longer zincating duration was higher than the conventional single zincating process. This morphology has contributed to the improvement of coating adhesion.

Abstract: Diamond coating on tungsten carbide (WC-Co) cutting tools with cobalt binder experiences delaminating failure due to the deleterious effect of cobalt. One of the methods used to reduce this effect is by coating an interlayer onto the substrate surface prior to diamond deposition. Different materials have been used as an interlayer which is normally deposited to the substrate surface using CVD and PVD techniques. Among different materials used as interlayer on WC-Co, nickel is considered as an attractive candidate due its good chemical and physical properties. In this study the potential of the electroplating technique for deposition of nickel interlayer on WC-Co will be investigated. Nickel deposition on WC-6%Co substrate was carried out by electroplating in a standard watts solution at constant plating parameters (Current: 0.1 Amp, electric potential: 1.0 V and pH: 3.5). The gap between anode and cathode was varied (5mm, 10mm and 15mm). The nickel coating formed on the hard metal surface was characterized in terms of the coating thickness, layer uniformity and coating hardness by using SEM and the micro hardness tester. Based on the results, desirable nickel coating properties were obtained when the separation distance between anode and cathode was 15mm.

Abstract: The methods for wear resistance testing is described and the experimental results for the dependence of the massive wear, wear speed, intensity of wear and wear resistance on the friction road and the time of a contact interaction are obtained. A testing micromanipulator with piezo actuators for measuring the roughness of the surface layer is developed. A methodology for thermographic testing and experimental results for wear and temperature changes in the contact by the wear process of the coatings under dry friction and abrasion is obtained

Abstract: Ni coatings with different grain sizes and preferred orientations were produced by the control of current density during a direct current electrodepositing process. The effects of grain size reduction and preferred orientation on the oxidation behavior in air at 600°C and 960°C of Ni coatings were investigated respectively. An important and interesting result is that after oxidation at 600°C, the Ni coating obtained at lower current density has a better oxidation resistance, whereas after oxidation at 960°C, the Ni coating obtained at higher current density has a more compact scale and a better oxidation resistance. For the Ni coatings oxidation at 600°C, the oxidation behavior was mainly influenced by grain size, whereas in the case of the Ni coatings oxidation at 960°C, the oxidation behavior was only slightly influenced by grain size. The changes in oxidation behavior of Ni coatings at 960°C can be attributed to the different preferred orientation and the corresponding oxidation mechanism.

Abstract: In this study, the FeS2 fine compound powders for active material were made by mechanical alloying using the Spex mixer mill. As the total milling time increased to 15hrs, the size of FeS2 powder decreased to 0.98um. Meanwhile, the treatment of nickel coating for FeS2 powder were also prepared by mechanical alloying using the ball milling machine, which has attracted much attention from the standpoints of improving the cycle life property and good columbic efficiency.

Abstract: The diffusion couples for experimental study were prepared by HVOF spraying of nickel and nickel with 20 wt.% of chromium powders onto an aluminium sheet surface. The interfaces with sharp gradients of chemical concentration of these elements were prepared. Annealing at temperatures of 600°C and 630°C, close to the Al + Al3Ni eutectic melting point (639.9°C), with different dwell times were used. During annealing, the reactants diffuse and form layers of Al3Ni2 and Al3Ni intermediate phase compositions. Moreover, nickel without the assistance of chromium diffuses preferably along the grain boundaries into aluminium substrate and produces the strengthening of the substrate by stable Al3Ni and metastable Al9Ni2 particles. The microstructures were obtained by scanning electron microscopy. Layer thickness measurements were realized by means of image analyses. Chemical composition was estimated by energy dispersive microanalysis measurements. According to the results of the analyses performed the average chemical interdiffusion coefficients and Wagner’s integral interdiffusion coefficients were calculated.

Abstract: Nickel coated gadolinium doped ceria (GDC) powder was synthesized by microwave radiation and combustion. For the synthesis, the precipitates of gadolinium cerium oxycarbonate hydrate (GdxCe2-xO(CO3)2·H2O) were formed by a microwave radiated reaction between cerium nitrate (Ce(NO3)3.6H2O) and gadolinium nitrate (Gd(NO3)3.6H2O) and urea (CO(NH2)2), then nickel coatings on the gadolinium cerium oxycarbonate hydrate were performed by further microwave reaction between nickel chloride and urea. The shape and size of the gadolinium cerium oxycarbonate hydrate particles were critically dependent on aging time during microwave radiation. The irregular particles were transformed to rod shape particles with well-crystallized with increasing aging time to 40 min at 70 - 80°C because of the gradual decomposition of urea during microwave radiation. Small nickel precursor particles were homogeneously coated on the gadolinium cerium oxycarbonate hydrate particles with rod shape with aid of microwave radiation at 80 °C for 40 min. As a result, the nickel coated GDC nanopowders were sucessfully produced by the microwave radiation synthesis and further microwave combusted at 450°C for 20 min.

Abstract: We have applied hybridization method to the surface modification by Ni coating on powder specimens of pure Mg and Mg-Mg2Ni eutectic alloy, and investigated the effect of the Ni coating on the hydrogenation kinetics in them. The hydrogenation kinetics at 350 degree C is greatly increased by the Ni coating for both the pure Mg and Mg-Mg2Ni eutectic alloy specimens. Thus, it is confirmed that the surface modification by the hybridization method is considerably effective to improve the hydrogenation kinetics in them. This improvement is thought to be a catalytic effect of the coated Ni. The hydrogenation kinetics of the Mg-Mg2Ni alloy specimen heat-treated at 470 degree C has increased compared with that of the as-cast alloy specimen. It is also confirmed that hydrogenation kinetics improves by the heat treatment to grow the eutectic structure consisted of Mg2Ni phase and Mg phase.