Papers by Keyword: Recrystallization

Abstract: The deformation and recrystallization behavior of two magnesium alloys, AZ31 and WE43, have been investigated. The cast alloys were heat treated to produce various distributions of second phase particles and deformed in a channel die at a strain rate of 10-4 s-1 at temperatures between 523 and 673 K. The alloys were subsequently annealed at temperatures between 708 and 798 K.The AZ31 and WE43 were extruded at 555 and 633 K, respectively. The microstructures were compared to those developed during channel die deformation. The tensile and compressive strengths and the texture of the alloys were determined in the as-extruded and recrystallised conditions.Optical microscopy and electron backscattered diffraction (EBSD) were used to characterize the microstructures of the alloys. The EBSD technique was used to determine the texture of the deformed and annealed samples.

Abstract: The wet oxidation of (0001), Si-face, 6H-SiC pre-amorphised by Ar+ implantation has been investigated in the temperature range between 750 and 950 °C. Electron microscopy analysis has been performed to obtain information on the evolution of the amorphous layer during the oxidation process. When the oxidation occurs on the amorphous substrate the observed rate is given by VOx(a)=3.8x107exp(-1.6eV/kT) nm/min, by far faster than that observed on single or polycrystalline 6H-SiC. For amorphous layer thickness of a few hundreds nanometer and processing time of a few tens of minutes this happens up to oxidation temperatures of about 910 °C, owing to the concomitant recrystallization process. At higher temperature, our oxidation data support the existence of a sudden variation of the recrystallization process that rapidly reduces the residual amorphous region and, consequently, the oxide thickness. However, it appears that this second recrystallization stage is faster than previously estimated. Structural detail of the starting amorphous-crystalline interface and of the early-recrystallized layers are reported and discussed.

Abstract: The effect of hot deformation process on the structure within the temperature range corresponding to the g→a+P transformation was tested for commercial carbon steel containing of 0.158% C. Hot compression tests were performed at computer controlled constant cooling rate. Before testing CCT diagrams were carefully determined in order to fit hot deformation conditions to the g→a+P phase transformation range. The material microstructure was examined by means of optical and electron transmission microscopy. It was found that ferrite, pearlite or bainite were typical microstructural components observed at hot deformed samples. Localized distribution of pearlite or bainite that resulted from flow localization was observed rarely. Precipitation of carbides on ferrite grain boundaries is the most typical microstructural effect of the hot deformation/precipitation interaction that was noted for the most of hot deformed samples.

Abstract: One of the most challenging problems to develop polycrystalline silicon thin-film solar cells is the growth of crystalline silicon on foreign, low-cost and low-temperature substrates. In this paper, a laser doping technique was developed for the plasma-deposited amorphous silicon film. A process combination of recrystallization and dopant diffusion (phosphorous or boron) was achieved simultaneously by the laser annealing process. The doping precursor was synthesized by a sol-gel method and was spin-coated on the sample. After laser irradiation, the grain size of the doped polycrystalline silicon was examined to be about 0.5~1.0 µm. The concentrations of 2×1019 and 5× 1018 cm-3 with Hall mobilities of 92.6 and 37.5 cm²/V-s were achieved for the laser-diffused phosphorous- and boron-type polysilicon films, respectively.

Abstract: A recrystallized Co-Ni-Cr-Mo based superalloy was produced by cold working of 72% and subsequent recrystallization heat treatment. Microstructural observation revealed that a full recrystallization of the cold-worked alloy occured when heat treatment was performed at and above 1273K for 1h. So that, recrystallization heat treatment was carried out in a temperature range from 1273K to 1473K for 1h~24h, by which the average grain size was controlled to 28µm～238µm. Tensile tests were carried out from room temperature (RT) to 1073K in order to understand the effect of grain size on the mechanical properties of the Co-Ni-Cr-Mo based superalloy. At RT and 943K, yield strength, tensile strength and elongation of the recrystallized alloy were improved with decreasing grain size. The alloy having a grain size less than 42µm exhibited a steady-state flow behavior in the true stress-true strain curve at 943K. However, the alloy having a grain size of 28µm showed lower yield strength than that of 42µm at 1073K. It was found that the steady state flow is closely related to the occurrence of {111}<112> deformation twinning in the Co-Ni-Cr-Mo based superalloy.

Abstract: The evolution of annealing textures and microstructures in the aluminum alloy 3103, which was subjected to deformation by either cold rolling or equal channel angular rolling (ECAR), was investigated. Samples of AA 3103 sheets were repeatedly deformed by ECAR up to six passes. In addition, AA 3103 was cold rolled to the same hardness level of the ECARed samples. Upon annealing, the cold rolled sample was recrystallized by the discontinuous recrystallization which gave rise to the formation of the cube texture and large grains bigger than 30 µm. In contrast, the ECARed sample was recrystallized by extended recovery which led to the formation of ultra-fine grains having a size smaller than 3.5 µm.

Abstract: Texture evolutions are determined by XRD and EBSD techniques during ferrite refinement through deformation-enhanced ferrite transformation (DEFT) and dynamic recrystallization (DREX). Evidences of transformation texture, deformation texture and recrystallization texture during DEFT are provided and compared with the texture during DREX. The influence of pass-interval during DEFT on texture is illustrated. Results are discussed in terms of the influences of ferrite grain size and deforming temperature.

Abstract: The recrystallization behavior of high strength automobile steel sheets (ZJ590L) developed by CSP technology is studied in this paper. The effect of the deformation temperature, reduction on the austenite grain size and the recrystallized fraction of ZJ590L steel during hot deformation has been investigated. Technique of test and analysis includes preparing stepped test piece and quantitative metallograph. The mechanism of austenite microstructure refinement has been discussed, which provides valuable references to set parameters of controlled rolling and controlled cooling process. The analysis shows that the austenite grain size fines with the increase of deformation temperature and reduction, and the recrystallized fraction increases. When the deformation temperature is above 1000°C and reduction exceeds 40%, complete recrystallization can be obtained.