Papers by Keyword: Secondary Recrystallization

Abstract: A pure iron tape with cube orientation was fabricated by cold rolling and annealing. The orientation characteristics of the pure iron tape were evaluated using electron back-scattering diffraction (EBSD) analysis. The secondary recrystallized grains with cube orientation was formed on the tape surface for the pure iron tape. The coarse grains with a grain size of ca. 1mm were observed on the tape surface. The areal fraction of cube orientations with an angular deviation ≤ 20 ̊ amounts to ca. 81%.

Abstract: In this study the effects of heating rate on the sharpness and size of Goss oriented ({110}<001>) grains during secondary recrystallization annealing at 900 °C was observed. The results show that, at the same annealing temperature, rapid heating of the samples to this temperature generates a higher drag force compared to a slower heating rate (5°C/min). The two groups of samples show different growth kinetics for Goss grains, in which at the longest annealing time, the rapid heating sample exhibits larger maximum Goss grain size compared to the slower heated samples.

Abstract: In conventional production of grain-oriented electrical steel, the content of silicon is limited to 3.0%~3.4%, which could control the ‘γ→α’ transformation process to obtain fine grain sizes in hot-rolling and disperse AlN particles in normalizing. In this study, the precipitation behaviors of S ans N in 4.5% Si-Fe alloy are inhibited during twin-roll strip casting process. And then the ideal microstructure and texture was obtained after the two-stage cold rolling and primary annealing. The evolution of microstructure and texture during the subsequent high temperature annealing were investigated. The results revealed that a sharp and developed Goss texture has been achieved by secondary recrystallization in the final annealing step and the magnetic induction B8 /Bsis above 1.76/1.90T.

Abstract: During abnormal grain growth, a few Goss grains grow exclusively fast and consume the matrix grains. The Goss abnormally-growing grain (AGG) has peculiar features which are irregular grain boundaries and very high frequency of peninsular grains nearby the growth front of AGG and island grains trapped inside AGG. These features might provide a clue for clarifying the mechanism of Goss AGG. The experimentally-observed microstructural feature and grain boundary characterization of Goss were approached by the solid-state wetting mechanism. In this study, observing the three-dimensional wetting morphology in serial section images of Goss AGG by EBSD, we report some direct microstrucrual evidence supporting solid-state wetting mechanism for Goss AGG. The solid-state wetting mechanism for the evolution of the Goss AGG in Fe-3%Si steel explains the microstructural features evolved during secondary recrystallization, which cannot be approached by the conventional theories based on the grain boundary mobility.

Abstract: It has been observed that grain size of Goss secondary grain has a strong correlation with deviation angle from the exact Goss orientation and sharper Goss grain has larger grain diameter. This orientation selectivity of secondary recrystallization has been investigated with the statistical model of grain growth in which inhibitor and texture are taken into account. The model assumes that sharper Goss grain has a higher frequency of CSL boundaries to the matrix grains and thus has lower statistical grain boundary energy and suffers lower pinning force from the inhibitor. The analysis showed that this model successfully explains orientation selectivity and depicts the effect of inhibitor and texture.

Abstract: The effects of inter-pass ageing temperature during cold rolling on structure, magnetic properties and mechanical properties of high permeability grain oriented electrical steel was studied. The samples were processed in a single-stage cold rolling to 0.27 mm thickness, with 88 % reduction, without and with inter-pass ageing treatment in order to determine the magnetic properties. To determine the changes in mechanical properties due to strain ageing, the samples underwent overlapped ageing, after pre-strain by rolling, under the same conditions of inter-pass ageing and then were subjected to tensile test. The effect of strain ageing was more pronounced in the thickness of 0.7 mm and the largest variation in yield strength was at 200°C in all evaluated thicknesses. At this temperature the largest amount of {110} orientation after primary recrystallization was also observed, as well as the lowest final grain size and consequently the best results of core loss. The magnetic induction had almost no alterations.

Abstract: Primary recrystallised sheets of 3% silicon steel from two different industrial processing routes have been examined after laboratory annealing to initiate secondary recrystallisation. Metallography included etching to reveal individual dislocations and sub-boundaries as well as EBSD in scanning electron microscopy. Residual low angle boundaries are not normally observed inside the secondary grains. The growth of secondaries appears to occur in a jerky manner, associated with local intrusions into the primary matrix that destabilise the interface. The frequency of occurrence of special low energy grain boundaries such as 9 and 5 is believed to dictate the selectivity of the Goss orientation in both types of steel sheet.

Abstract: Grain growth processes in real polycrystalline materials are mostly characterized by the presence of restraining forces, originating, among others, from second phase particles dispersion (Zener drag) or solute atoms segregating at the grain boundaries (solute drag). Both the restraining mechanisms were introduced in the framework of the statistical theory of grain growth, showing their peculiar effects on kinetics and on grain size distribution evolution [1,2,. The present work moves from the previous results and gives a further clarification of pseudo-steady state kinetics occurring under particular solute drag inhibition intensity and will discuss it in comparison with grain growth stagnation conditions produced by Zener drag. In case of second phase particle inhibiting grain growth, the normal case in real systems is the time and temperature dependence of the inhibition intensity due to the evolution of precipitates (e.g. Ostwald ripening. Such evolutions of inhibition, which typically drops with increasing temperature, can cause microstructure instabilities like abnormal grain growth or secondary recrystallization. It is thus introduced in the model a time-temperature depending inhibition drop, which influences both kinetics and grain size distribution evolution. Conditions for the onset of particular effects like abnormal grain growth are assessed and discussed.

Abstract: The selective abnormal grain growth (AGG) of Goss grains in Fe-3%Si steel was investigated using a parallel Monte-Carlo (MC) simulation based on the new concept of sub-boundary enhanced solid-state wetting. Goss grains with low angle sub-boundaries will induce solid-state wetting against matrix grains with a moderate variation in grain boundary energy. Three-dimensional MC simulations of microstructure evolution with textures and grain boundary distributions matched to experimental data is using in this study.

Abstract: On the basis of Hillerts model of grain growth, a new model of Goss secondary recrystallization in silicon steel has been developed in which inhibitor and grain boundary energy are taken into account. An analysis shows that these two parameters synergistically affect secondary recrystallization and Goss grain evolves to a coarse grain as inhibitor intensity increases and statistical grain boundary energy decreases. This model successfully explains Goss secondary recrystallization.