Papers by Keyword: Slurry Method

Abstract: Metal foams are widely produced by using different techniques such as compaction and replication method. In this study, slurry method also known as replication method has been used to produce SS316L foams. SS316L powders (50wt% and 60wt%) were mixed with the binders and distilled water by using mechanical stirrer. Polyethylene Glycol (PEG) and Carboxyl Methyl Cellulose (CMC) were used as binders. Polyurethane (PU) foam was used as scaffold and dipped into SS316L slurry then dried in room temperature for 24 hours. Sintering process has been done in two different temperatures which were 1200°C and 1300°C in vacuum furnace. The morphological study was performed using Scanning Electron Microscopy (SEM) and Energy Dispersive X-Ray (EDX). The SEM micrograph showed that the cells were interconnected and the structures become denser as the sintering temperature increase. The average pores size is ranging from 252.8 μm-353.8 μm, while strut size ranging from 50.2 μm-79.9 μm based on SEM micrograph analysis. The elemental analysis from EDX showed the element presence in the SS316L foam remain from SS316L powder which are Chromium (Cr), Nickel (Ni), Molybdenum (Mo), Cooper (Cu), Nitrogen (N₂), Sulphur (S) and Silicon (Si). Higher sintering temperature contributes better grain growth between particles where the point-contact between the particles expanded and disappear the small pores.

Abstract: Nickel superalloy was coated by aluminide coatings by the slurry method. The slurry as active mixture containing aluminium and silicon powders, an activator and a binder. The coating were obtained by annealed in argon atmosphere. The structure of these coatings is two zonal and depends on time and temperature of producing. The phase composition was determined using following techniques: scanning electron microscopy (SEM) equipped with Xray microanalysis (EDS) combined with electron backscatter diffraction (EBSD) and Xray diffraction (XRD).

Abstract: The slurry aluminide coatings are produced on the three kind of substrates: hightemperature creep resistant cast steel, titanium alloy and nickel alloy. The slurry as active mixture containing aluminium and silicon powders, an activator and an inorganic binder. The coating were obtained by annealed in air atmosphere. The structure of these coatings is two zonal and depend on the type of substrate and technological parameters of producing.

Abstract: Metal foams are well-known as engineered materials with unique combination of physical and mechanical properties, yielding an attractive material for use in the aerospace industry, automotive and medical industry. In this study the method that been used to produce SS316L foam is slurry method. Slurry of stainless steel is prepared by mixing binder material such as methyl cellulose (CMC), polyethylene glycol (PEG) and distilled water by using ball milling machine. Then, the sample is sintered at different temperatures which are 1300°C, 1350°C and 1400°C. The value of porosity and density of SS316L foam are collected utilizing Archimedes method. As the result, the porosity percentage found in the range of 4.77 % to 59.80% meanwhile density value ranging from 0.402g/cm3 to 0.952g/cm3. The highest value of porosity is 59.80% at 1300°C for 40wt% SS316L, while, the highest value of density is 0.952g/cm³ at 1350°C for 60wt% SS316L. These results was followed the theory of porosity and density which are the value of porosity is inversely proportional to the density.

Abstract: Sintering is a key step in the preparation of metal foams. The present work focuses on the sintering effects on the properties of titanium foam prepared using the slurry technique. Sintering affects the density as well as the mechanical properties of the sintered parts. To achieve a high density of the titanium alloy foam, the effects of various parameters including temperature, time profile and composition have to be characterized and optimized. This paper reports the use of the Taguchi method in characterizing and optimizing the sintering process parameters of titanium alloys. The effect of four sintering factors: composition, sintering temperature, heating rate and soaking time to the density has been studied. The titanium slurry was prepared by mixing titanium alloy powder, polyethylene glycol (PEG), methylcellulose and water. Polyurethane (PU) foam was then impregnated into the slurry and dried at room temperature. This was later sintered in a high temperature vacuum furnace. The various factors were assigned to an L9 orthogonal array. From the Analysis of Variance (ANOVA), the sintering temperature was found to give the highest percentage of contribution (34.73) followed by the composition of the titanium alloy powder (26.41) and the heating rate (0.64). The optimum density for the sintered titanium alloy foam was 1.4873±0.918 gcm-1. Confirmatory experiments have produced results that lay within the 90% confidence interval.

Abstract: In this paper, titanium alloy was used to prepare titanium foam using the slurry method. The compressive strength is the most important properties to be considered to produce a good sample. To achieve a high compressive strength of the titanium alloy foam, the effects of various parameters including temperature, time profile and composition have to be characterised and optimised. This paper reports the use of the Taguchi method in optimising the processing parameters of pure titanium foams. The effects of four sintering factors, namely, composition, sintering temperature, heating rate and soaking time on the compressive strength has been studied. The titanium slurry was prepared by mixing titanium alloy powder, polyethylene glycol (PEG), methylcellulose and water. Polyurethane (PU) foams were then impregnated into the slurry and later dried at room temperature. These were next sintered in a high temperature vacuum furnace. The various factors were assigned to an L9 orthogonal array. From the Analysis of Variance (ANOVA), the composition of titanium has the highest percentage of contribution (64.64) to the compressive strength followed by the soaking time of sintering factor (6.01). The optimum compressive strength was found to be 38.03 MPa for this titanium alloy foam. It was achieved with a 750% composition of titanium, sintering temperature of 1250oC, a heating rate of 1.5oC/min and 120 minutes of soaking time.