Papers by Keyword: TRIP

Abstract: During the hot bulk forming of long parts, inhomogeneous distributions of deformations and temperatures occur. The gradients of these distributions lead to complex, overlaying residual stresses, which can cause critical geometric deviations and mechanical failures. Common finite element (FE)-simulations for designing a process are in principle capable to predict the thermal, mechanical and metallurgical effects, but require extended material models. Thereby, the total strain increment can be described through the partial strain components of the elastic, plastic, thermal transformation related and transformation plasticity strain. To allow the numerical prediction of the distortion of long hot formed parts, an experimental characterisation of the TRIP and backflow effects is presented for the steel 31CrMoV9. Time temperature transformation (TTT) and continuous cooling transformation (CCT) diagrams are determined with JMatPro and verified by means ofmicrostructure analysis and hardness measurements. Based on these diagrams, the transformation plasticity is investigated through dilatometric tests whereby tensile and compressive loads are applied during the phase transformation. The martensite phase transformation showed the highest amounts of TRIP strains, whilst the bainite transformation exhibited lower strains but a high tensile backflow strain. For perlite the beginning of the phase transformation was delayed and its duration extended due to the induced loads.

Abstract: At temperatures of 290 K and 77 K, the phase composition and mechanical properties ofnonequiatomic medium-entropy (MEA) alloys Fe40Mn40Co10Cr10 and Fe50Mn30Co10Cr10 werecompared in the coarse-grained (CG) and nanostructured (NS) states, in which additionaldeformation mechanisms are activated under load: phase transformations in the MEAFe50Mn30Co10Cr10 (MEA TRIP) and twinning in the MEA Fe40Mn40Co10Cr10 alloy (MEA TWIP). Itis shown that in the NS state in both alloys, in contrast to the CG state, a complete phase transitionfrom the fcc to the hcp phase is observed, the content of which weakly depends on the temperatureand the number of torsion revolutions during high-pressure torsion (HPT). The transition from theCG to the NS state leads to an increase in the microhardness (in the NS MEA TWIP by 3.7 and inthe NS MEA TRIP by 2.25). In the CG state, a thermally activated character of plastic deformationis observed for both alloys in the temperature range of 290 – 77 K. In the NS state, MEA TWIPremains plastic under active compression deformation at 290 K and 77 K, whereas in NS MEATRIP under similar conditions, macroscopic plasticity is absent. Tensile deformation up to 50 % at30 K in the CG state for both alloys leads to a significant decrease in the absolute values of Young'smodulus over the entire temperature range.

Abstract: To increase the safety of steels in high performance cases like crash energy absorption, even better properties of the materials are necessary. To advance this research, a TWIP and a TRIP steel were combined in a laminated composite via roll bonding at 450 °C with the goal of using accumulative roll bonding (ARB) in later research to further enhance the properties reaching an ultra-fine-grained material. Two different TWIP layer thicknesses (2 mm and 3 mm) were experimentally roll bonded with a 3 mm thick TRIP layer each using a 4-high rolling mill. A modular Python-based simulation incorporating coupled solving of ordinary differential equations of the temperatures and the horizontal stress changes of the layers were implemented to predict deformation and bonding behavior. Simulated results matched well with experimental data in terms of final geometry and temperature, while roll force deviations indicated the need for the refining of the used model. Furthermore, experimentally asymmetric layer relationships at the beginning and the addition of a thin (10 µm) Ni interlayer were found to enhance bond strength in high-strength steel laminates.

Abstract: The main objective of this work was to obtain information about the hydrogen diffusion behaviour in a cold-worked austenitic stainless steel (X3CrMnNiMoN17-8-4) in which deformation-induced martensite formation occurs during mechanical deformation. Three different states of pre-deformation (31 %, 39 % and 49 %) that showed induced phase transformation from austenite to α’martensite as well as the solution-annealed material were part of this study. All samples were charged with hydrogen in a 0.1 M NaOH solution. This charging took place electrolytic with 10 mA cm^-2 at three different temperatures (50 °C; 65 °C and 80 °C) in the double cell according to Devanathan and Stachurski. Due to the very slow diffusion of hydrogen through austenite, the samples were not charged until the equilibrium state was reached. To find out the necessary diffusion parameters, the data were fitted with numerical optimisation. Using this method, the effective diffusion coefficients of charging could be determined for all material states. The study also contains microscopic analyses to visualize the effect of cold working on the microstructure of the material. The appearance of α’-martensite significantly contributes to the susceptibility to hydrogen uptake leading to increasing diffusion coefficients in relation to higher pre-deformation.

Abstract: Process maps according to Parasad et al. are already widely used to make statements about the formability of materials and their forming energy. However, these process maps only apply to conventional incompressible materials. At the TU Bergakademie Freiberg, these process maps have already been extended for particle-reinforced incompressible solid materials with a homogeneous particle distribution. The next step is to adapt the model for compressible particle-reinforced matertials so that they can also be used in powder metallurgy. The problem here is that the volume decreases as a result of compaction during powder forming. In powder metallurgy, however, compaction plays an important role. On the one hand, the compaction of the components leads to an increase in the material properties. On the other hand, pores pose a high risk of fractures and cracking. For this reason, it is the aim of this paper to make the existing process maps for incompressible materials usable for compressible materials by corresponding adaptations of the models prevailing in powder metallurgy. Furthermore, the effects of a homogeneous particle distribution and a graded particle distribution within the TRIP matrix composites on the process maps will be investigated. For this reason, process maps are produced in the temperature ranges between 700 – 1050 °C, with forming speeds of 0.001 – 100 s^-1 and residual porosity of 10 – 30 %. For this purpose, specimens with corresponding residual porosity and homogeneously distributed ZrO₂ 5 vol.%, 10 vol.%, 15 vol.% and 20 vol.% as well as a graded layer structure of corresponding ZrO₂ proportions are prepared. With the aid of these specimens, flow curves are determined and adjusted at appropriate temperatures and forming speeds during compression tests. The energy dissipation and an instability map are then modelled from these flow curves and a process map is derived. It was found that with increasing ZrO₂ content in the homogeneous and the graded structure, the areas that allow damage-free forming become smaller. The same applies with decreasing residual porosity. Nevertheless, the areas, which allow failure-free forming, are larger than the possible forming areas of solid components. However, the power dissipation efficiency of incompressible specimens is significantly lower than that of compressible specimen [1]. In addition, it was observed that with increasing ZrO₂ content and decreasing residual porosity, the efficiency of the power dissipation in the formable areas decreases. It was also found that the distribution of the reinforcing particles has a significant influence on the flow curves and the associated process maps, then the graded specimen do not represent a superposition of the individual process maps of the homogeneous specimens.

Abstract: The addition of titanium is a well-known microalloying concept for hot rolled structural steels. Concerning advanced high strength steels for the automotive sector, the use of Ti microalloying (usually with Nb-V) has been an active research area. However, Ti addition has not been explored in depth. For the current contribution, a laboratory hot rolled 0.2C-2.4Mn-1.5Si steel with and without Ti addition was studied. Mechanical testing of the hot strip revealed a very high UTS (1GPa) for the Ti added steel, whilst for the unalloyed chemistry the UTS was some 300 MPa lower. Observation of the hot rolled microstructures via optical microscopy showed a significantly higher hardenability for the Ti added steel. Moreover, X-ray diffraction analysis indicated a significant amount of retained austenite in the Ti added strip, which transformed completely to martensite after the tensile test. Further analysis via TEM and chemical extraction indicated that Ti was present both as Ti (C,N) precipitates and in solution. Finally, in light of these observations, the possible mechanisms leading to the enhanced hardenability observed for the Ti added hot rolled strip steel were discussed.

Abstract: Q&P annealing cycles with different partitioning conditions were performed on cold rolled 0.2C-2.22Mn-1.44Si-0.21Cr steel. An important influence of partitioning temperature and time on the evolution of retained austenite fraction was shown through the saturation magnetization measurements. Such effect of partitioning conditions was also observed on the evolution of mechanical behavior. The evolution of microstructure and mechanical properties with the partitioning conditions was analyzed. Mechanical stability of retained austenite as a function of partitioning time was also assessed. Finally, modeling of the obtained stress-strain curves was performed and some explanations of the observed tendencies between partitioning conditions and tensile properties were proposed.

Abstract: Metastable β-type titanium alloys are highly suitable for use as structural biomaterials applied to hard tissue, i.e., as cortical bone (hereafter, bone) replacing implants. However, their mechanical biocompatibitities, such as the Young’s modulus, strength and ductility balance, fatigue strength, resistance against fatigue crack propagation and fracture toughness, require improvenent for increased compatibility with bone. Through deformation, the metastable β-phase in a metastable β-type titanium alloy is transformed into various phases, such as α’ martensite, α” martensite, and ω-phases with exact phase depending by metastable β-phase stability. In addition, twinning is also induced by deformation. Deformation twinning effectively enhances the work hardening in the metastable β-type titanium alloy, leading to increased strength and ductility. This improvement is accompanied by with other deformation-induced transformations including the appearance of deformation-induced martensite and ω-phase transformation. The enhancement of the mechanical biocompatibility of various materials using the abovementioned deformation-induced transformation is described in this paper, for both newly developed metastable β-type Ti-Mo and Ti-Cr alloys for biomedical applications.

Abstract: The material flow in particle reinforced metal-matrix-composites (MMC) had been investigated. The composite consisted of TRIP steel and magnesium stabilized ZrO₂ particles (Mg‑PSZ) in volume fractions of 0 %, 5 % and 20 %. The basic materials were produced by hot-pressing and showed a very homogeneous particle distribution and a almost full density. Then the samples were cut to wedge shape and hot-rolled with a constant roll gap. Caused by the shape, the true strain increased over the length and reached a maximum of true strain of 0.6. The strain rate was set to be higher than 0.1 and lower than 10/ s. After rolling, it was possible to combine rolling force, true strain and the material flow due to the grid on the surface. With an increase in volume fraction of Mg‑PSZ the rolling force increases as well. Metallographic examinations were performed to determine and document the flow of particles within the composite due to true strain conditions. It was found that the particles flow with the base material and turn parallel to the rolling direction. This effect was measured using the degree of orientation of partially oriented linear structure elements Ω_12, according to ASTM E 1268-01. The index was increasing with increasing true strain value. Further microscopic examination showed debonding of the interface between particles and matrix-material. For MMC’s having a volume fraction of 20 % Mg-PSZ a true strain at fracture of 0.5 to 0.6 was determined.

Abstract: In the second half of the last century, the automobile industries were affected from the petroleum crisis caused mainly by the wars in the Middle East. These crises led the automakers reconsider their vehicles. One of the most important events after that was the adoption of new steels by the industry. One example is the TRIP steels (Transformation-induced plasticity). In this work, a specimen of TRIP steels was etched using LePera reagent. The obtained images were analyzed using digital processing. Using the ImageJ software the methods threshold and watershed were studied. The methods were compared: the morphological characteristics and volumetric fraction of the retained austenite and martensite phases were analyzed. The results showed that the threshold led to a higher number of identified grains with lower mean area and total area fraction than the watershed method.