Papers by Keyword: Ultrafine Grained

Abstract: A new Severe Plastic Deformation (SPD) technique namely Equal Channel Angular Pressing with Parallel Channels (ECAP-PC) was developed to improve the performance of traditional ECAP. Traditional ECAP produces a gross distortion at both ends during the process. Thus, it resulted in high cost process, because it can cause waste materials that have been estimated from 30% to 50%. To overcome the problem, an alternative procedure was developed in which the ECAP was conducted using two parallel channels, the materials used AA1070 and AA6061 powder with Alumina Nano-Fiber (ANF) as reinforcement. Mechanical properties and Scanning Electron Microscope (SEM) were observed in room temperature pressure and 400^OC heating pressure. Both results were compared to determine the effect of temperature on each process. The result was that at 400^OC temperature pressure, the hardness generated more uniform with hardness average reached 69.3 and 94.52 HV₁₀ and at room temperature pressure, the hardness generated less uniform with an average 30.1 and 73.6 HV₁₀. In hot pressure there was not any micro-crack, but in room temperature pressure there were some micro-crack.

Abstract: During the last decade Equal Channel Angular Pressing (ECAP) has emerged as a widely known procedure for the fabrication of ultrafine grained metals and alloys. This review examines recent developments related to the use of ECAP for grain refinement. In the current study the part of capsules wrapper for powder material to be compressed where the powder AA6061 was wrapped in copper sheet and heated at a temperature of 400 ^OC in hot pressed under the pressure of 400 MPa. Afterward the powder in solid condition was cooled in the air and then does analysis characterization. The sample results of AA6061 are ECAP as is and heat treatment with type Anneal and Artificial Aging (T6) where heat treatment is heated at a temperature of 530 °C for 1 h followed by heating at a temperature of 100 °C for one day and the other for heating at a temperature of 415°C for 2.5 hours followed by heating at a temperature of 177 °C for 8 hours. This paper explains the characteristics of each sample where analyses are based on the mechanism of properties to determine how much change of mechanical properties and microstructure. Heat treatment effect on grain coarsening so that the mechanical properties can be engineered.

Abstract: Aluminum is one of the nonferrous metals with very wide applications. It has unique properties such as light weight and it is ductile has additionally, lower melting point compared to iron. Equal Channel Angular Consolidation (ECAC) is manufacturing method to produce alloys with high strength by consolidation at elevated temperatures. ECAC method can produce a fine grain and combined with oxide inclusion from particle surfaces, high strength. This research will examine the applicability of Equal Channel Angular Consolidation to incorporate aluminum Al 7075 series powder at a temperature of 400^OC under pressure of 400 MPa. The effects of heat treatment regimes on grain size of the ECAC samples are observed. The results show hardness of 7075 Aluminum series after ECAC process reaching 120 HV₁₀ and decreases down to 110 HV₁₀ after T6 heat treatment. Hardness further decreases after annealing process, down to 104 HV₁₀. Decline in hardness is accompanied with the increased grain size, which accompanies increased ductility.

Abstract: Ultrafine grained Al-4wt%Cu-(2.5-10) vol.% SiC metal matrix composite powders were produced from a mixture of Al, Cu and SiC powders using high energy mechanical milling (HEMM). The composite powders produced were first hot pressed at 300°C with a pressure of 240 MPa to produce cylindrical powder compacts with a relative density in the range of 80-94% which decreased with increasing the SiC volume fraction. Powder compact forging was utilized to consolidate the powder compacts into nearly fully dense forged disks. With increasing the volume fraction of SiC from 2.5% to 10%, the average microhardness of the forged disks increased from 73HV to 162HV. The fracture strength of the forged disks increased from 225 to 412 MPa with increasing the volume fraction of SiC particles from 2.5 to 10%. The Al-4wt%Cu-2.5vol.%SiC forged disk did not show any macroscopic plastic yielding, while the Al-4wt%Cu-(7.5 and 10)vol.% SiC forged disk showed macroscopic plastic yielding with a small plastic strain to fracture (~1%).

Abstract: Interest in processing of bulk ultrafine-grained materials has grown significantly over the last years. Severe plastic deformation processes such as twist extrusion have been the essence of these researches and used to decrease the bulk grain size. The bulk gain size can reduce if twist extrusion process combines with a conventional forming technique. In this study, the effects of reduction by employing the rolling process after the twist extrusion method were considered. The twist extrusion process of the commercially pure aluminum sample was carried out using a twisted die with 60º die angle, and the samples were processed through rolling subsequently. As a result of rolling, average microstructure grain size decreased significantly and the hardness amount increased accordingly

Abstract: The microstructure, fatigue crack growth behaviour and hardness of ultra fine grained 6061 aluminium alloy obtained by equal angle channel processing was studied. ECAP resulted in significant grain refinement down to the sub micron level and corresponding increase in hardness. Results point to a similar fatigue threshold stress intensity range and fatigue crack growth rates for 1, 2, 4 and 6 passes of ECAP.

Abstract: Severe plastic predeformation of crystalline materials leads not only to formation of a steady-state dislocation structure including low-angle boundaries, but also brings the high-angle boundary structure into a steady state. When the steady-state flow stress is high enough, the material becomes ultrafine-grained or even nanocrystalline. The change from coarse-grained to ultrafine-grained is accompanied by a distinct change in the steady-state deformation resistance that is measured after predeformation. This is explained by two opposing effects of high-angle boundaries, namely enhanced dislocation storage and accelerated dislocation recovery. The first one causes net hardening at high temperature-normalized strain rate Z (Zener–Hollomon), the second one net softening at low Z. This means that the rate-sensitivity of the flow stress is enhanced, which causes the paradoxon of enhanced strength at enhanced ductility. Tests with abrupt large changes of deformation conditions bring the strain associated with dynamic recovery into the focus. The results of such tests indicate that the boundaries, low-angle as well as high-angle ones, migrate under concentrated stress during deformation and thereby contribute to straining and recovery. The corresponding system of differential equations needed to model structure evolution and deformation kinetics on a semi-empirical basis is briefly discussed.

Abstract: Specimens of medium carbon steel were quenched and warm-compressed on a Gleeble 3500 Machine. The microstructure of the specimens was studied by using an optical microscope and a transmission electron microscopy. And the properties were investigated by using tensile tests and hardness tests. Results show that the starting microstructure is lath martensite with a small amount of flake martensite. After 50% compression at 550-650°C, ultrafine grains can be observed in the specimens. The microstructure of the specimens compressed at 600°C is equiaxed ultrafine ferrite grains + nano-carbides and a good combination of strength and ductility is obtained. The tensile strength and total elongation are 861MPa and 19.1%, respectively. The hardness is 233.81Hv.

Abstract: An ultrahigh carbon steel alloy containing 1.4 wt pct carbon (UHCS-1.4C) was studied. The steel was processed into ultrafine grain and fully spheroidized microstructure through a controlled rolling and controlled-cooling divorced eutectoid transformation, and was then given austempering treatment to form bainite. The mechanical properties of the heat-treated steel were evaluated by tension tests at room temperature. After austenitized at 850 °C and then austempered at 300 - 350 °C, the microstructure was ultrafine upper bainite, retained austenite, and unsolvable cementite. It was shown that the ultimate tensile strengths of UHCS-1.4C ranged from 1420 to 1830 MPa, elongations to failure from 6 to 14%; the ultimate tensile strength increases with decreasing austempering temperature, while the tensile ductility decreases. The fracture surface of bainitic UHCS-1.4C consists mainly of dimples and voids, which reveal a ductile fracture. The present results indicate that ultrahigh carbon steel can be easily processed to achieve bainitic microstructures and unique properties.

Abstract: The Mg96Y3Zn1 alloy processed by equal channel angular pressing has been investigated. It was found that the Mg96Y3Zn1 alloy processed by ECAP obtained ultrafine grains and exhibits excellent mechanical properties. After ECAP, the average grain size of Mg96Y3Zn1 alloy refined to about 400 nm. The highest strengths with yield strength of 381.45MPa and ultimate tensile strength of 438.33MPa were obtained after 2 passes at 623K. It was found that cracks were preferentially initiated and propagated in the interior of X-phase during the tensile test. As a result, the elongation of alloy is decreased with pass number increasing.