Papers by Keyword: Ultrafine Grained Structure

Abstract: The microstructure evolution and mechanical properties of a copper alloy subjected to deformation at temperatures of 20 °C and 400 °C to total strains from 1 to 4 were examined. The formation of planar low-angle boundaries with moderate misorientations occurs within initial grains at relatively small strains regardless of deformation temperature. Upon further processing the misorientations of these boundaries progressively increase and the new ultrafine grains develop. Continuous dynamic recrystallization takes place during deformation at ambient and elevated temperatures. The kinetics of dynamic recrystallization is discussed in terms of a modified Johnson-Mehl-Avrami-Kolmogorov relationship. The large plastic straining results in significant strengthening, the ultimate tensile strength increases from 190 MPa in the initial state to 440 MPa and to 400 MPa after total strain of 4 at 20 °C and 400 °C, respectively. A modified Hall-Petch relationship is applied to evaluate the contribution of grain refinement and dislocation density to the overall strengthening.

Abstract: The article presents the results of an investigation of microstructure, mechanical properties and corrosion resistance of magnesium alloy WE43 processed by rotary swaging. The resulting microstructure is characterized by an average size of structural elements of 0.5 – 0.8 μm. The grain refinement leads to an increase in the strength of the alloy to 393 – 416 MPa while the tensile elongation stays at a level of 7 – 12.5%. The microstructure produced by rotary swaging does not lead to deterioration of the resistance of the alloy to electrochemical and chemical corrosion.

Abstract: It is shown that formation of ultrafine-grained structure in EK61 superalloy up to grain sizes less than 1 μm provides to realize superplastic properties. The influence of deformation in the temperature range 600-1100 °C and strain rate range 10^-4s^-1– 10^-3s^-1 on the microstructure and properties of ultrafine-grained nickel-based alloy EK61 is studied. It is established that in temperature range 750-900 °C the alloy demonstrates superplasticity (SP) characteristics: strain rate sensitivity factor “m” correspond to 0.39-0.59, stable structure and low changes in the form and size of grains. The maximum SP is displayed at temperatures of 800 °C, wherein the elongation is 1431 %. It has been experimentally confirmed that the use of low-temperature superplasticity is a promising for processing sound solid phase joints by pressure welding of similar and dissimilar Ni-based superalloys.

Abstract: Influence of friction stir welding (FSW) on microstructure of an Al-4.57Mg-0.35Mn-0.2Sc-0.09Zr (wt. pct.) alloy was studied. Following parameters of FSW were used: the rotation speeds of 500, 650 and 800 rpm, the traverse speed of 75 mm/min and the tilt angle of 2.5°. Defect-free welds were obtained using all these parameters. FSW leads to the formation of fully recrystallized microstructures with average grain sizes less 2 μm and a moderate dislocation density of ~10¹³ m^–2 in the stir zone. No evidence for abnormal grain growth was found in the heat affected zone of the weld. The nanoscale Al₃(Sc,Zr) dispersoids coarsened to 21 nm but retained coherent interfaces and cube-cube orientation relationship with the matrix.

Abstract: The results of development of new resource-saving technologies of local shape-forming under superplastic deformation conditions (SP) by means of roll-forming and rotary swaging are presented. These technologies are efficient for fabrication of discs, shells, rings up to 800 mm in diameter, as well as hollow shafts made of heat-resistant nickel-, titanium-and iron-based alloys that are used in aircraft engines and ground power installations. In particular, to implement innovative technologies a universal SRZhD-800 roll-forming mill has been developed for discs roll-forming made of heat-resistant alloys under SP. An efficiency of using of semi-finished products with prepared ultrafine grained (UFG) structure for generating precise complex geometry profile parts both homogeneous and regulated structure that changing in the radial direction of the disc and for obtaining high mechanical properties that are optimized taking operational conditions into account is proved. The technological process of rotary swaging under SP conditions has been developed for fabrication parts made of high alloy heat-resistant alloys using demountable mandrels. This method allows to obtain precise complex geometry profile parts such as disc with a thin cone flange which is characterized by homogeneous structure and high mechanical properties.

Abstract: The ultrafine grained structure of an AA5024 with an average size of ∼0.7 μm was produced by equal-channel angular pressing (ECAP) at 300°C with a total strain of ~12. Superplastic behavior of this alloy was examined in the temperature interval 175 - 300°C at strain rates ranging from 10^-4 to 10^-1 s^-1. The maximum elongation-to-failure of ~1200% with the corresponding strain rate sensitivity coefficient, m, of ∼0.49 was attained at a temperature of 275°C and a strain rate of 5.6×10^–3s^–1. At 175°C (~0.53T_m, where T_m is the melting point), the elongation-to-failure of ~370% with the m value of ~0.3 was found at ε̇=1.4×10^–4 s^–1.

Abstract: Severe plastic deformation is a well known procedure for fabrication considerable grain refinement in metal materials. Equal channel angular pressing (ECAP) is one of these severe plastic deformation techniques which allows the receiving of the bulk ultrafine grained (UFG) metals. It is well known that the ECAP method leads to significant improvement of strength of investigated materials, but the fracture mechanisms of UFG metals at low temperature are not enough studied. The investigation was performed on low-alloy constructional steel 09G2S (GOST) after application of ECAP. Fracture toughness tests were performed on Charpy impact testing specimens at low temperature. The experiments demonstrate that ECAP treatment has the effect on increasing of fracture resistance of steel 09G2S at low temperature.

Abstract: Mechanisms of dynamic recrystallization operating at severe plastic deformation in a wide temperature range are reviewed for aluminum alloys. The main mechanism of grain refinement in all aluminum alloys is continuous dynamic recrystallization (CDRX). Temperature, deformation process and distribution of secondary phases strongly affect the CDRX mechanism. Initial formation of geometrically necessary boundaries (GNBs) and a dispersion of nanoscale particles accelerate CDRX facilitating the formation of a 3D network of low-angle boundaries (LAB) followed by their gradual transformation to high-angle boundaries (HAB). At high and intermediate temperatures, 3D networks of LABs may evolve due to rearrangement of lattice dislocations by climb, and mutual intersection of GNB, respectively. At high temperatures, in aluminum alloys containing no nanoscale dispersoids the CDRX occurs through the impingement of initial boundaries forced by deformation-induced LABs. This recrystallization process is termed as geometric dynamic recrystallization (GDRX). At low temperatures, the extensive grain refinement occurs through a continuous reaction which is distinguished from CDRX by restricted rearrangement of lattice dislocation. Introduction of large misorientation may occur through the formation of 3D networks of GNBs, only.

Abstract: Diffusion bonding of Ti-6Al-4V titanium alloy in the coarse grained and ultrafine grained state was performed. The effect of initial structure and surface condition, as well as temperature and time, on the quality of joints was established. It is shown that, due to low-temperature superplasticity and high diffusion rate, samples with ultrafine grained structure demonstrate better bondability than coarse grained samples

Abstract: Equal channel angular pressing (ECAP) results in grain-subgrain structure formation in Cu0.75 %Cr alloy with the average size of structure elements of 320 ± 73 nm Addition of hafnium into the Cu-Cr alloy leads to decrease of average size down to 225±82 nm and to increase of the high angle boundaries fraction from 40% to 53%. Microhardness of the Cu-0.7 %Cr-0.9 %Hf alloy is higher, than of the Cu-0.75 %Cr alloy, as after ECAP, so after heating when the aging processes occur in the temperature interval 400–550 °С. The strength in the tension tests of the Cu-0.7 %Cr-0.9 %Hf alloy after ECAP rises in 2.2 times compared with the quenched state. The aging leads to additional strength growth by 19%.