Papers by Keyword: X-Ray

Abstract: Lead hydroxyapatite (PbHAP, chemical formula Pb₁₀(PO₄)₆(OH)₂) has been synthesized by ceramic (solid-state reaction) and semi-ceramic (precipitation) methods. The samples were prepared through a solid-state reaction conducted at 830 °C for 60 hours, with the y values ranging from 0.95 to 1.00. We have developed and created the most efficient preparation methods. The well-known technique was used - semi-ceramic (precipitation) deposition of lead and hydroxyapatite. For this purpose, several advanced devices were used to obtain an accurate structural structure of lead hydroxyapatite compounds. It has been observed, as in the case of chemical synthesis, that the elements (lead, phosphorus, and oxygen) appear to be distributed homogeneously within the crystals, regardless of the method of composition, which indicates that the samples are homogeneous. More importantly, the "solid-state reaction" method favored a specific composition range, while the "precipitation" method performed well for other composition ranges. The above methods indicate an ideal method, according to the desired structure, that should be developed for lead hydroxyapatite, depending on its composition. This research aims to establish the first steps in developing a new method for preparing lead hydroxyapatite compounds with the desired properties to improve their purity and crystal structure for potential uses in the future.

Abstract: In this article an x-ray method of analysing modified vehicle series is presented. A method of electrochemical analysis of a vehicle's series was also used beforehand to highlight its modification. This method is particularly useful in identifying and characterizing changes in the structural or material composition of vehicles that have undergone modifications. Before discussing the x-ray analysis, the article also mentions the use of electrochemical analysis as an initial approach to highlight modifications in vehicle series. Finally, the advantages and disadvantages of the x-ray analysis method are presented.

Abstract: Coronavirus (COVID-19) has grown to be one of the most dangerous and acute illnesses in recent years, and it has now spread across the globe. In order to prevent COVID-19, early detection of the Coronavirus is necessary. Using a convolutional neural network (CNN) and long short-term memory (LSTM), we have suggested a model for automatically diagnosing COVID-19 from X-ray images. In this model, CNN is used to extract deep features, while LSTM is utilized to identify those features. The proposed method can aid in the diagnosis and treatment of patients with COVID-19. As a final step, this technology will be able to accurately detect the severity of the disease in the lungs and provide it with an automated diagnostic. This model will be hosted on the website so that hospital visits may be minimized and diagnosis can be delivered at home, if necessary, thereby giving a solution for COVID-19 containment.

Abstract: Clinching is a cost efficient method for joining components in series production. To assure the clinch point’s quality, the force displacement curve during clinching or the bottom thickness are monitored. The most significant geometrical characteristics of the clinch point, neck thickness and undercut, are usually tested destructively by microsectioning. However, micrograph preparation goes ahead with a resetting of elastic deformations and crack-closing after unloading. To generate a comprehensive knowledge of the clinch point’s inner geometry under load, in-situ computed tomography (CT) and acoustic testing (TDA) can be combined. While the TDA is highly sensitive to the inner state of the clinch point, it could detect critical events like crack development during loading. If such events are indicated, the loading process is stopped and a stepped in-situ CT of the following crack and deformation development is performed. In this paper, the concept is applied to the process of clinching itself, providing a detailed three-dimensional insight in the development of the joining zone. A test set-up is used which allows a stepwise clinching of two aluminium sheets EN AW 6014. Furthermore, this set-up is positioned within a CT system. In order to minimize X-ray absorption, a beryllium cylinder is used within the set-up frame and clinching tools are made from Si3N4. The actuator and sensor necessary for the TDA are integrated in the set-up. In regular process steps, the clinching process is interrupted in order to perform a TDA and a CT scan. In order to enhance the visibility of the interface, a thin tin layer is positioned between the sheets prior clinching. It is shown, that the test-set up allows a monitoring of the dynamic behaviour of the specimen during clinching while the CT scans visualize the inner geometry and material flow non-destructively.

Abstract: Ti-based intermetallic compounds are characterized by low machinability, therefore, to obtain accurate dimensions and shape of the surface grinding and Wire EDM are used. The unique properties of NiTi intermetallic alloys are largely influenced by structural phase transformations and variations in microhardness caused by processing accompanied by thermal phenomena. Having an understanding of the physics of the process, it is possible to counteract negative effects, which helps to preserve thermomechanical properties of the final NiTi products. Accumulation of knowledge about the quality of processing with various abrasive tools is part of the larger research presented in this article. Samples of titanium nickelide with a temperature A_f=+25 ⁰С were abraded with ordinary and high porosity SiC wheels. The article studied phase transformations using X-ray diffraction analysis and microhardness. The experimental data were processed using mathematical statistics. X-ray diffraction patterns and microhardness analysis showed that a significant effect on the structural transformation and corresponding increase in microhardness is exerted by grinding with green SiC wheels with normal porosity caused by an increased thermal effect on the surface. Simultaneously, the impact of Wire EDM process on microhardness in preparing workpieces for grinding was evaluated. It was established that grinding of Ti-based intermetallic compounds with memory effect should be performed by SiC wheels with an open structure of high porosity.

Abstract: An iterative polynomial fitting method is proposed for the estimate of the baseline of the X-ray fluorescence spectrum signal. The new method generates automatic thresholds by comparing the X-ray fluorescence spectrum signal with the calculated signal from polynomial fitting in the iterative processes. The signal peaks are cut out consecutively in the iterative processes so the polynomial fitting will finally give a good estimation of the baseline. Simulated data and real data from the soil analysis spectrum are used to demonstrate the feasibility of the proposed method.

Abstract: When joining lightweight parts of various materials, clinching is a cost efficient solution. In a production line, the quality of a clinch point is primarily controlled by measurement of dimensions, which are accessible from outside. However, methods such as visual testing and measuring the bottom thickness as well as the outer diameter are not able to deliver any information about the most significant geometrical characteristic of the clinch point, neck thickness and undercut. Furthermore, ex-situ destructive methods such as microsectioning cannot detect elastic deformations and cracks that close after unloading. In order to exceed the current limits, a new non-destructive in-situ testing method for the clinching process is necessary. This work proposes a concept to characterize clinch points in-situ by combining two complementary non-destructive methods, namely, computed tomography (CT) and ultrasonic testing. Firstly, clinch points with different geometrical characteristics are analysed experimentally using ex-situ CT to get a highly spatially resolved 3D-image of the object. In this context, highly X-ray attenuating materials enhancing the visibility of the sheet-sheet interface are investigated. Secondly, the test specimens are modelled using finite element method (FEM) and a transient dynamic analysis (TDA) is conducted to study the effect of the geometrical differences on the deformation energy and to qualify the TDA as a fast in-situ non-destructive method for characterizing clinch points at high temporal resolution.

Abstract: Performing X-ray stress measurement by a new method called the cosα method is spreading in Japan. The cosα method is characterized in that the entire diffraction ring is used and analysed. As a result, the measurement speed is fast, and the device can be downsized. On the other hand, the conventional sin²ψ method requires precise measurement of diffracted X-rays at several X-ray incident angles, which increases the measurement time and the size of the device. In addition, since only a small part of the diffraction ring generated during the X-ray irradiation is used, some of the information on the diffraction ring cannot be used so it is a wasteful method. In 2012, cosα method equipment was released in Japan. Since then, cosα method X-ray stress measurements have been performed at more than 300 facilities. In response to this situation, the Japan Society for Nondestructive Inspection (JSNDI) together with public and private institutions established a study group on the cosα method in 2014, and examined the cosα method and its appropriate use. In this paper, we report the results of this study group.

Abstract: The paper presents results of tests conducted on self-compacting mixes with the addition of engineered steel fibres. There were used four types of fibres. The fibres were added at 5 levels of the volume ratio. Firstly, fresh mixes were tested (slump flow, class of viscosity and rheological characteristics). Secondly, properties of hardened concretes were tested (compressive strength and flexural strength). Hardened concretes were also tested using non-destructive method, namely X-ray computed tomography. The tests confirmed the possibility of using steel fibres for reinforcing self-compacting concrete. The workability of mixes was maintaining and the assumed technological parameters for hardened concretes were kept. It was found that longer fibres are more likely to be oriented parallel to the direction of the mix flow. Thus, they can operate efficiently under flexural loading of the cast beam.

Abstract: Lipids and proteins can influence each other in so many different ways. Lipids may affect the structure of membrane proteins by influencing their backbone conformation, the tilt, rotation angles of their transmembrane (TM) segments, and the orientation of their side chains. The membrane-spanning parts in integral membrane proteins are predominantly hydrophobic, and most often helical. At the lipid-protein interface, the TM part of the protein and the hydrocarbon chains of the lipid molecules have to coexist to maintain the integrity of the membrane. Lipids are important components of lipid membrane are used in various experiments reported in this thesis and can act as model lipid bilayers. Once they support on solid substrate like silicon wafers, their structural properties can investigate by X-ray and neutron reflectivity and by other useful techniques. Reflectivity technique can provide detailed information such as their thickness and interaction between lipids and peptides. The thesis reports a detailed investigation of these lipids and peptides by X-ray and neutron reflection techniques