Papers by Keyword: β Phase

Abstract: The results of the investigations on five different titanium alloys were presented in this paper. Two two-phase α+β alloys (Ti-6Al-4V and Ti-6Al-2Sn-4Zr-6Mo) as well as two β alloys (Ti-10V-2Fe-3Al and Ti-3Al-8V-6Cr-4Mo-4Zr) were studied. Moreover, Ti-48Al-2Cr-2Nb intermetallic alloy (γ alloy) was also investigated. All investigated alloys were tested in compression on Gleeble thermomechanical simulator under various strain rate and temperature conditions. Metallographic observations of the microstructure of tested samples allowed determining thermomechanical conditions under which dynamic recrystallization or recovery processes occurred in the investigated alloys. The obtained results also showed the importance of the influence of strong exothermic effect resulting from deformation process on recovery and recrystallization processes in these alloys. The methodology of distinguishing subgrains formed during recovery process from the grains resulting from recrystallization was also presented in this study.

Abstract: The effects of pre-aging and natural aging on the bake hardening behavior of Al-0.62Mg-0.93Si (mass%) alloy with multi-step aging process were investigated by means of Vickers hardness test, tensile test, differential scanning calorimetry analysis (DSC) and transmission electron microscopy (TEM). The characteristics of nanoclusters (nano scale solute atom clusters) formed during pre-aging and natural aging were also investigated using the three dimensional atom probe (3DAP) analysis. The results revealed the occurrence of natural age hardening and that the bake hardening response was decreased after the extended natural aging even though the pre-aging was conducted before natural aging. Since the 3DAP results exhibited the Si-rich clusters were newly formed during extended natural aging, it was assumed that the Si-rich clusters caused the natural age hardening and the reduced bake hardening response corresponding to Cluster(1). The decrease of the bake hardening response was markedly higher in the later stage of bake hardening than in the early stage. The size of the β’’ precipitates were reduced with increasing the natural aging time. Exothermic peaks of Peak 2 and Peak 2’ were observed in the DSC curves for the alloys pre-aged at 363K. Peak 2’ became larger with the natural aging time. This is well understood by the following model. The transition from Cluster(2) to the β’’ phase occurs preferentially at the early stage of the bake hardening. Then the growth of the β’’ phase is inhibited by the presence of Cluster(1) at the later stage of bake hardening. The combined formation of Cluster(1) and Cluster(2) by the multi-step aging essentially affects the bake hardening response and the β’’ precipitates in the Al-Mg-Si alloys.

Abstract: In this study, the effect of oxygen addition on the microstructures of Ti-18%Mo-10%Cr alloy was investigated. The alloy was fabricated by a powder metallurgy method. The samples were subjected to sintering at 1300°C for 4 hours and furnace cooling. A Bo-Md method was initially applied for predicting stable phase. Calculation using the Bo-Md method showed that Ti-18%Mo-10%Cr alloy have bcc (β) phase at ambient temperature. All samples with various oxygen contents exhibited needle-like structures within equiaxed grains. The increase of oxygen content promoted formation of porosity in the α phase. Calculation of phase stability using JMatPro^TM showed that the decrease of β phase’s stability was not due to formation of the α phase on sintering, but due to promotion of nucleation and grain growth of diffusional α phase upon furnace cooling. It was also shown that vol.% of porosity of the alloy slightly increased with increasing oxygen content. Therefore, the increase of oxygen concentration could accelerate the formation of α phase and reduce the alloy’s density. The hardness increased as the oxygen concentration increased. The increase of the hardness might be due to combination of the solid solution hardening of oxygen and the precipitation hardening of α phase.

Abstract: The effects of Al, Zr additions on the microstructure and properties of a β matrix Mg-Li-Al-Zr alloy of hot forged, cold rolled and heat- treated states have been systematically investigated. The tensile properties of the alloy was tested, and microstructure was studied by X-ray diffraction and SEM methods. The results showed that the addition of zirconium in the aluminum containing Mg-Li alloy was effective for grain refinement. The alloy containing zirconium of rolled state exhibited higher strength and satisfied ductility compared with the alloy without zirconium. The existence of zirconium in the alloy was mainly in the form of Al-Zr compounds of Al2Zr andAl3Zr. The reason for less age-hardening effect may be caused by the capture of aluminum by zirconium and as a consequent by the lake of aluminum in the matrix.