Preparation of Nanocrystalline Copper Powders by Aqueous Reduction

Qin, Ying; Zhang, Peng Yuan; Chen, Jian Feng

doi:10.4028/www.scientific.net/AMR.11-12.575

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Home Advanced Materials Research AICAM 2005Preparation of Nanocrystalline Copper Powders by...

Preparation of Nanocrystalline Copper Powders by Aqueous Reduction

Abstract:

This paper aims at a simple preparation method of nanocrystalline copper powders through copper sulfate reduction by potassium borohydride in aqueous solution. The product powders obtained in various conditions were investigated by X-ray powder diffraction, transmission electron microscope and particle size distribution analyzer. The parameters that influence the preparation process of copper crystalline were researched, such as the effect of complexing agent, the molar ratio of copper sulfate to potassium borohydride and the quantity of protective polymer. Finally, the preferable reaction conditions were determined, and well-dispersed nanocrystalline copper powders with average diameter of 28.4nm were obtained.

Info:

Periodical:

Advanced Materials Research (Volumes 11-12)

Main Theme:

AICAM 2005

Edited by:

Masayuki Nogami, Riguang Jin, Toshihiro Kasuga and Wantai Yang

Pages:

575-578

DOI:

10.4028/www.scientific.net/AMR.11-12.575

Citation:

Y. Qin, P. Y. Zhang, J. F. Chen, "Preparation of Nanocrystalline Copper Powders by Aqueous Reduction", Advanced Materials Research, Vols. 11-12, pp. 575-578, 2006

Online since:

February 2006

Authors:

Ying Qin, Peng Yuan Zhang, Jian Feng Chen

Keywords:

Aqueous, Complexing Effect, Nanocrystalline Copper Powders, Reduction

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