Preparation and Characterization of Helical Structure ZnS by Solvothermal Method

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Helical structure ZnS were successfully prepared via solvothermal method by the reaction of zinc acetate and sodium sulphide. The composition, morphology, and microstructure of the sample were characterized by X-ray diffraction (XRD), high resolution transmission electron microscopy (HRTEM), the corresponding selected area electron diffraction (SAED) and X-ray energy spectrum (EDS). The experiment results show that the sample is 1-D hexagonal crystal ZnS and grows along the [002] direction, and is helical structure, with lengths in the range of 100-200 nm, the diameter about 5-15 nm, and pitch about 20nm.

Info:

Periodical:

Advanced Materials Research (Volumes 233-235)

Edited by:

Zhong Cao, Lixian Sun, Xueqiang Cao, Yinghe He

Pages:

1954-1957

DOI:

10.4028/www.scientific.net/AMR.233-235.1954

Citation:

X. Y. Yan et al., "Preparation and Characterization of Helical Structure ZnS by Solvothermal Method", Advanced Materials Research, Vols. 233-235, pp. 1954-1957, 2011

Online since:

May 2011

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$35.00

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