Measuring the Phthalates of Xiangjiang River Using Liquid-Liquid Extraction Gas Chromatography

Abstract:

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Objective: To observe the phthalates pollution situation in water environment and design the liquid-liquid extraction gas chromatography method to measure phthalates in Xiangjiang River water. Methods: The water samples were collected from six monitor points of the Xiangjiang River’s Changsha period. After liquid-liquid extraction, gas chromatography was used to measure and analyze the phthalates pollution in this period of the river. Results: Dioctyl phthalate resin (DOP) and dibutyl phthalate (2- ethylhexyl) phthalate (DEHP) were detectable in all samples from six monitor points, the concentrations of DEHP were from 0.62-15.23μg/L, DOP were from 0.04-0.21μg/L. Conclusion: The optimum conditions for the extraction of phthalates are: 0.025ml dichloromethane as extraction solvent, centrifuge speed at 4000r/min, extraction time 20 minutes, and this method is appropriate for monitoring the phthalates pollution in water environment.

Info:

Periodical:

Advanced Materials Research (Volumes 301-303)

Edited by:

Riza Esa and Yanwen Wu

Pages:

752-755

DOI:

10.4028/www.scientific.net/AMR.301-303.752

Citation:

X. J. Zhu and Y. Y. Qiu, "Measuring the Phthalates of Xiangjiang River Using Liquid-Liquid Extraction Gas Chromatography", Advanced Materials Research, Vols. 301-303, pp. 752-755, 2011

Online since:

July 2011

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$35.00

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