Synthesis of n-Amyl Chloroacetate Catalyzed by Activated Carbon Supported Phosphotungstic Acid

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Phosphotungstic acid(abbreviated as PW12) supported on active carbon was used as catalyst of n-Amyl chloroacetate synthesis. Review the influence of various factors on esterification ratio, such as ratio of alcohol and acid, reaction temperature, the amount of catalyst and so on. The experiments indicated that the activity of PW12 supported on active carbon was better, the optimum reaction conditions were followings, loading of PW12 was 18%, ratio of alcohol and acid was 1.3:1, the percent of catalyst in reactants was 2.5%.

Info:

Periodical:

Advanced Materials Research (Volumes 581-582)

Edited by:

Jimmy (C.M.) Kao, Wen-Pei Sung and Ran Chen

Pages:

202-205

Citation:

S. P. Wang et al., "Synthesis of n-Amyl Chloroacetate Catalyzed by Activated Carbon Supported Phosphotungstic Acid", Advanced Materials Research, Vols. 581-582, pp. 202-205, 2012

Online since:

October 2012

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$41.00

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DOI: https://doi.org/10.1080/01614948708078072

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