Microstructural Studies of Zr-2.5Nb and Zircaloy-2 Pressure Tubes Irradiated in Indian Pressurized Heavy Water Reactors

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The Indian PHWR uses Zr-2.5% Nb pressure tubes and its in-reactor performance mainly irradiation creep and growth depends strongly on its microstructure. A detailed microstructural examination was carried out on unirradiated pressure tubes off-cuts and an irradiated pressure tube S-07 of KAPS-2 (operated for 8 effective full power years (EFPYs)), Microstructural characterization was carried out using transmission electron microscopy. Microstructual observation of un-irradiated off-cuts shows the lamellar morphology of the -Zr along with the -phase present as stingers between two alpha laths as well as fine and coarse beta globules. The size of -Zr lamellae was found to be in the range from 0.17 to 0.2 m, 1.8 to 2.4 m and 1.7 to 2.8 m in the radial, circumferential and axial direction respectively (aspect ratio of 1:7:8). TEM-EDS analysis showed composition of the  phase tin the range of 15-50 wt%Nb. The irradiated pressure tube samples obtained from 13 locations were showing average alpha grain width, grain length and aspect ratio in the range of 0.17-0.27 micron, 1.7-2.3 micron and 7.1-8.5 respectively. Extensive modification in beta morphology could be seen at the high flux and high temperature regions. The  phase was observed to have globulised completely in many regions. They were present at the interface of -Zr laths as well as within the lath. The Nb concentration of the  phase appeared to have increased as the volume fraction had reduced. The microstructure details of irradiated and un-irradiated pressure tubes obtained in this study is expected to help in modeling the dimensional change occurring during irradiation in reactor.

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Edited by:

B.S.S. Daniel and G.P. Chaudhari

Pages:

56-61

Citation:

D. Srivastava et al., "Microstructural Studies of Zr-2.5Nb and Zircaloy-2 Pressure Tubes Irradiated in Indian Pressurized Heavy Water Reactors", Advanced Materials Research, Vol. 585, pp. 56-61, 2012

Online since:

November 2012

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$38.00

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