1st International Conference On New Materials for Extreme Environment

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Authors: Weon Ju Kim, Seok Min Kang, Ji Yeon Park
Abstract: Microstructure and mechanical/thermal properties of SiCf/SiC composites additionally reinforced with SiC nanowires were investigated. SiC nanowires could be grown successfully within the SiC fiber preform by a chemical vapor infiltration (CVI) process through a control of the deposition parameters. The incorporation of the SiC nanowires into the fiber perform was clearly shown to be effective in increasing the efficiency of the matrix infiltration, and thus resulted in a higher density in a shorter CVI time. The modification of the pore structure and the reduction of the macro-pores in the composite resulted in higher mechanical and thermal properties than the conventional CVI counterpart. The matrix deposition on both surfaces of the SiC fibers and nanowires induced smaller matrix grains in the nanowire-reinforced composite, and thus a higher hardness and elastic modulus than the conventional one after an ion irradiation.
Authors: Stephen Peter Brookes, Hans Joachim Kühn, Birgit Skrotzki, Hellmuth Klingelhöffer, Rainer Sievert, Janine Pfetzing, Dennis Peter, Gunther F. Eggeler
Abstract: A material family to replace the current superalloys in aeronautical gas turbine engines is considered to be that of gamma Titanium Aluminide (-TiAl) alloys. Structural components in aeronautical gas turbine engines typically experience large variations in temperatures and multiaxial states of stress under non-isothermal conditions. The uniaxial, torsional and bi-axial thermo-mechanical fatigue (TMF) behaviour of this -TiAl alloy have been examined at 400 – 800oC with strain amplitudes from 0.15% to 0.7%. The tests were conducted at both in-phase (IP) and out-of-phase (OP). The effects of TMF on the microstructure were also investigated. For the same equivalent mechanical strain amplitude uniaxial IP tests showed significantly longer lifetimes than pure torsional TMF tests. The non-proportional multiaxial OP test showed the lowest lifetimes at the same equivalent mechanical strain amplitude compared to the other types of tests.
Authors: I. López-Galilea, G. Pintsuk, C. García-Rosales, Jochen Linke
Abstract: The technical design solution for the future thermonuclear fusion reactor, ITER, must guarantee a reasonable lifetime from a safety and economical point of view. Carbon fibre reinforced carbon (CFC) is envisaged as a corrective material solution for the strike point area of ITER divertor due to its high thermal shock resistance necessary to withstand excessive heat loads during transient thermal loads; in particular plasma disruptions that can deposit energy densities of several ten MJm-2 with a typical timescale in the order of milliseconds. In this work, as potential alternative to CFCs new finely dispersed TiC-doped isotropic graphites with high thermal conductivity and mechanical strength, manufactured using synthetic mesophase pitch “AR” as raw material, have been evaluated under typical disruption conditions using an energetic electron beam at the JUDITH facility.
Authors: Vaclav Mentl, Josef Bystricky
Abstract: Mathematical modelling and virtual testing of components and structures represent a useful and economic tool for design and safety assessment. The basic mechanical properties which can be found in material standards are not relevant in cases where the real service conditions differ from those applied during standardised testing. Thus e.g. mechanical behaviour at higher strain rates can be interesting for the car components when the simulation of crash situations is used during structure development. The dynamic compression tests are usually performed by means of drop towers, by means of high speed hydraulic testing machines or Hopkinson bar method. At the Mechanical Testing Laboratory of the SKODA Research Inst. in Pilsen, Czech Republic, an instrumentation of Charpy pendulum testing machine was realised in order that it was possible to perfom dynamic compression tests, [1], and the compatibility of obtained results in comparison with traditional impact compression tests was verified within the round–robin carried out by TC5 ESIS Sub-Committee on “Mechanical Testing at Intermediate Strain Rates“, [2]. A new striking tup and load measurement system were designed and callibrated. At the same time, a new software was developed which makes it possible to evaluate the test force-deformation record. The goal of this study was 1. to check the possibility of compression testing of high strength materilas by mens of Charpy pendulum, and 2. to study the strain rate influence on basic mechanical properties.
Authors: K. Mergia, Marco Grattarola, S. Messoloras, Carlo Gualco, Michael Hofmann
Abstract: In plasma facing components (PFC) for nuclear fusion reactors tungsten or carbon based tiles need to be cooled through a heat sink. The joint between the PFC and the heat sink can be realized using a brazing process through the employment of compliant layer of either a low yield material, like copper, or a high yield material, like molybdenum. Experimental verification of the induced stresses during the brazing process is of vital importance. Strains and residual stresses have been measured in Mo/CuCrZr brazed tiles using neutron diffraction. The strains and stresses were measured in Mo tile along the weld direction and at different distances from it. The experimental results are compared with Finite Element Simulations.
Authors: F.M. Halliday, David E.J. Armstrong, John D. Murphy, Steve G. Roberts
Abstract: The mechanical properties of Fe-Cr alloys were investigated in as-grown and in post-ion-implanted conditions. Sets of specimens were produced using dual implantations of Fe+ ions to give 1µm deep damaged layers with average damage levels of 0.35 displacements per atom and 5.33 displacements per atom. Nanoindentation was used to measure hardness as a function of depth and showed that implanted material had a higher hardness than unimplanted material. Additionally, micron-scale cantilevers were fabricated from the ion-damaged surface of the material and were tested using a nanoindenter for AFM-imaging and loading. The mechanical properties deduced from the controlled loading of these cantilevers pertain only to radiation-damaged material, and for the high-dose material show significant changes in Young’s modulus, yield stress and work-hardening.
Authors: Zbigniew Oksiuta, Nadine L. Baluc
Abstract: Six oxide dispersion strengthened (ODS) ferritic steels, with the composition of Fe-(12-14)Cr-2W-(0.1-0.3-0.5)Ti-0.3Y2O3 (wt.%), have been prepared by mechanically alloying elemental powders of Fe, Cr, W, and Ti with Y2O3 nano-particles followed by hot isostatic pressing. The influence of the chemical composition on the microstructure and mechanical properties of various materials was studied. It was found that the chromium content has a significant influence on the microstructure and mechanical properties of the compacted ingots. The 14Cr ODS steel exhibits slightly higher ultimate tensile strength and yield strength values than the 12Cr ODS steel. The total elongation and uniform elongation of both materials, in general, decrease with raising the test temperature, although in the case of the 12Cr ODS steel the elongation is about 30% higher than that of the 14Cr ODS material. In what concerns the effect of titanium content it can be concluded that variations between 0.1 and 0.3% have no visible effects on the microstructure and Charpy impact properties of compacted specimens. However, the microstructure of specimens with 0.5%Ti contains large TiO2 particles with a size in the range of 50-500nm, which have detrimental influence on the mechanical properties of that material.
Authors: Patrick Olier, Zbigniew Oksiuta, Jean François Melat, Didier Hamon, Thomas Leblond, Yann de Carlan, Nadine L. Baluc
Abstract: A new ODS composition (Fe-14Cr-2W-0.3Ti-0.3Y2O3) developed in the ExtreMat integrated Project has been produced by mechanical alloying techniques and consolidated by hot extrusion. This study summarizes some results of characterization and cold workability tests carried out at CEA and EPFL. It appears that the microstructure is fine and uniform after hot extrusion. According to microprobe analysis, solute elements are homogenously distributed in the matrix. However, the relatively high hardness level measured after hot extrusion and heat treatment may be detrimental in case of additional cold processing which is required to produce final shape like thin plates or cladding tubes. An assessment of the cold workability and the effect of the degree of cold work by rolling on recrystallisation temperature are addressed here. It is found that this material can be successfully cold rolled with a high degree of cold work (up to 60% of thickness reduction) without any damage. According to optical micrographs and Differential Scanning Calorimetry (DSC) measurements, it seems that the recrystallisation temperature remains always very high (above 1400°C) even though cold work level increases (up to 66% of thickness reduction). However, the hardness values begin to decrease for heat treatment temperatures above 1200°C for hot worked conditions and below 1000°C for cold worked conditions, respectively.
Authors: I. Uytdenhouwen, R. Chaouadi, Jochen Linke, V. Massaut, G. Van Oost
Abstract: Tungsten and tungsten alloys are promising metals as protective materials for the armour in future fusion reactors. These metals exhibit the highest melting point, superior thermo-mechanical properties, low erosion and moderate neutron activation properties. The main drawback is their intrinsic brittleness at room temperature and their low recrystallization temperature. During thermal shock events in ITER, tungsten materials will exhibit various crack formations and failure mechanisms. The extensive heat loads on the surface of the material will create high thermal stresses, huge temperature rises and therefore large strain rates in the subsurface layers. This paper deals with the flow properties combining both temperature and strain rate effects of a lanthanum oxide dispersion strengthened tungsten material and the influence of grain orientation on its ductility. Promising results were obtained using a yield strength model based on a thermally-activated slip process that rationalizes the data.

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