Advanced Materials Research Vols. 89-91

Abstract: Plane strain compression tests have been carried out to investigate the variation of friction coefficient for the ferritic stainless steel, AISI 430, during single and multi pass hit deformation using glass lubricant and BN. A graphical method has been employed to evaluate the friction coefficient. It is found that the friction coefficient declines as strain increases under slip friction conditions with glass lubricant. On the contrary, under partial sticking friction condition with BN, the friction coefficient increases as strain increases. Furthermore, the variation of the friction coefficient on multipass hit is almost identical with single hit until the second pass, but the value of the friction coefficient on the third pass is slightly higher than that observed following single pass deformation.

Abstract: The mechanical characteristics of dentine have been investigated on local scale by micro-hardness and instrumented indentation tests. FIMEC, an indentation technique employing a cylindrical punch, permitted measurements of elastic modulus, yield stress, stress-relaxation and creep. The punch diameter (Φ = 0.5 mm) is much larger than the tubule size thus data are not so largely scattered as in micro- and nano-indentation tests but, at the same time, is small enough to guarantee a good resolution in mapping the mechanical properties in different tooth positions. The results are in agreement with literature data obtained by means of various experimental techniques. Furthermore, through tests of mechanical spectroscopy carried out on bar-shaped samples (13 mm x 4 mm x 0.8 mm) the dynamic modulus and the damping factor Q-1 have been measured.

Abstract: The precipitation behavior of nano–scale particles formed in Cu–base alloys was studied by means of transmission electron microscopy (TEM) and SQUID measurements. Linear arrangements of two or more nano–scale particles cubic in shape were observed in the <100> orientations of matrices in a Cu–Co alloy. Although the trend was less explicit in a Cu–Fe alloy, Fe precipitates accompanying twin–like lattice modulations were found in the decomposition, when no deformation was applied. The present SQUID measurements revealed several significant influences to magnetic properties were induced during the precipitation in Cu–base alloys. Lorentz electron microscopy confirmed that phase transformation from γ → α occurred at the stage that the Fe particles reach to 40~60nm in size.

Abstract: The tensile property and hydrogen embrittlement (HE) behavior in the submicrocrystalline ultra-low carbon steel produced by HPT straining were investigated. Elongated grains with 300 nm thickness and 600 nm length with high dislocation density were formed by the HPT straining at a rotation-speed of 0.2 rpm under a compression pressure of 5 GPa. The engineering tensile strength of the HPT processed ultra-low carbon steel for > 5 turns was 1.9 GPa, which is similar to the value of maraging high-alloy steels. The elongation increased with strain (at 5 to 10 turns), is caused by the reduction of the stress concentration due to the existence of continuously recrystallized grains. HE occurred in the HPT processed specimen for 5 turns with high tensile strength of 1.9 GPa under hydrogen atmosphere. However, its HE was suppressed via recovery process by annealing at low temperature while maintaining the high strength.

Abstract: The effect of Thermomechanical Processing (TMP) on the fine structure (dislocation density and fragments evolution), recrystallization, carbide transformations and tendency toward intercrystalline corrosion (ICC) and corrosion-mechanical strength of AISI 321 type steels is described. It’s shown that the grain size and overall amount of carbide phase has almost no effect on ICC. With an increase in dislocation density a tendency is observed toward a reduction in corrosion rate, but increases with an increase in proportion of recrystallized material. This connection is explained by an increasing of the level of local microstresses, which may be arranged structurally in the form of partial disclinations and aggravate ICC. A new test procedure was developed for estimating the corrosion-mechanical strength of steel. It follows from the obtained data that the hot working with the following accelerate cooling under industrial conditions does not develop a tendency toward corrosion cracking in 3% agueous NaCl solution.