Interdiffusion in single-phase couples was investigated at temperatures ranging from 1118 to 1583K (tables 31 and 32). The concentration distributions after annealing were determined by means of electron-probe micro-analysis. The interdiffusion coefficients were then calculated by using the Boltzmann-Matano method. No significant concentration dependence of interdiffusion was detected in either compound. The diffusivities could be described by relationships of the form:
TiAl: D (m2/s) = 0.00028 exp[-295(kJ/mol)/RT]
Ti3Al: D (m2/s) = 0.001 exp[-312(kJ/mol)/RT]
W.Sprengel, H.Nakajima, H.Oikawa: Materials Science and Engineering A, 1996, 213[1-2], 45-50
Table 31
Interdiffusion in TiAl
Temperature (K) |
D (m2/s)
|
1116 |
6.35 x 10-18 |
1165 | 1.09 x 10-17 |
1270 | 2.08 x 10-16 |
1270 | 2.85 x 10-16 |
1276 | 1.57 x 10-16 |
1371 | 1.54 x 10-15 |
1473 | 1.27 x 10-14 |
1473 | 1.10 x 10-14 |
1489 | 1.49 x 10-14 |
1583 | 3.92 x 10-14
|
Table 32
Interdiffusion in Ti3Al
Temperature (K) |
D (m2/s)
|
1171 |
1.2 x 10-17 |
1273 | 1.9 x 10-16 |
1327 | 5.3 x 10-16 |
1374 | 1.5 x 10-15 |
1404 | 2.8 x 10-15
|