The chronopotentiometric method was used to study the reaction, UIV + e → UIII, in molten 50 or 38.2mol%AlCl3 mixtures. For temperatures ranging from 250 to 400C (table 156), the activation energy for diffusion in the 50mol%AlCl3 mixture was calculated to be 5.4kcal/mol, while that for the 38.2mol%AlCl3 mixture was 4.1kcal/mol.
L.Martinot, T.Gerard, G.Duyckaerts: Inorganic and Nuclear Chemistry Letters, 1973, 9, 657-65
Table 156
Diffusivity of UIV in NaCl-AlCl3 Melts
Temperature (C) | AlCl3 (mol%) | D (cm2/s) |
250 | 50 | 5.1 x 10-5 |
250 | 38.2 | 7.1 x 10-5 |
300 | 50 | 7.5 x 10-5 |
300 | 38.2 | 9.5 x 10-5 |
350 | 50 | 1.1 x 10-4 |
350 | 38.2 | 1.5 x 10-4 |
400 | 50 | 1.6 x 10-4 |
400 | 38.2 | 1.7 x 10-4 |