Ultra-small-angle X-ray scattering data were obtained from deformed single-crystal Al samples. These data were consistent with recent theoretical predictions of scattering from dislocation walls, allowing quantitative microstructural parameters to be extracted.

Ultra Small-Angle X-Ray Scattering from Dislocation Structures. G.G.Long, L.E.Levine: Acta Crystallographica A, 2005, 61[6], 557-67