Hydrogen etching was carried out on the (00•1)-oriented 6H–SiC wafer at 1450 to
1650C. Surface topography and morphology was characterized by atomic force
microscopy. Optimal conditions were found, under which all scratches due to the
polishing process were efficiently removed and the atomically smooth, clean
surface of SiC(00•1) was achieved. The most characteristic elements observed on
the perfectly etched surface were straight-line steps of equal height and nearly the
same width. The atomic force microscopic imaging also revealed intrinsic defects
of the samples. Conditions were found for maintaining the saturation of etching
products on the surface at the level enabling the empty core dislocations to be
formed during etching. The observed population of the dislocations ranges between
107 and 108cm−2. Burgers vectors of the dislocations as evaluated on the basis of
Frank's model were equal to 2 or 3 lattice constants.
Empty Core Screw Dislocations Formed on 6H–SiC(0001) During Hydrogen
Etching. M.Grodzicki, P.Mazur, S.Zuber, G.Urbanik, A.Ciszewski: Thin Solid
Films, 2008, 516[21], 7530-7