The diffusion of magnesium was studied in GaN layers grown onto sapphire
substrate by atmospheric pressure metal-organic vapour-phase-epitaxy in a socalled
home-made reactor. Secondary ion mass spectroscopy was used to visualise
the Mg profiles in two kinds of multi-sublayer GaN structure. One structure was
grown with a variable flow of Ga precursor and the second one using a variable
growth temperature. In both cases, the Mg dopant precursor (Cp2Mg) flow was
kept constant. Using Fick's second law to fit the experimental secondary ion mass
spectroscopy data, an increasing and then a saturating Mg diffusion coefficient as a
function of Mg concentration was deduced. The Mg incorporation was found to
increase at lower growth rates, i.e. when the Ga precursor flow was reduced.
Furthermore, based upon the temperature-related behaviour, it was found that the
activation energy for Mg diffusion coefficient in GaN was 1.9eV. It was suggested
that Mg diffused via substitutional sites.
Magnesium Diffusion Profile in GaN Grown by MOVPE. Z.Benzarti, I.Halidou,
Z.Bougrioua, T.Boufaden, B.El Jani: Journal of Crystal Growth, 2008, 310[14],
3274-7