Regrowth of GaN buffer layer on nanoporous GaN at chamber temperatures of
750, 850 and 1000C were used to study the mechanism behind threading
dislocations reduction in the GaN film subsequently overgrown. The growth of a
100nm GaN buffer layer at 850C causes dislocations to bend into the underlying
GaN and annihilated at the interface of GaN buffer/nanoporous GaN. Thermal
treatment of nanoporous GaN in MOCVD growth chamber at 850 C in NH3 and N2
ambient leads to the pinning of the threading dislocations at its surface edge steps
by impurity -vacancy complexes of SiNx. The SiNx were formed by the impinging
adatoms of NH3 which interact with Si dangling bonds at the sub-grain boundaries
of the nanoporous Si-doped GaN. When the nanoporous GaN sample undergoes
rapid thermal annealing in N2 ambient, no effective filling of these voids were
observed and dislocations density was not substantial reduced. Regrowth of GaN at
850 C re-structured the nanoporous GaN, forming a SiNx complex at the voids or
pores which pinned dislocation propagation. This explained the mechanism behind
dislocation annihilation in regrown GaN on nanoporous GaN template with the use
of additional interfacial GaN buffer layer.
Threading Dislocations Annihilation in Regrown GaN Film on Nanoporous GaN
Template. C.B.Soh, H.Hartono, S.Y.Chow, S.J.Chua, S.Tripathy: Physica Status
Solidi), 2009, 6[S2], S699-702