It was noted that an idealized crystal structure for sapphire (α-Al2O3) (perfect
oxygen hcp packing, flat cation planes perpendicular to [00•1]) had been used by
Kronberg (1957) and many others over the past 50 years in order to describe basal
slip and basal twinning at the atomic level. However, it had been recognized over a
decade ago that the actual structure of sapphire allows much simpler atomic
mechanisms to be postulated for basal slip and basal twinning. These models were
supported by convincing arguments derived from chemical and structural
considerations. Recently, a climb-dissociated basal dislocation in the boundary of a
manufactured bicrystal was observed by atomic resolution transmission electron
microscopy. The images were interpreted as indicating non-stoichiometric charged
dislocation cores and it was inferred that, during dislocation motion on the basal
plane, the basal dislocations had to move according to a variant of Kronberg's
mechanism. This conclusion was difficult to reconcile, with (i) models based upon
the actual structure, (ii) weak-beam TEM images, which contradicted important
implications of this variant of Kronberg's model, (iii) implications concerning
dislocation motion in ionic materials, and (iv) the possibility that interface
dislocations can be subject to entirely different constraints than apply to gliding
lattice dislocations.
Do Moving Basal Dislocations in Sapphire (α-Al2O3) Have Non-Stoichiometric
Cores? K.P.D.Lagerlöf, J.Castaing, A.H.Heuer: Philosophical Magazine, 2009,
89[5], 489-99