It was noted that, in these ceramics, proton conductance was hampered by
microstructural defects that acted as barriers to hydrogen diffusion. Respective
contributions of bulk and grain boundaries to the overall conductivity was usually
found via impedance measurements but further information on hydrogen transport
could be obtained using nuclear micro-analysis based upon the use of MeV lightion
micro-beams. A contribution of ion-beam micro-analysis to the study of
hydrogen transport in BaCe0.9Y0.1O3 was reported. ERDA hydrogen profiling,
performed on partially hydrated samples at 200 and 500C, revealed concentration
gradients from which the diffusion coefficients could be derived with the help of a
simple Fickian diffusion model.
Hydrogen Diffusion in High Temperature Proton Conducting Ceramics. S.Sorieul,
S.Miro, M.Taillades-Jacquin, J.Dailly, F.Mauvy, M.H.Berger, P.Berger: Nuclear
Instruments and Methods in Physics Research B, 2008, 266[8], 1430-3