Films of Ba0.5Sr0.5TiO3 were grown heteroepitaxially onto (001) MgO substrates by
pulsed laser deposition to fabricate microwave phase shifters for the frequency
range: 45MHz to 50GHz. Both as-grown and ex situ annealed films had a cube-oncube
epitaxial relationship with <100> Ba0.5Sr0.5TiO3ǁ<100>MgO. Threading
dislocations were the predominant defects, mostly with Burgers vectors b = <101>.
Growth at 10-1 mbar oxygen pressure, compared to 10-4mbar, resulted in
significantly better properties. Ex situ annealing of the film grown at 0.1mbar
resulted in a reduction of 40% in threading dislocation density and a 40% increase
in dielectric tunability.
Effect of Growth Defects on Microwave Properties in Epitaxial Ba0.5Sr0.5TiO3 Thin
Films Grown on (001) MgO by Pulsed Laser Deposition. Y.Y.Tse, P.M.Suherman,
T.J.Jackson, I.P.Jones: Philosophical Magazine, 2008, 88[16], 2505-18